CN103122287A - Soapberry total-nutrient handmade soap and preparation method thereof - Google Patents
Soapberry total-nutrient handmade soap and preparation method thereof Download PDFInfo
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- CN103122287A CN103122287A CN2013100987502A CN201310098750A CN103122287A CN 103122287 A CN103122287 A CN 103122287A CN 2013100987502 A CN2013100987502 A CN 2013100987502A CN 201310098750 A CN201310098750 A CN 201310098750A CN 103122287 A CN103122287 A CN 103122287A
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Abstract
The invention discloses a soapberry total-nutrient handmade soap which comprises the following components in parts by mass: 1.75 parts of soapberry total-nutrient solution, 1.5 parts of olive oil, 2.5 parts of palm oil, 1 part of coconut oil and 0.75 part of sodium hydroxide; and 0.1-0.2 part of soapberry shell powder or 0.1-0.3 part of soapberry extract also can be added. The handmade soap disclosed by the invention has a brown color; no other pigment is added, and the nutrient components of the soapberry are maintained at the same time; and apart from a healthcare effect, the handmade soap realizes a cleaning effect as well as an effect of killing and suppressing staphylococcus aureus, salmonella and escherichia coli. The soapberry total-nutrient handmade soap disclosed by the invention is gentle to skin, ensures exquisite foaming and can avoid irritating harm to skin caused by chemical substances and reduce the aging degree of skin. According to the invention, the production technology is simple, and the production cost is low.
Description
Technical field
The present invention relates to the articles for washing processing technique field, particularly relate to the making method of the full nutrition handmade soap of a kind of Seed of Chinese Soapberry.
Background technology
Seed of Chinese Soapberry (
Sapindus mukurossiGaertn
.), belong to the fallen leaves megaphanerophyte of Sapindaceae Sapindus, be commonly called as oil and suffer from son, fertile pearl etc., mainly originate in China Yangtze valley reach on the south wide geographic area, the use of Chang Zuowei washing among the people.Containing abundant glucosides class material in Seed of Chinese Soapberry, be mainly triterpene saponin, account for the 4-6% of shell, is a kind of nonionic surface active agent of natural degradable, and it reduces capillary ability and even is better than some synthetic surfactant.In addition, also contain in the Seed of Chinese Soapberry shell and enrich natural nutrition conditioning material, as tea-polyphenol, forulic acid, tartaric acid, a large amount of vitamins C and sugar etc., have antibiotic, anti-inflammatory, whitening, the function such as anti-dandruff, antipruritic.
There are some researches show, stronger through its surfactivity of Seed of Chinese Soapberry juice of ultrasonic extraction, the soil removability of deoiling is better than commercial washing composition, and poisonous element arsenic, cadmium, mercury, the lead amount of this extracting solution are lower.Seed of Chinese Soapberry surfactant through extracting has very low micelle-forming concentration and surface tension, illustrates that its surfactivity is strong.The Seed of Chinese Soapberry surfactant can produce foam in the deionized water of lower concentration, and the foam lasting stability.
China's Seed of Chinese Soapberry shell aboundresources, the existing Seed of Chinese Soapberry shell that develops mainly concentrates on separation, purification sapindoside, is used for the aspects such as washing, medicine, farm chemical emulgent.So far, there is no the report of the full nutrition handmade soap of Seed of Chinese Soapberry aspect, the full nutrition handmade soap of Seed of Chinese Soapberry has very wide market outlook.
Summary of the invention
In view of this, the object of the present invention is to provide full nutrition handmade soap of a kind of Seed of Chinese Soapberry and preparation method thereof.
The full nutrition handmade soap of Seed of Chinese Soapberry of the present invention, the mass fraction of its component and each component is:
1.75 parts of Seed of Chinese Soapberry pancebrins, 1.5 parts, sweet oil, 2.5 parts of plam oils, 1 part of Oleum Cocois, 0.75 part, sodium hydroxide.
Also contain Seed of Chinese Soapberry shell powder 0.1-0.2 part or Seed of Chinese Soapberry medicinal extract 0.1-0.3 part in the full nutrition handmade soap of described Seed of Chinese Soapberry.
The making method of the full nutrition handmade soap of Seed of Chinese Soapberry of the present invention realizes successively as follows:
(1) by described mass fraction, the Seed of Chinese Soapberry pancebrin is slowly poured in sodium hydroxide, the limit bevelling stirs, until sodium hydroxide dissolves fully, gets Seed of Chinese Soapberry pancebrin alkali lye, is cooled to 40-50 ℃ of insulation;
(2) by described mass fraction, with sweet oil, plam oil, Oleum Cocois Hybrid Heating, after liquefy, stopped heating gets mixing oil, is cooled to 40-50 ℃ of insulation;
(3) Seed of Chinese Soapberry pancebrin alkali lye is slowly poured in mixing oil, the limit bevelling stirs, until reaction mass thickens;
(4) reaction mass is poured in mould, with plastics film, mould is built, in 30-40 ℃ of insulation 24 hours, get the full nutrition handmade soap of Seed of Chinese Soapberry;
(5) demoulding and the full nutrition handmade soap of gained Seed of Chinese Soapberry is put in shady and cool place's saponification 4-12 week, packing gets product.
After step (3) reaction mass thickens, can add Seed of Chinese Soapberry shell powder or Seed of Chinese Soapberry medicinal extract by described mass fraction, and mix.
Different seasons is different because of envrionment temperature, and the ripe required time of handmade soap saponification was not waited in 4-12 week.Envrionment temperature is high, and the ripe required time of saponification is short; Envrionment temperature is low, and the ripe required time of saponification is long.
The preparation method of Seed of Chinese Soapberry pancebrin is as follows:
Get the Seed of Chinese Soapberry shell, 80 ℃ of oven dry add Seed of Chinese Soapberry shell quality 3-4 water doubly, and (pressure is under 500～600mmHg) conditions in decompression, ebuillition of heated, extracted 1.5 hours, and filtered reserved filtrate, filter residue adds Seed of Chinese Soapberry shell quality 3-4 water doubly to extract with under condition again, repeat 3 times, then merging filtrate is concentrated into filtrate 3 times and adds 1/2nd of water total mass, namely obtains the Seed of Chinese Soapberry pancebrin.
The Seed of Chinese Soapberry shell is pulverized 400 mesh sieves namely got Seed of Chinese Soapberry shell powder
The preparation method of Seed of Chinese Soapberry medicinal extract is as follows:
Get the Seed of Chinese Soapberry shell, 80 ℃ of oven dry are crushed to 100 orders, add the soaked in absolute ethyl alcohol of 10 times of Seed of Chinese Soapberry shell quality to extract 24h, suction filtration, and reserved filtrate, ethanol is removed in underpressure distillation, namely gets Seed of Chinese Soapberry medicinal extract.
The full nutrition handmade soap of Seed of Chinese Soapberry of the present invention washing effect is splendid, can be used for washing one's face, has one's hair wash, has a bath.
The invention has the advantages that:
The full nutrition handmade soap of Seed of Chinese Soapberry not only plays the cleaning effect, and streptococcus aureus, Salmonellas and intestinal bacteria are had kills and restraining effect.In addition, the tea-polyphenol in Seed of Chinese Soapberry is water-soluble substances, washes one's face with it and can remove facial grease, convergence pore, can sterilization, sterilization, resisting age of skin, can reduce the radiation of daylight middle-ultraviolet lamp to the damage of skin etc.; Forulic acid in Seed of Chinese Soapberry is the cosmetic factors that scientific circles generally acknowledge, can improve skin quality, makes its exquisiteness, gloss, high resilience, antibiotic, anti-inflammatory in addition simultaneously, anti-oxidant, remove the effects such as free radical, anticoagulation; Tartaric acid in Seed of Chinese Soapberry can help skin removed to be deposited in outer field aging cutin, accelerates skin renewal, helps improve skin comedo, blackspot, wrinkle, xerosis cutis, the skin problem such as coarse etc.Meet modern people to the pursuit of the articles for washing of natural, ecosystem.
The Seed of Chinese Soapberry shell itself carries brown, therefore keep itself color.Compare with at present commercially available perfumed soap, this soap is different with it is, at first keeps the natural color of Seed of Chinese Soapberry, there is no the interpolation of other pigments; Secondly, keep as far as possible the nutritive ingredient of Seed of Chinese Soapberry itself in handmade soap; Moreover handmade soap can produce 25% glycerine in making processes, makes it more to moisten, moisturizing.
The full nutrition handmade soap of Seed of Chinese Soapberry is gentle to skin, foaming is fine and smooth, can avoid chemical substance to the stimulation injury of skin, reduces the degree of aging of skin.Production technique of the present invention is simple, and production cost is low.
Embodiment
Embodiment 1:
Get Seed of Chinese Soapberry shell 100Kg, 80 ℃ of oven dry add 400 Kg water, (pressure is under 500～600mmHg) conditions in decompression, ebuillition of heated extracted 1.5 hours, filtered reserved filtrate, filter residue adds 300 Kg waters to extract with under condition again, filter reserved filtrate, filter residue adds under 300 Kg water same pieces again and extracts, merging filtrate, then filtrate is concentrated into 500 Kg, namely obtains the Seed of Chinese Soapberry pancebrin.
Get Seed of Chinese Soapberry shell 100Kg, 80 ℃ of oven dry are crushed to 100 orders, add the 1000Kg soaked in absolute ethyl alcohol to extract 24h, suction filtration, and reserved filtrate, ethanol is removed in underpressure distillation, namely gets Seed of Chinese Soapberry medicinal extract.
Seed of Chinese Soapberry shell 100Kg is pulverized 400 mesh sieves namely got Seed of Chinese Soapberry shell powder
Embodiment 2:
(1) Seed of Chinese Soapberry pancebrin 17.5 Kg are slowly poured in 7.5Kg sodium hydroxide, the limit bevelling stirs, until sodium hydroxide dissolves fully, gets Seed of Chinese Soapberry pancebrin alkali lye, is cooled to 45 ℃ of insulations;
(2) with sweet oil 15Kg, plam oil 25 Kg, Oleum Cocois 10Kg Hybrid Heating, after liquefy, stopped heating gets mixing oil, is cooled to 50 ℃ of insulations;
(3) Seed of Chinese Soapberry pancebrin alkali lye is slowly poured in mixing oil, the limit bevelling stirs, until reaction mass thickens;
(4) reaction mass is poured in mould, with plastics film, mould is built, in 30-40 ℃ of insulation 24 hours, get the full nutrition handmade soap of Seed of Chinese Soapberry;
(5) demoulding and the full nutrition handmade soap of gained Seed of Chinese Soapberry is put in shady and cool place 4 weeks of saponification, packing gets product.
Embodiment 3:
(1) Seed of Chinese Soapberry pancebrin 175 Kg are slowly poured in 75Kg sodium hydroxide, the limit bevelling stirs, until sodium hydroxide dissolves fully, gets Seed of Chinese Soapberry pancebrin alkali lye, is cooled to 50 ℃ of insulations;
(2) with sweet oil 150Kg, plam oil 250 Kg, Oleum Cocois 100Kg Hybrid Heating, after liquefy, stopped heating gets mixing oil, is cooled to 45 ℃ of insulations;
(3) Seed of Chinese Soapberry pancebrin alkali lye is slowly poured in mixing oil, the limit bevelling stirs, until reaction mass thickens, then adds Seed of Chinese Soapberry shell powder 20Kg and mixes;
(4) reaction mass is poured in mould, with plastics film, mould is built, in 30-40 ℃ of insulation 24 hours, get the full nutrition handmade soap of Seed of Chinese Soapberry;
(5) demoulding and the full nutrition handmade soap of gained Seed of Chinese Soapberry is put in shady and cool place 8 weeks of saponification, packing gets product.
Embodiment 4:
(1) Seed of Chinese Soapberry pancebrin 17.5Kg is slowly poured in 7.5Kg sodium hydroxide, the limit bevelling stirs, until sodium hydroxide dissolves fully, gets Seed of Chinese Soapberry pancebrin alkali lye, is cooled to 40 ℃ of insulations;
(2) with sweet oil 15Kg, plam oil 25 Kg, Oleum Cocois 10 Kg Hybrid Heating, after liquefy, stopped heating gets mixing oil, is cooled to 40 ℃ of insulations;
(3) Seed of Chinese Soapberry pancebrin alkali lye is slowly poured in mixing oil, the limit bevelling stirs, until reaction mass thickens, then adds Seed of Chinese Soapberry medicinal extract 3Kg and mixes;
(4) reaction mass is poured in mould, with plastics film, mould is built, in 30-40 ℃ of insulation 24 hours, get the full nutrition handmade soap of Seed of Chinese Soapberry;
(5) demoulding and the full nutrition handmade soap of gained Seed of Chinese Soapberry is put in shady and cool place 12 weeks of saponification, packing gets product.
Claims (3)
1. full nutrition handmade soap of Seed of Chinese Soapberry is characterized in that the mass fraction of its component and each component is:
1.75 parts of Seed of Chinese Soapberry pancebrins, 1.5 parts, sweet oil, 2.5 parts of plam oils, 1 part of Oleum Cocois, 0.75 part, sodium hydroxide;
The preparation method of Seed of Chinese Soapberry pancebrin is as follows:
Get the Seed of Chinese Soapberry shell, 80 ℃ of oven dry add Seed of Chinese Soapberry shell quality 3-4 water doubly, are under 500～600mmHg condition at pressure, ebuillition of heated, extracted 1.5 hours, and filtered reserved filtrate, filter residue adds Seed of Chinese Soapberry shell quality 3-4 water doubly to extract with under condition again, repeat 3 times, then merging filtrate is concentrated into filtrate 3 times and adds 1/2nd of water total mass, namely obtains the Seed of Chinese Soapberry pancebrin.
2. the full nutrition handmade soap of a kind of Seed of Chinese Soapberry claimed in claim 1, is characterized in that, also contains Seed of Chinese Soapberry shell powder 0.1-0.2 part or Seed of Chinese Soapberry medicinal extract 0.1-0.3 part in this handmade soap;
The Seed of Chinese Soapberry shell is pulverized 400 mesh sieves namely got Seed of Chinese Soapberry shell powder;
The preparation method of Seed of Chinese Soapberry medicinal extract is as follows:
Get the Seed of Chinese Soapberry shell, 80 ℃ of oven dry are crushed to 100 orders, add the soaked in absolute ethyl alcohol of 10 times of Seed of Chinese Soapberry shell quality to extract 24h, suction filtration, and reserved filtrate, ethanol is removed in underpressure distillation, namely gets Seed of Chinese Soapberry medicinal extract.
3. the preparation method of the full nutrition handmade soap of the described a kind of Seed of Chinese Soapberry of claim 1 or 2 is characterized in that realizing as follows successively:
(1) by described mass fraction, the Seed of Chinese Soapberry pancebrin is slowly poured in sodium hydroxide, the limit bevelling stirs, until sodium hydroxide dissolves fully, gets Seed of Chinese Soapberry pancebrin alkali lye, is cooled to 40-50 ℃ of insulation;
(2) by described mass fraction, with sweet oil, plam oil, Oleum Cocois Hybrid Heating, after liquefy, stopped heating gets mixing oil, is cooled to 40-50 ℃ of insulation;
(3) Seed of Chinese Soapberry pancebrin alkali lye is slowly poured in mixing oil, the limit bevelling stirs, until reaction mass thickens;
(4) reaction mass is poured in mould, with plastics film, mould is built, in 30-40 ℃ of insulation 24 hours, get the full nutrition handmade soap of Seed of Chinese Soapberry;
(5) demoulding and the full nutrition handmade soap of gained Seed of Chinese Soapberry is put in shady and cool place's saponification 4-12 week, packing gets product;
After step (3) reaction mass thickens, can add Seed of Chinese Soapberry shell powder or Seed of Chinese Soapberry medicinal extract by described mass fraction, and mix.
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| CN2013100987502A CN103122287A (en) | 2013-03-26 | 2013-03-26 | Soapberry total-nutrient handmade soap and preparation method thereof |
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Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104327744A (en) * | 2014-09-23 | 2015-02-04 | 北京泰克美高新技术有限公司 | Application of Chinese soapberry extract and Chinese soapberry composition in automobile washing and washing |
| US9217127B2 (en) | 2013-08-05 | 2015-12-22 | Greenology Products, Inc. | Organic cleaning composition |
| US9217125B2 (en) | 2013-08-05 | 2015-12-22 | Greenology Products, Inc. | Organic cleaning composition |
| CN105543017A (en) * | 2016-03-07 | 2016-05-04 | 黄圭鹏 | Sisal hemp soap |
| CN105567473A (en) * | 2016-01-07 | 2016-05-11 | 福建农林大学 | Soap containing bamboo fungus extract and preparation method thereof |
| CN105754759A (en) * | 2014-12-19 | 2016-07-13 | 朱甜密 | Cleaning and skin caring handmade soap |
| CN105861201A (en) * | 2016-04-19 | 2016-08-17 | 和和实业股份有限公司 | Method for preparing cleaning supply by taking Chinese soapberry fruit pulp as partial raw material |
| US9447366B2 (en) | 2013-08-05 | 2016-09-20 | Greenology Products, Inc. | Organic cleaning composition |
| CN106214814A (en) * | 2016-07-28 | 2016-12-14 | 南京正宽医药科技有限公司 | The extracting method of a kind of Fructus Sapindi Mukouossi extracting solution and liquid soap |
| CN106753912A (en) * | 2016-11-22 | 2017-05-31 | 陕西中医药大学 | A kind of shinyleaf yellowhorn oil handmade soap and preparation method thereof |
| CN107090376A (en) * | 2017-05-09 | 2017-08-25 | 贵州务川国韵生物科技有限公司 | Wormwood soap |
| CN107557196A (en) * | 2017-08-25 | 2018-01-09 | 张悦健 | Liquid soap and preparation method thereof |
| CN108774613A (en) * | 2018-04-03 | 2018-11-09 | 浙江海洋大学 | A kind of soapberry pericarp handmade soap and preparation method thereof |
| CN109609299A (en) * | 2019-01-23 | 2019-04-12 | 杭州善舒生物科技有限公司 | A kind of nanometer of soapberry soap and preparation method thereof |
| CN111378539A (en) * | 2018-12-28 | 2020-07-07 | 黑龙江惠美佳制药有限公司 | Handmade soap containing cannabis polyphenol extract |
| CN111607468A (en) * | 2020-06-08 | 2020-09-01 | 武汉马应龙大健康有限公司 | Soapberry handmade soap and preparation method thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
| CN113813213A (en) * | 2021-11-08 | 2021-12-21 | 青岛科技大学 | Antibacterial and body taste-removing radix curcumae and soapberry composition and preparation method thereof |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US9447366B2 (en) | 2013-08-05 | 2016-09-20 | Greenology Products, Inc. | Organic cleaning composition |
| US9217127B2 (en) | 2013-08-05 | 2015-12-22 | Greenology Products, Inc. | Organic cleaning composition |
| US9217125B2 (en) | 2013-08-05 | 2015-12-22 | Greenology Products, Inc. | Organic cleaning composition |
| CN104327744A (en) * | 2014-09-23 | 2015-02-04 | 北京泰克美高新技术有限公司 | Application of Chinese soapberry extract and Chinese soapberry composition in automobile washing and washing |
| CN105754759A (en) * | 2014-12-19 | 2016-07-13 | 朱甜密 | Cleaning and skin caring handmade soap |
| CN105567473A (en) * | 2016-01-07 | 2016-05-11 | 福建农林大学 | Soap containing bamboo fungus extract and preparation method thereof |
| CN105543017A (en) * | 2016-03-07 | 2016-05-04 | 黄圭鹏 | Sisal hemp soap |
| CN105861201B (en) * | 2016-04-19 | 2018-04-27 | 和和实业股份有限公司 | It is the method that part material prepares cleaning supplies with soapberry pulp |
| CN105861201A (en) * | 2016-04-19 | 2016-08-17 | 和和实业股份有限公司 | Method for preparing cleaning supply by taking Chinese soapberry fruit pulp as partial raw material |
| CN106214814A (en) * | 2016-07-28 | 2016-12-14 | 南京正宽医药科技有限公司 | The extracting method of a kind of Fructus Sapindi Mukouossi extracting solution and liquid soap |
| CN106753912A (en) * | 2016-11-22 | 2017-05-31 | 陕西中医药大学 | A kind of shinyleaf yellowhorn oil handmade soap and preparation method thereof |
| CN107090376A (en) * | 2017-05-09 | 2017-08-25 | 贵州务川国韵生物科技有限公司 | Wormwood soap |
| CN107557196A (en) * | 2017-08-25 | 2018-01-09 | 张悦健 | Liquid soap and preparation method thereof |
| CN108774613A (en) * | 2018-04-03 | 2018-11-09 | 浙江海洋大学 | A kind of soapberry pericarp handmade soap and preparation method thereof |
| CN111378539A (en) * | 2018-12-28 | 2020-07-07 | 黑龙江惠美佳制药有限公司 | Handmade soap containing cannabis polyphenol extract |
| CN109609299A (en) * | 2019-01-23 | 2019-04-12 | 杭州善舒生物科技有限公司 | A kind of nanometer of soapberry soap and preparation method thereof |
| CN111607468A (en) * | 2020-06-08 | 2020-09-01 | 武汉马应龙大健康有限公司 | Soapberry handmade soap and preparation method thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
| CN113813213A (en) * | 2021-11-08 | 2021-12-21 | 青岛科技大学 | Antibacterial and body taste-removing radix curcumae and soapberry composition and preparation method thereof |
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Application publication date: 20130529 |