CN111956525A - Petal shower gel and preparation method thereof - Google Patents

Petal shower gel and preparation method thereof Download PDF

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Publication number
CN111956525A
CN111956525A CN202010982699.1A CN202010982699A CN111956525A CN 111956525 A CN111956525 A CN 111956525A CN 202010982699 A CN202010982699 A CN 202010982699A CN 111956525 A CN111956525 A CN 111956525A
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parts
water
stirring
petal
petals
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揭成渝
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Foshan Nanhai Guicheng Eifel Cosmetics Co ltd
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Foshan Nanhai Guicheng Eifel Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/463Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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    • A61Q19/10Washing or bathing preparations
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract

The invention provides petal shower gel and a preparation method thereof, wherein the petal shower gel is prepared from the following raw materials in parts by weight: 6.0-16 parts of sodium laureth sulfate, 0.5-3 parts of cocamide DEA, 0.5-4 parts of cocamidopropyl betaine, 0.5-2.5 parts of sodium chloride, 0.05-0.15 part of EDTA disodium, 0.1-0.5 part of preservative, 0.3-2.5 parts of essence, 0.01-1.0 part of fresh petals, 0.8-10 parts of suspending agent, 0.6-8 parts of triethanolamine and 60-80 parts of water. The invention solves the problems of disinfection, impurity removal, suspension, long-term complete appearance maintenance and the like of fresh flower petals in the shower gel, and leads the sold commodity shower gel to be more beautiful and more moist to skin; the preparation method has the advantages of simplifying the manufacturing process of the product, saving time, improving efficiency, reducing cost and energy consumption, having the function of environmental protection, improving quality, improving curative effect and the like.

Description

Petal shower gel and preparation method thereof
Technical Field
The invention relates to the technical field of shower gel and preparation thereof, in particular to petal shower gel and a preparation method thereof.
Background
The bath product is a cosmetic used by people for cleaning the skin of the whole body when people take a bath, and is a product with higher use frequency in daily life because of convenient use and abundant varieties which are favored by most people. The bath lotion is also called as bath lotion and refers to a liquid cleaning agent used during bathing, and the bath lotion does not have the rigid feeling like soap when contacting the skin of people. The rose petal bath lotion is developed by modern scientific technology until now. The petal shower gel literally enables people to think that the shower gel and the petals are combined together, think that people can smell the odor of fragrant petals emitted on the body of people, so that the bathing interest of people is increased, and after the people take a bath, the body is left with the petal fragrance, so that the skin can be whitened and moistened, and the petal shower gel is deeply welcomed by consumers. However, the petal shower gel has a plurality of problems in preparation, and the development of the petal shower gel is limited. For example: petal pretreatment, if the treatment is not good, bacteria can be brought in, and the storage and the quality of the shower gel are influenced. The integrity of the petals is ensured in the preparation process. How to ensure the dispersion degree of the petals and the fading of the petals when the petals are stored for a long time.
Patent application No. CN201810685491.6 discloses a petal shower gel and a preparation method thereof, and the formula comprises 10-20 parts of surfactant, 3.5-12 parts of suspending agent, 5-20 parts of humectant, 0.05-0.1 part of azomagenta, 0.1-0.5 part of titanium dioxide, 1-2 parts of forming agent, 0.2-1 part of skin care agent, 1-2 parts of preservative, 0.1-0.8 part of essence, 0.5-1 part of cherry petal and 50-70 parts of deionized water. The method comprises the following steps: step1, uniformly stirring part of deionized water, azoic fuchsin and titanium dioxide, adding cherry petals, continuously stirring, adding a suspending agent, and uniformly stirring to obtain a mixture A; step2, adding the rest deionized water into a stirring kettle, heating to 70 ℃, sequentially adding essence, surfactant, humectant, forming agent, skin care agent and preservative under stirring, and stirring uniformly to obtain a mixture B; and Step3, adding the mixture A into the mixture B, uniformly stirring, and adding a pH regulator to regulate the pH to 6.5 to obtain the petal shower gel. Titanium dioxide is needed for color protection, and in practical application, the titanium dioxide particles are round due to the addition of titanium dioxide, and the particle size is large, so that the transparency of the shower gel is reduced, and the petal presenting effect is influenced. In addition, the problems of suspension, defoaming, complete petals and the like are not considered in the preparation process, so that in the prepared shower gel, the petals are in a fine-crushed shape, few complete petals exist, and the petals cannot be uniformly distributed in the shower gel, mostly gather or float or sink, and when the shower gel is used, the holding bottle needs to be shaken to disperse the petals. Therefore, there is an urgent need for those skilled in the art to develop a new petal bath lotion formulation and a preparation method thereof to solve the problems of disinfection, impurity removal, suspension and long-term maintenance of intact appearance of fresh flower petals in the bath lotion.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides the petal shower gel and the preparation method thereof, which solve the problems of disinfection, impurity removal, suspension, long-term complete appearance maintenance and the like of the petals of the fresh flowers in the shower gel, and ensure that the sold commodity shower gel is more attractive and moister to the skin; the preparation method has the advantages of simplifying the manufacturing process of the product, saving time, improving efficiency, reducing cost and energy consumption, having the function of environmental protection, improving quality, improving curative effect and the like.
The technical scheme of the invention is realized as follows:
the petal shower gel is prepared from the following raw materials in parts by weight: 6.0-16 parts of sodium laureth sulfate, 0.5-3 parts of cocamide DEA, 0.5-4 parts of cocamidopropyl betaine, 0.5-2.5 parts of sodium chloride, 0.05-0.15 part of EDTA disodium, 0.1-0.5 part of preservative, 0.3-2.5 parts of essence, 0.01-1.0 part of fresh petals, 0.8-10 parts of suspending agent, 0.6-8 parts of triethanolamine and 60-80 parts of water.
Preferably, the feed is prepared from the following raw materials in parts by weight: 10 parts of sodium laureth sulfate, 1.25 parts of sodium laureth sulfate, 1.5 parts of cocamide DEA, 2 parts of cocamidopropyl betaine, 0.8 part of sodium chloride, 0.1 part of disodium EDTA, 0.4 part of preservative, 1.0 part of essence, 0.15 part of fresh petals, 6.4 parts of suspending agent, 1.4 parts of triethanolamine and 75 parts of water.
Preferably, the petals are one of jasmine petals, roses and cherry blossoms. .
Preferably, the preservative is DMDM hydantoin.
Preferably, the suspending agent is an acrylic acid (ester) copolymer.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shape, decolorizing with 70-80 deg.C water for 30-50min, cleaning impurities, sterilizing with 100 deg.C water for 30-50min, taking out, and draining;
(2) sequentially adding water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel, stirring at a stirring speed of 60-80r/min for 10-20min to dissolve uniformly;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at a stirring speed of 60-70r/min for 15-20min, wherein the sodium chloride is dissolved by water according to a weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the weight part ratio of the pigment to water is 1:200, and when the pigment is used, the pigment is uniformly dispersed by water; adding the petals processed in the step (1), stirring at a speed of 10-20r/min for 3-5min, heating to 50-60 ℃, keeping the temperature for 20-30min, adding a preservative and essence into the reaction container after defoaming and cooling to 25-45 ℃, stirring at a speed of 10-20r/min for 5-10 min;
(5) firstly, diluting a suspending agent by water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine by water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring for 10-20min at the speed of 10-20 r/min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
The invention has the following beneficial effects:
(1) the petal shower gel and the preparation method thereof select one of jasmine petals, roses and cherry blossom independently and are not mixed with other plant components because the petals of the jasmine, the rose and the cherry blossom are moderate in size and regular in shape, are very soft after treatment, have good moistening degree on skin, are easy to wash and cannot be adhered to the skin; when the petals are added, the petal shape can be guaranteed not to be damaged by adopting a slow speed, after superficial floating color removal treatment, the remained color is kept stable, the petals are not easy to change color and fade, and the shower gel is enabled to keep stable appearance for a long time. Adopt the disinfection to the petal to handle and prevent that the petal from taking place rotten in long-term storage, prevent remaining dust gravel on the petal simultaneously, guarantee that the shower bath deposits the stability of in-process system and petal for a long time. The invention solves the problems of disinfection, impurity removal, suspension, long-term complete appearance maintenance and the like of fresh flower petals in the shower gel, and leads the sold commodity shower gel to be more beautiful and more moist to skin.
(2) According to the petal shower gel and the preparation method thereof, when sodium chloride is added, the problem of uneven dispersion when the sodium chloride is directly added into a system can be solved by dissolving with water, and the petal treatment process can be synchronously carried out with the blending process of other raw materials, so that the preparation method simplifies the manufacturing process of the product, saves time, improves efficiency, reduces cost and energy consumption, has an environment protection function, improves quality, improves curative effect and the like.
Detailed Description
For a more clear understanding of the technical features, objects and advantages of the present invention, reference is now made to the following detailed description of the embodiments of the present invention taken in conjunction with the accompanying drawings, which are included to illustrate and not to limit the scope of the present invention.
Example 1
The petal shower gel is prepared from the following raw materials in parts by weight: 10 parts of sodium laureth sulfate, 1.25 parts of sodium laureth sulfate, 1.5 parts of cocamide DEA, 2 parts of cocamidopropyl betaine, 0.8 part of sodium chloride, 0.1 part of disodium EDTA (ethylene diamine tetraacetic acid), 0.4 part of preservative DMDM hydantoin, 1.0 part of essence, 0.15 part of fresh jasmine petals, 6.4 parts of suspending agent acrylic acid (ester) copolymer, 1.4 parts of triethanolamine and 75 parts of water.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shapes, decolorizing with 75 deg.C water for 40min, cleaning impurities, sterilizing with 100 deg.C water for 40min, taking out, and draining;
(2) adding 67 parts of water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel in sequence, stirring and dissolving uniformly, wherein the stirring speed is 70r/min, and the stirring time is 15 min;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at a stirring speed of 65r/min for 17min, wherein the sodium chloride is dissolved by water according to a weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the weight part ratio of the pigment to water is 1:200, and when the pigment is used, the pigment is uniformly dispersed by water; adding the petals processed in the step (1), stirring at a speed of 15r/min for 4min, heating to 55 ℃, keeping the temperature for 25min, adding a preservative and essence into the reaction container after defoaming and cooling to 35 ℃, and stirring at a speed of 15r/min for 8 min;
(5) firstly diluting a suspending agent with water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine with water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring for 15min at the speed of 15 r/min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Example 2
The petal shower gel is prepared from the following raw materials in parts by weight: 6.0 parts of sodium laureth sulfate, 3 parts of sodium laureth sulfate, 0.5 part of cocamide DEA, 4 parts of cocamidopropyl betaine, 0.5 part of sodium chloride, 0.15 part of disodium EDTA (ethylene diamine tetraacetic acid), 0.1 part of preservative DMDM hydantoin, 2.5 parts of essence, 0.01 part of fresh rose petals, 10 parts of suspending agent acrylic acid (ester) copolymer, 0.6 part of triethanolamine and 73 parts of water.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shape, decolorizing with 70 deg.C water for 30min, cleaning impurities, sterilizing with 100 deg.C water for 30-50min, taking out, and draining;
(2) adding 62 parts of water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel in sequence, stirring and dissolving uniformly, wherein the stirring speed is 60r/min, and the stirring time is 10 min;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at a stirring speed of 60r/min for 15min, wherein the sodium chloride is dissolved by water according to a weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the weight part ratio of the pigment to water is 1:200, and when the pigment is used, the pigment is uniformly dispersed by water; adding the petals processed in the step (1), stirring at a speed of 10r/min for 3min, heating to 50 ℃, keeping the temperature for 20min, adding a preservative and essence into the reaction container after defoaming and cooling to 25 ℃, and stirring at a speed of 10r/min for 5 min;
(5) firstly diluting a suspending agent with water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine with water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring at the speed of 10r/min for 10 min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Example 3
The petal shower gel is prepared from the following raw materials in parts by weight: 16 parts of sodium laureth sulfate, 0.5 part of sodium laureth sulfate, 3 parts of cocamide DEA, 0.5 part of cocamidopropyl betaine, 2.5 parts of sodium chloride, 0.05 part of disodium EDTA (ethylene diamine tetraacetic acid), 0.5 part of preservative DMDM hydantoin, 0.3 part of essence, 1.0 part of fresh cherry petals, 0.8 part of suspending agent acrylic acid (ester) copolymer, 8 parts of triethanolamine and 67 parts of water.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shapes, decolorizing with 80 deg.C water for 50min, cleaning impurities, sterilizing with 100 deg.C water for 50min, taking out, and draining;
(2) adding 56 parts of water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel in sequence, stirring at a stirring speed of 80r/min for 20min to dissolve uniformly;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at a stirring speed of 70r/min for 20min, wherein the sodium chloride is dissolved by water according to a weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the weight part ratio of the pigment to water is 1:200, and when the pigment is used, the pigment is uniformly dispersed by water; adding the petals processed in the step (1), stirring at a speed of 20r/min for 5min, heating to 60 ℃, keeping the temperature for 30min, adding a preservative and essence into the reaction container after defoaming and cooling to 45 ℃, and stirring at a speed of 20r/min for 10 min;
(5) firstly diluting a suspending agent by water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine by water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring for 20min at the speed of 20 r/min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Example 4
The petal shower gel is prepared from the following raw materials in parts by weight: 4.12 parts of sodium laureth sulfate, 1.5 parts of sodium laureth sulfate, 2 parts of cocamide DEA, 1.5 parts of cocamidopropyl betaine, 2 parts of sodium chloride, 0.1 part of disodium EDTA (ethylene diamine tetraacetic acid), 0.2 part of preservative DMDM hydantoin, 0.6 part of essence, 0.08 part of fresh jasmine petals, 0.9 part of suspending agent acrylic acid (ester) copolymer, 7 parts of triethanolamine and 80 parts of water.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shapes, decolorizing with 70 deg.C water for 50min, cleaning impurities, sterilizing with 100 deg.C water for 300min, taking out, and draining;
(2) adding 70 parts of water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel in sequence, stirring and dissolving uniformly, wherein the stirring speed is 60r/min, and the stirring time is 20 min;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at a stirring speed of 60r/min for 20min, wherein the sodium chloride is dissolved by water according to a weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the pigment and water are uniformly dispersed by water when the pigment is used, and the weight part ratio of the pigment to the water is 1: 200; adding the petals processed in the step (1), stirring at a speed of 10r/min for 5min, heating to 50 ℃, keeping the temperature for 30min, adding a preservative and essence into the reaction container after defoaming and cooling to 25 ℃, and stirring at a speed of 20r/min for 5 min;
(5) firstly diluting a suspending agent by water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine by water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring at the speed of 10r/min for 20 min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Example 5
The petal shower gel is prepared from the following raw materials in parts by weight: 11.66 parts of sodium laureth sulfate, 2 parts of sodium laureth sulfate, 2 parts of cocamide DEA, 3 parts of cocamidopropyl betaine, 2.3 parts of sodium chloride, 0.12 part of disodium EDTA (ethylene diamine tetraacetic acid), 0.4 part of preservative DMDM hydantoin, 1.5 parts of essence, 0.02 part of fresh jasmine petals, 9 parts of suspending agent acrylic acid (ester) copolymer, 8 parts of triethanolamine and 60 parts of water.
A preparation method of petal shower gel comprises the following steps:
(1) selecting fresh petals with complete shapes, decolorizing with 80 deg.C water for 30min, cleaning impurities, sterilizing with 100 deg.C water for 50min, taking out, and draining;
(2) adding 41 parts of water, disodium EDTA, sodium laureth sulfate and cocamide DEA into a reaction vessel in sequence, stirring and dissolving uniformly at a stirring speed of 80r/min for 10 min;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into a reaction container, uniformly stirring at the stirring speed of 70r/min for 15min, wherein the sodium chloride is dissolved by water according to the weight ratio of 1:1 and then added into the reaction container for use;
(4) adding a pigment into the reaction container, wherein the weight part ratio of the pigment to water is 1:200, and when the pigment is used, the pigment is uniformly dispersed by water; adding the petals processed in the step (1), stirring at a speed of 20r/min for 3min, heating to 60 ℃, keeping the temperature for 20min, adding a preservative and essence into the reaction container after defoaming and cooling to 45 ℃, and stirring at a speed of 10r/min for 10 min;
(5) firstly diluting a suspending agent by water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine by water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring for 10min at the speed of 20 r/min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
And carrying out performance index inspection on the product. The test results are listed in table 12.
Comparative example 1
Selecting the raw material proportion and the preparation method of the embodiment 1, and only having the difference that the flower petals with complete shapes directly selected in the step (1) are removed, and are not decolorized or disinfected, and are fished out and drained for later use; the other preparation steps are the same.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Comparative example 2
The raw material proportion and the preparation method of the embodiment 1 are selected, the only difference is that in the step (1), the selected flower petals with complete shapes are decolorized for 40min by water with the temperature of 75 ℃, and are not disinfected, fished out and drained for later use. The other preparation steps are the same.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Comparative example 3
Selecting the raw material proportion and the preparation method of the embodiment 1, and the only difference is that in the step (1), only the selected flower petals with complete shapes are directly cleaned without decolorization, and then sterilized by water with the temperature of 100 ℃ for 50min, and then fished out and drained for later use; the other preparation steps are the same.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Comparative example 4
The raw material proportion and the preparation method of the embodiment 1 are selected, the only difference is that the stirring speed after the petals are added in the step (4) is improved to 30r/min from 15r/min, and other preparation steps are the same.
And carrying out performance index inspection on the product. The test results are listed in table 1.
Comparative example 5
The raw material proportion and the preparation method of the embodiment 1 are selected, the only difference is that the petals are not added in the step (4), the petals are added at the last of the step (5), the stirring speed is 15r/min, the stirring time is 4min, and other preparation steps are the same.
And carrying out performance index inspection on the product. The test results are listed in table 1.
First, performance detection
The petal shapes and colors of the petal body washes obtained in examples 1 to 5 and comparative examples 1 to 2 were observed as shown in Table 1 below.
TABLE 1
Figure BDA0002688124720000121
As can be seen from Table 1, the petal shower gel prepared by the method has regular shape, the petal shape is not damaged, the remained color is kept stable, the petals are not easy to discolor and fade, the petals are uniformly dispersed in the shower gel, the transparency of the shower gel is good, the complete petals are better shown, and the commodity keeps long-term stable appearance. The invention solves the problems of disinfection, impurity removal, suspension, long-term complete appearance maintenance and the like of fresh flower petals in the shower gel, and leads the sold commodity shower gel to be more beautiful and more moist to skin.
The above embodiments are merely provided to help understand the method and core principle of the present invention, and the main steps and embodiments of the present invention are described in detail by using specific examples. To those skilled in the art, the various conditions and parameters may be varied as desired in a particular implementation in accordance with the principles of the invention, and in view of the foregoing, the description is not to be taken as limiting the invention.

Claims (10)

1. The petal shower gel is characterized in that: the feed is prepared from the following raw materials in parts by weight: 6.0-16 parts of sodium laureth sulfate, 0.5-3 parts of cocamide DEA, 0.5-4 parts of cocamidopropyl betaine, 0.5-2.5 parts of sodium chloride, 0.05-0.15 part of EDTA disodium, 0.1-0.5 part of preservative, 0.3-2.5 parts of essence, 0.01-1.0 part of fresh petals, 0.8-10 parts of suspending agent, 0.6-8 parts of triethanolamine and 60-80 parts of water.
2. The petal body wash of claim 1, wherein: the feed is prepared from the following raw materials in parts by weight: 10 parts of sodium laureth sulfate, 1.25 parts of sodium laureth sulfate, 1.5 parts of cocamide DEA, 2 parts of cocamidopropyl betaine, 0.8 part of sodium chloride, 0.1 part of disodium EDTA, 0.4 part of preservative, 1.0 part of essence, 0.15 part of fresh petals, 6.4 parts of suspending agent, 1.4 parts of triethanolamine and 75 parts of water.
3. The petal body wash of claim 1, wherein: the fresh petal is one of jasmine petal, rose and cherry blossom.
4. The petal body wash of claim 1, wherein: the preservative is DMDM hydantoin.
5. The petal body wash of claim 1, wherein: the suspending agent is acrylic acid (ester) copolymer.
6. A method for preparing a petal body wash according to any one of claims 1 to 5, which comprises the steps of: the method comprises the following steps:
(1) selecting fresh petals with complete shape, decolorizing with 70-80 deg.C water for 30-50min, cleaning impurities, sterilizing with 100 deg.C water for 30-50min, taking out, and draining;
(2) sequentially adding water, disodium EDTA, sodium laureth sulfate and DEA into a reaction vessel, and uniformly stirring and dissolving;
(3) sequentially adding the cocamidopropyl betaine, the sodium chloride and the essence into the reaction vessel and uniformly stirring;
(4) adding the petals processed in the step (1) into a reaction container, stirring at a speed of 10-20r/min for 3-5min, heating to 50-60 ℃, preserving heat for 20-30min, adding a preservative and essence into the reaction container after defoaming and cooling to 25-45 ℃, stirring at a speed of 10-20r/min for 5-10 min;
(5) firstly diluting a suspending agent with water according to the weight part ratio of 1:1, adding the suspending agent into a reaction container, diluting triethanolamine with water according to the weight part ratio of 1:1, adding the triethanolamine into the reaction container, and stirring at the speed of 10-20r/min for 10-20 min;
(6) sampling and analyzing, and testing the pH value to be 6.5-7.5 to obtain the finished product.
7. The preparation method of the petal body wash of claim 6, which is characterized in that: the stirring speed of the step (2) is 60-80r/min, and the stirring time is 10-20 min.
8. The preparation method of the petal body wash of claim 6, which is characterized in that: and (4) adding a pigment before adding the petals, wherein the weight part ratio of the pigment to water is 1:200, and the pigment is uniformly dispersed with water when in use.
9. The preparation method of the petal body wash of claim 6, which is characterized in that: in the step (3), sodium chloride is dissolved by water according to the weight part ratio of 1:1 and then added into a reaction vessel for use.
10. The preparation method of the petal body wash of claim 6, which is characterized in that: the stirring speed of the step (3) is 60-70r/min, and the stirring time is 15-20 min.
CN202010982699.1A 2020-09-17 2020-09-17 Petal shower gel and preparation method thereof Pending CN111956525A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102885030A (en) * 2012-10-29 2013-01-23 广州栋方日化有限公司 Method for maintaining stability of rose petals in faintly-acid or neutral cosmetic system
CN103263372A (en) * 2013-05-24 2013-08-28 苏州工业园区黎姿化妆品有限公司 Natural flower petal and cosmetic adopting same
CN103271856A (en) * 2013-05-28 2013-09-04 上海亚缇沐语生物科技有限公司 Jasmine flower shower gel and preparation method thereof
CN107912427A (en) * 2017-12-07 2018-04-17 广州栋方生物科技股份有限公司 A kind of flower used for cosmetic and its color-retention method
CN109820784A (en) * 2019-04-01 2019-05-31 贵州阿斯科科技开发有限公司 A kind of petal shower cream and preparation method thereof
CN109820783A (en) * 2019-03-22 2019-05-31 云南省农业科学院花卉研究所 A kind of discoloration method of plant petals
CN110251437A (en) * 2019-08-01 2019-09-20 广东嘉丹婷日用品有限公司 A kind of shower cream and preparation method thereof containing fresh flower petal

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102885030A (en) * 2012-10-29 2013-01-23 广州栋方日化有限公司 Method for maintaining stability of rose petals in faintly-acid or neutral cosmetic system
CN103263372A (en) * 2013-05-24 2013-08-28 苏州工业园区黎姿化妆品有限公司 Natural flower petal and cosmetic adopting same
CN103271856A (en) * 2013-05-28 2013-09-04 上海亚缇沐语生物科技有限公司 Jasmine flower shower gel and preparation method thereof
CN107912427A (en) * 2017-12-07 2018-04-17 广州栋方生物科技股份有限公司 A kind of flower used for cosmetic and its color-retention method
CN109820783A (en) * 2019-03-22 2019-05-31 云南省农业科学院花卉研究所 A kind of discoloration method of plant petals
CN109820784A (en) * 2019-04-01 2019-05-31 贵州阿斯科科技开发有限公司 A kind of petal shower cream and preparation method thereof
CN110251437A (en) * 2019-08-01 2019-09-20 广东嘉丹婷日用品有限公司 A kind of shower cream and preparation method thereof containing fresh flower petal

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