CN102559422A - Soapberry detergent and preparation method thereof - Google Patents
Soapberry detergent and preparation method thereof Download PDFInfo
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- CN102559422A CN102559422A CN2011103428883A CN201110342888A CN102559422A CN 102559422 A CN102559422 A CN 102559422A CN 2011103428883 A CN2011103428883 A CN 2011103428883A CN 201110342888 A CN201110342888 A CN 201110342888A CN 102559422 A CN102559422 A CN 102559422A
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- Prior art keywords
- seed
- pulp
- chinese soapberry
- sanitising agent
- soapberry fruit
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- 240000003377 Shepherdia canadensis Species 0.000 title abstract 15
- 235000018324 Shepherdia canadensis Nutrition 0.000 title abstract 15
- 239000003599 detergent Substances 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 2
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 72
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000001035 drying Methods 0.000 claims abstract description 19
- 241000580955 Sapindus mukorossi Species 0.000 claims description 109
- 239000003795 chemical substances by application Substances 0.000 claims description 88
- 239000000284 extract Substances 0.000 claims description 31
- 238000000034 method Methods 0.000 claims description 22
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 20
- 238000007670 refining Methods 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 16
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- BLSQLHNBWJLIBQ-OZXSUGGESA-N (2R,4S)-terconazole Chemical compound C1CN(C(C)C)CCN1C(C=C1)=CC=C1OC[C@@H]1O[C@@](CN2N=CN=C2)(C=2C(=CC(Cl)=CC=2)Cl)OC1 BLSQLHNBWJLIBQ-OZXSUGGESA-N 0.000 claims description 6
- 229940089256 fungistat Drugs 0.000 claims description 6
- 159000000000 sodium salts Chemical class 0.000 claims description 6
- 238000000746 purification Methods 0.000 claims description 5
- 229930183111 sapindoside Natural products 0.000 claims description 5
- 235000011194 food seasoning agent Nutrition 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 6
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract description 4
- 229930182490 saponin Natural products 0.000 abstract description 4
- 150000007949 saponins Chemical class 0.000 abstract description 4
- 239000012459 cleaning agent Substances 0.000 abstract 4
- 238000000605 extraction Methods 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 239000011259 mixed solution Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 5
- 235000017491 Bambusa tulda Nutrition 0.000 description 5
- 241001330002 Bambuseae Species 0.000 description 5
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 5
- 239000011425 bamboo Substances 0.000 description 5
- 238000004806 packaging method and process Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 3
- 210000000481 breast Anatomy 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- 235000021419 vinegar Nutrition 0.000 description 3
- 239000000052 vinegar Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 241000737241 Cocos Species 0.000 description 2
- 235000013162 Cocos nucifera Nutrition 0.000 description 2
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 229940097411 palm acid Drugs 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002453 shampoo Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- GJCOSYZMQJWQCA-UHFFFAOYSA-N 9H-xanthene Chemical compound C1=CC=C2CC3=CC=CC=C3OC2=C1 GJCOSYZMQJWQCA-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 241001116389 Aloe Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000002252 acyl group Chemical group 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 235000011399 aloe vera Nutrition 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229960001631 carbomer Drugs 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 229940094506 lauryl betaine Drugs 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- DVEKCXOJTLDBFE-UHFFFAOYSA-N n-dodecyl-n,n-dimethylglycinate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC([O-])=O DVEKCXOJTLDBFE-UHFFFAOYSA-N 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000001259 polydextrose Substances 0.000 description 1
- 229940035035 polydextrose Drugs 0.000 description 1
- 235000013856 polydextrose Nutrition 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- PFNFFQXMRSDOHW-UHFFFAOYSA-N spermine Chemical compound NCCCNCCCCNCCCN PFNFFQXMRSDOHW-UHFFFAOYSA-N 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 229940125725 tranquilizer Drugs 0.000 description 1
- 239000003204 tranquilizing agent Substances 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
Abstract
The invention provides a cleaning agent containing soapberry fruit or pulp and a preparation method thereof, wherein the cleaning agent containing soapberry fruit or pulp comprises a cleaning agent and refined soapberry fruit or pulp, the refined soapberry fruit or pulp comprises the following components in percentage by weight: the weight ratio of the cleaning agent to the refined soapberry fruit or pulp is 0.5/30-3/30, wherein the refined soapberry fruit or pulp is obtained by drying soapberry fruit, cleaning the soapberry fruit or the soapberry pulp with seed removed with ethanol solution or isopropanol solution, or taking out after immersing in the ethanol solution or isopropanol solution, and drying. Therefore, the detergent containing the soapberry fruit or the soapberry pulp is not easy to rot, and the soapberry saponin is continuously released during the use period because the detergent contains the natural soapberry fruit or the natural soapberry pulp.
Description
Technical field
The present invention relates to have the sanitising agent and the method for manufacture thereof of natural plant fruit, specifically, relate to the sanitising agent and the method for manufacture thereof that contain the Seed of Chinese Soapberry fruit.
Background technology
Early stage Seed of Chinese Soapberry is widely used in the aspect of cleaning decontamination.But along with progress of science and technology, after increasing petrochemical industry cleaning product came out, Seed of Chinese Soapberry just was substituted gradually.Yet for meeting environmental protection with healthy, the sanitising agent of being processed by natural material extensively gets consumer reception, so also is no lack of the cleaning supplies that natural materials such as containing each plant extract liquor or plant body is processed on the market in recent years.As contain the Seed of Chinese Soapberry fruit perfumed soap M370602, washing granule CN101659909A, herbage washing powder US5840669, contain the hair washing breast TW20094424 of Seed of Chinese Soapberry extract.
Bath oil, shampoo, clean hand breast, the milk of washing one's face etc. have the cleaning supplies that contain the pore forming material class; Often use ionogen such as artificial synthetic three celestial glue (Xanthan), CMC 99.5 (CMC), Natvosol (HEC), carbomer (Carbopol) or sodium salt, adjust the stickiness of sanitising agent.
General sanitising agent such as bath oil, shampoo, clean hand breast, cleansing milk or the like need to add the stickiness that viscosity increaser is adjusted sanitising agent mostly.Moreover though it is a lot of to contain the sanitising agent of Seed of Chinese Soapberry extract on the market, yet wherein contained plant extraction liquid hold-up proportion is often very low, even unreal.The human consumer also is difficult to contained by the outward appearance identification sanitising agent of Seed of Chinese Soapberry extract, and whether it contains the Seed of Chinese Soapberry extract really.
Mostly the cleaning supplies that contain Seed of Chinese Soapberry fruit or its pulp powder in addition are solid-like or powdery (like M370602, CN101659909A, US5840669).It is because undressed natural Seed of Chinese Soapberry fruit, and the storage life is often less than 3 months, make moist or after soaked the storage life shorter.Therefore if directly the interpolation Seed of Chinese Soapberry is to cleaning supplies, has poor stability, be easy to generate problem such as corruption.
Summary of the invention
Hence one can see that, and the above-mentioned sanitising agent that contains the Seed of Chinese Soapberry extract still remains to be improved.The present invention provides a kind of method of manufacture that contains the sanitising agent of Seed of Chinese Soapberry extract in order to solve above-mentioned shortcoming.The present invention utilizes gradation to add the stickiness that the Seed of Chinese Soapberry extract is adjusted sanitising agent, rather than adjusts the stickiness of sanitising agent through adding viscosity increaser (thickening material).The invention provides a kind of method of manufacture that contains the sanitising agent of Seed of Chinese Soapberry fruit or pulp, the Seed of Chinese Soapberry fruit or the pulp that are about to after refining are added in the sanitising agent that is divided in packaging vessel, place for some time, make it discharge sapindoside.The above-mentioned sapindoside that in the sanitising agent of packaging vessel, disengages, soapmaking mode in the promptly so-called bottle.
According to an aspect of the present invention; The invention provides a kind of method of manufacture that contains the sanitising agent of Seed of Chinese Soapberry fruit or pulp; The method of manufacture of said sanitising agent is with Seed of Chinese Soapberry fruit or pulp after Seed of Chinese Soapberry fruit or pulp process for purification are refining; With Seed of Chinese Soapberry fruit or the pulp after refining: sanitising agent with refining after the weight ratio of Seed of Chinese Soapberry fruit or pulp be that 0.5/30～3/30 ratio is added in the sanitising agent, place more than 15 days, make it discharge sapindoside; Said Seed of Chinese Soapberry fruit or pulp process for purification are earlier the Seed of Chinese Soapberry fruit to be carried out drying treatment; Again with the Seed of Chinese Soapberry fruit or remove the Seed of Chinese Soapberry pulp of kind of benevolence; Clean with ethanolic soln or aqueous isopropanol, or take out after immersing ethanolic soln or aqueous isopropanol, and make its drying.
Preferably, said drying treatment was meant under 80～120 ℃, with dry 8～12 hours of Seed of Chinese Soapberry fruit; Or with air seasoning Exposure to Sunlight 3～7 days.
Preferably, Seed of Chinese Soapberry fruit or pulp after refining: sanitising agent with refining after Seed of Chinese Soapberry fruit or the weight ratio of pulp be 2/30～3/30.
Preferably, said sanitising agent comprises the Seed of Chinese Soapberry extract that 3.5～10 weight parts are above at least.
Preferably, said sanitising agent comprises the sodium salt of 0.1～4 weight part, the zero(ppm) water of 55～75 weight parts, the interfacial agent of 3～23 weight parts, the glycerine of 3～12 weight parts, the multiple fat agent of 0.1～1.4 weight part, the fungistat and the above Seed of Chinese Soapberry extract of 3.5～10 weight parts of 0.05～0.35 weight part.
According to a further aspect in the invention, the invention provides a kind of sanitising agent that contains Seed of Chinese Soapberry fruit or pulp, Seed of Chinese Soapberry fruit or pulp after the said sanitising agent that contains Seed of Chinese Soapberry fruit or pulp comprises sanitising agent and makes with extra care; Wherein, Seed of Chinese Soapberry fruit or pulp after refining: sanitising agent with refining after Seed of Chinese Soapberry fruit or the weight ratio of pulp be 0.5/30～3/30; Seed of Chinese Soapberry fruit after said the making with extra care or pulp are meant and earlier the Seed of Chinese Soapberry fruit are carried out drying treatment; Again with the Seed of Chinese Soapberry fruit or remove the Seed of Chinese Soapberry pulp of kind of benevolence; Clean with ethanolic soln or aqueous isopropanol, or take out after immersing ethanolic soln or aqueous isopropanol, and make its drying.
Preferably, said sanitising agent comprises the Seed of Chinese Soapberry extract that 3.5～10 weight parts are above at least.
Preferably, said sanitising agent comprises the sodium salt of 0.1～4 weight part, the zero(ppm) water of 55～75 weight parts, the interfacial agent of 3～23 weight parts, the glycerine of 3～12 weight parts, the multiple fat agent of 0.1～1.4 weight part, the fungistat and the above Seed of Chinese Soapberry extract of 3.5～10 weight parts of 0.05～0.35 weight part.
Therefore, just can process the sanitising agent that contains natural Seed of Chinese Soapberry fruit or pulp through method provided by the invention, and since this Seed of Chinese Soapberry fruit or pulp through refinement treatment, therefore perishable not.
And owing to contain natural Seed of Chinese Soapberry fruit or pulp in the sanitising agent, sapindoside also can constantly disengage during use.It is different from through externally adding the mode in the sanitising agent again to after the extraction, through the mode of soapmaking in the bottle, can let the user clearly see disengaging of saponin(e.
In addition, the sanitising agent that the present invention processes generally cleans the purposes (for example: skin, hair, clothing, vegetables and fruits cleaning or other clean purposes) except can be used for, and the goods of the present invention of low stickiness also can be used as the sanitising agent of makeup removing usefulness.
Embodiment
Contain the manufacturing of the sanitising agent of Seed of Chinese Soapberry extract:
At normal temperatures; 0.1～4 weight part (is preferably 1～2 weight part; More preferably be 2 weight parts) sodium salt be added to 55～75 weight parts and (be preferably 60～70 weight parts; More preferably be 65～67 weight parts) zero(ppm) water in, stir make its dissolving after, add 3～23 weight parts and (be preferably 8～17 weight part teepols and 3～10 weight part both sexes interfacial agents; More preferably be 10～15 weight part teepols and 5～8 weight part both sexes interfacial agents) interfacial agent, and stir.Then add 3～12 weight parts and (be preferably 4～11 weight parts according to order; More preferably be 5～10 weight parts) the multiple fat agent, fungistat (being preferably 0.1～0.25 weight part) back of 0.05～0.35 weight part of glycerine, 0.1～1.4 weight part (being preferably 0.15～1.15 weight part) form mixed solution; Again by needed stickiness with addition manner repeatedly; 3.5～10 weight parts (are preferably 4.5～7 weight parts; More preferably be 4.5 weight parts) the Seed of Chinese Soapberry extract add in the above-mentioned mixed solution, form the sanitising agent contain the Seed of Chinese Soapberry extract.Also can optionally add various additives in right amount simultaneously, for example: bamboo vinegar liquid, bamboo carbon powder, aloe or essential oil or the like according to its needed purpose.Wherein the particle size of bamboo carbon powder must be preferably 12000 sieve meshes greater than 2000 sieve meshes.
Wherein this interfacial agent comprises at least a in employed teepol of general sanitising agent and the both sexes interfacial agent.Wherein the preferred anionic surfactants interfacial agent comprise that bay ether sodium sulfate, alkyl poly-dextrose are sweet, at least a in the interfacial agent of acyl group musculamine acid sodium and Amino acid system.Wherein preferred both sexes interfacial agent comprises at least a in AMONYL 380LC, cocoyl-trimethyl-glycine and the lauryl betaine.
The wherein above-mentioned multiple fat agent of using as the foam tranquilizer preferably includes at least a in coconut monoethanolamide DEA, VT 18 acid amides DEA and the PEG-7 coconut palm acid glycerol.
Wherein above-mentioned fungistat preferably includes at least a in phenylformic acid formicester, methylchloroisothiazandnone and the methylisothiazolinone.
Wherein the Seed of Chinese Soapberry extract obtain the extraction process (CN1056525A, CN101225349A, spy open 2000-192089, I302101) that can use general industry commonly used, as: with water as extraction solvent; Or extract with cold extraction mode, promptly with low boiling point organic solvent (as: C1～C4 alcohols or C2～C5 ester class) as extraction solvent, and the extraction liquid distillation obtained extract.
Seed of Chinese Soapberry fruit or pulp process for purification:
Cause the fruit or the putrid factor of pulp easily for making Seed of Chinese Soapberry ability prolonged preservation, removing, the present invention carries out drying treatment with the Seed of Chinese Soapberry fruit and cleans.This drying treatment can use general drying treatment mode commonly used to carry out, for example: under 80～120 ℃, (be preferably 80～100 ℃) with drying machine, go through 8～12 hours (being preferably 8～10 hours), make its dry moisture of removing; Or, make its dry moisture of removing with air seasoning Exposure to Sunlight 3～7 days.
Optionally further with the Seed of Chinese Soapberry fruit or through removing the Seed of Chinese Soapberry pulp of kind of benevolence; Clean with alcohol solution (normal use like ethanolic soln or aqueous isopropanol); Or immerse alcohol solution (normal use like ethanolic soln or aqueous isopropanol) back and take out and carry out 1 time or repeatedly for several times, and make its drying.
Contain the manufacturing of the sanitising agent of Seed of Chinese Soapberry pulp:
After the sanitising agent that will contain the Seed of Chinese Soapberry extract is sub-packed in packaging vessel; Seed of Chinese Soapberry fruit after refining or pulp are directly added in the sanitising agent that contains the Seed of Chinese Soapberry extract after the packing, make (Seed of Chinese Soapberry fruit or pulp): (sanitising agent and Seed of Chinese Soapberry fruit or pulp) weight ratio=0.5/30～3/30, placement for some time (is good more than 15 days; Better more than 30 days; But can not be above 5 years), make its saponin(e that disengages Seed of Chinese Soapberry naturally, the sanitising agent of employed Seed of Chinese Soapberry extract is not limited to the sanitising agent that contains the Seed of Chinese Soapberry extract that the present invention manufactures in the method for manufacture; As long as when not hindering flesh and blood of the present invention, can adopt other sanitising agent.Just; Aforementioned proportion is merely the ratio of preferred exemplary; It still can be according to the ratio of required situation adjustment Seed of Chinese Soapberry fruit or pulp, as long as just the present invention makes (Seed of Chinese Soapberry fruit or pulp): effect of the present invention can be reached in (sanitising agent and Seed of Chinese Soapberry fruit or pulp) >=0.5/30.
Embodiment 1
In normal temperature, the sodium-chlor of 2 weight parts is added in the zero(ppm) water of 65 weight parts, stir make its dissolving after, add the bay ether sodium sulfate of 15 weight parts and the AMONYL 380LC of 8 weight parts, and stir.Form mixed solution after then adding the methylisothiazolinone of methylchloroisothiazandnone and 0.05 weight part of phenylformic acid formicester, 0.05 weight part of coconut monoethanolamide DEA, 0.15 weight part of glycerine, 0.15 weight part of 5 weight parts according to order; Again the Seed of Chinese Soapberry extract of about 4.5 weight parts is added in the above-mentioned mixed solution with addition manner repeatedly, and adds 0.1 weight part bamboo vinegar and form the sanitising agent that contains the Seed of Chinese Soapberry extract.
Embodiment 2
In normal temperature, the sodium-chlor of 2 weight parts is added in the zero(ppm) water of 67 weight parts, stir make its dissolving after, add the bay ether sodium sulfate of 10 weight parts and the AMONYL 380LC of 5 weight parts, and stir.Form mixed solution after then adding the methylisothiazolinone of methylchloroisothiazandnone and 0.05 weight part of phenylformic acid formicester, 0.05 weight part of PEG-7 coconut palm acid glycerol, 0.15 weight part of coconut monoethanolamide DEA, 1 weight part of glycerine, 0.15 weight part of 10 weight parts according to order; Again with the Seed of Chinese Soapberry extract of about 4.5 weight parts with addition manner repeatedly; Be added in the above-mentioned mixed solution, and the bamboo vinegar that adds 0.1 weight part forms the sanitising agent contain the Seed of Chinese Soapberry extract.
Embodiment 3
With the Seed of Chinese Soapberry fruit with three board throughcirculation dryer SKS-48CA of a specified duration 90 ℃ of dryings 10 hours, again the Seed of Chinese Soapberry pulp is separated with kind of benevolence.With taking-up immediately behind the Seed of Chinese Soapberry pulp immersion ethanolic soln, and make its drying.
After the sanitising agent branch that will contain the Seed of Chinese Soapberry extract is filled to packaging vessel; Get and contain in the sanitising agent of Seed of Chinese Soapberry extract after Seed of Chinese Soapberry pulp after refining directly adds packing; Make (Seed of Chinese Soapberry pulp): (sanitising agent and Seed of Chinese Soapberry pulp)=1: 30; Place more than 30 days, make the sanitising agent that contains Seed of Chinese Soapberry pulp.
Embodiment 4
Except making (Seed of Chinese Soapberry pulp): (sanitising agent and Seed of Chinese Soapberry pulp)=2: 30, all the other embodiments carry out with embodiment 3.
Embodiment 5
To rock by embodiment 3, the 4 prepared sanitising agents that contain Seed of Chinese Soapberry pulp, make the base section that contains higher saponin constituent and the sanitising agent uniform mixing on top, can obtain the sanitising agent of low stickiness.
What need statement is that foregoing invention content and embodiment are intended to prove the practical application of technical scheme provided by the present invention, should not be construed as the qualification to protection domain of the present invention.Those skilled in the art are in spirit of the present invention and principle, when doing various modifications, being equal to replacement or improvement.Protection scope of the present invention is as the criterion with appended claims.
Claims (8)
1. method of manufacture that contains the sanitising agent of Seed of Chinese Soapberry fruit or pulp; It is characterized in that; The method of manufacture of said sanitising agent is with Seed of Chinese Soapberry fruit or pulp after Seed of Chinese Soapberry fruit or pulp process for purification are refining; According to Seed of Chinese Soapberry fruit or the pulp after refining: sanitising agent with refining after the weight ratio of Seed of Chinese Soapberry fruit or pulp be that 0.5/30～3/30 ratio is added in the sanitising agent, place more than 15 days, make it discharge sapindoside; Said Seed of Chinese Soapberry fruit or pulp process for purification are earlier the Seed of Chinese Soapberry fruit to be carried out drying treatment; Again with the Seed of Chinese Soapberry fruit or remove the Seed of Chinese Soapberry pulp of kind of benevolence; Clean with ethanolic soln or aqueous isopropanol, or take out after immersing ethanolic soln or aqueous isopropanol, and make its drying.
2. method of manufacture as claimed in claim 1 is characterized in that, said drying treatment is meant under 80～120 ℃, with dry 8～12 hours of Seed of Chinese Soapberry fruit; Or with air seasoning Exposure to Sunlight 3～7 days.
3. according to claim 1 or claim 2 method of manufacture is characterized in that, Seed of Chinese Soapberry fruit or pulp after refining: sanitising agent with refining after Seed of Chinese Soapberry fruit or the weight ratio of pulp be 2/30～3/30.
4. according to claim 1 or claim 2 method of manufacture is characterized in that, said sanitising agent comprises the Seed of Chinese Soapberry extract that 3.5～10 weight parts are above at least.
5. according to claim 1 or claim 2 method of manufacture; It is characterized in that said sanitising agent comprises the sodium salt of 0.1～4 weight part, the zero(ppm) water of 55～75 weight parts, the interfacial agent of 3～23 weight parts, the glycerine of 3～12 weight parts, the multiple fat agent of 0.1～1.4 weight part, the fungistat and the above Seed of Chinese Soapberry extract of 3.5～10 weight parts of 0.05～0.35 weight part.
6. a sanitising agent that contains Seed of Chinese Soapberry fruit or pulp is characterized in that, Seed of Chinese Soapberry fruit or pulp after the said sanitising agent that contains Seed of Chinese Soapberry fruit or pulp comprises sanitising agent and makes with extra care; Wherein, Seed of Chinese Soapberry fruit or pulp after refining: sanitising agent with refining after Seed of Chinese Soapberry fruit or the weight ratio of pulp be 0.5/30～3/30; Seed of Chinese Soapberry fruit after said the making with extra care or pulp are meant and earlier the Seed of Chinese Soapberry fruit are carried out drying treatment; Again with the Seed of Chinese Soapberry fruit or remove the Seed of Chinese Soapberry pulp of kind of benevolence; Clean with ethanolic soln or aqueous isopropanol, or take out after immersing ethanolic soln or aqueous isopropanol, and make its drying.
7. the sanitising agent that contains Seed of Chinese Soapberry fruit or pulp as claimed in claim 6 is characterized in that, said sanitising agent comprises the Seed of Chinese Soapberry extract that 3.5～10 weight parts are above at least.
8. the sanitising agent that contains Seed of Chinese Soapberry fruit or pulp as claimed in claim 6; It is characterized in that said sanitising agent comprises the sodium salt of 0.1～4 weight part, the zero(ppm) water of 55～75 weight parts, the interfacial agent of 3～23 weight parts, the glycerine of 3～12 weight parts, the multiple fat agent of 0.1～1.4 weight part, the fungistat and the above Seed of Chinese Soapberry extract of 3.5～10 weight parts of 0.05～0.35 weight part.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW099142091 | 2010-12-03 | ||
| TW99142091A TW201113063A (en) | 2010-12-03 | 2010-12-03 | Sapindus detergent and method for manufacturing the same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102559422A true CN102559422A (en) | 2012-07-11 |
| CN102559422B CN102559422B (en) | 2013-10-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110342888 Active CN102559422B (en) | 2010-12-03 | 2011-11-03 | Soapberry detergent and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN102559422B (en) |
| TW (1) | TW201113063A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103122287A (en) * | 2013-03-26 | 2013-05-29 | 西南大学 | Soapberry total-nutrient handmade soap and preparation method thereof |
| CN105316119A (en) * | 2015-10-20 | 2016-02-10 | 成都市三禾田生物技术有限公司 | Sapindoside infant laundry detergent and preparation method thereof |
| CN109010211A (en) * | 2018-09-21 | 2018-12-18 | 张惠柳 | It is a kind of for preventing and treating the facial cleanser of subcutaneous fat tumor |
| CN110075013A (en) * | 2019-05-28 | 2019-08-02 | 上海思珥生物科技有限公司 | A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101225349A (en) * | 2007-01-18 | 2008-07-23 | 郭景龙 | Liquid detergent and method for preparing same |
-
2010
- 2010-12-03 TW TW99142091A patent/TW201113063A/en unknown
-
2011
- 2011-11-03 CN CN 201110342888 patent/CN102559422B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101225349A (en) * | 2007-01-18 | 2008-07-23 | 郭景龙 | Liquid detergent and method for preparing same |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103122287A (en) * | 2013-03-26 | 2013-05-29 | 西南大学 | Soapberry total-nutrient handmade soap and preparation method thereof |
| CN105316119A (en) * | 2015-10-20 | 2016-02-10 | 成都市三禾田生物技术有限公司 | Sapindoside infant laundry detergent and preparation method thereof |
| CN105316119B (en) * | 2015-10-20 | 2018-10-09 | 成都市三禾田生物技术有限公司 | A kind of sapindoside Infant laundry detergent and preparation method thereof |
| CN109010211A (en) * | 2018-09-21 | 2018-12-18 | 张惠柳 | It is a kind of for preventing and treating the facial cleanser of subcutaneous fat tumor |
| CN110075013A (en) * | 2019-05-28 | 2019-08-02 | 上海思珥生物科技有限公司 | A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201113063A (en) | 2011-04-16 |
| TWI350191B (en) | 2011-10-11 |
| CN102559422B (en) | 2013-10-30 |
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