CN106753912A - A kind of shinyleaf yellowhorn oil handmade soap and preparation method thereof - Google Patents
A kind of shinyleaf yellowhorn oil handmade soap and preparation method thereof Download PDFInfo
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- CN106753912A CN106753912A CN201611032069.8A CN201611032069A CN106753912A CN 106753912 A CN106753912 A CN 106753912A CN 201611032069 A CN201611032069 A CN 201611032069A CN 106753912 A CN106753912 A CN 106753912A
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- oil
- shiny
- yellowhorn
- shinyleaf yellowhorn
- handmade soap
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The present invention relates to a kind of shinyleaf yellowhorn oil handmade soap and preparation method thereof, shinyleaf yellowhorn oil handmade soap clicks raw material and is made：13 parts of 50 80 parts of shiny-leaved yellowhorn seed kernel oil, 20 50 parts of conventional substrate oil, 10 15 parts of shinyleaf yellowhorn shell, 26 parts of highly basic and additive.Preparation method：The mixing match of matrix oil is carried out first, the shinyleaf yellowhorn shell Aqueous extracts and grease that then will be mixed with highly basic react to form saponification thing, then pour into sizing in mould, taking out the handmade soap cutting of sizing, ageing is 7 to pH, and digestion time is no less than 3 months, obtains final product handmade soap.Obtained handmade soap has the functional effects such as anti-oxidant, antiallergy, moisturizing significantly, and the distinguishing feature that pure natural, safety has no side effect, and has a extensive future.
Description
Technical field
The invention belongs to cosmetics and cleaning supplies field, and in particular to a kind of shinyleaf yellowhorn oil handmade soap and its preparation side
Method.
Background technology
As one of woody oil tree species that poverty alleviation industrialization is widelyd popularize national precisely, shiny-leaved yellowhorn (Xanthoceras
Sorbifolia Bunge) there are many unique advantages, shiny-leaved yellowhorn belongs to for Sapindaceae (Sapience) shiny-leaved yellowhorn belongs to, single
Category single, is the distinctive rare traditional oil tree of China, there is the title of northern oil tea.The seeds have cold-resistant, drought-enduring, resistance to soil
The features such as earth is barren, therefore it is especially suitable for the most parts of the north especially place such as northern Shensi, Gansu, Ningxia, northeast and Inner Mongol
Growth.At present, there have been the cultivation of large-scale shiny-leaved yellowhorn and plantation in these areas, add national forestry portion in the end of the year in 2015 and
At 2016 beginning of the years, hold the accurate poverty alleviation boosting of shiny-leaved yellowhorn industry development in Xianyang, Shanxi province city and Beijing Great Hall of the People respectively big
Meeting, to conducting vigorous propaganda and popularization for the seeds, it is anticipated that the planted area of the seeds and distributed areas meeting in the near future
Greatly increase.
Shiny-leaved yellowhorn whole body all has many effect and function --- and shinyleaf yellowhorn shell extract is rich in saponin(e, and text therein
Hat shell glycosides has the effect of the senile dementia that improves significantly；Various active composition is rich in shiny-leaved yellowhorn flower and shiny-leaved yellowhorn leaf.But
It is that it is worth noting that, its tangible China of the industry was had been developed as long as decades, and country and governments at all levels are big in recent years
Push extensively with support, but never big improvement.Current situation is that shiny-leaved yellowhorn cultivated areas constantly expand, are engaged in shiny-leaved yellowhorn
The enterprise and peasant household of plantation are continuously increased, but in the market is rarely seen for the Related product of shiny-leaved yellowhorn.The reason for causing such situation is a lot,
Crucial the reason for is that the research and development of downstream product are delayed, causes substantial amounts of raw material such as seed, flower, leaf etc. to overstock and wave
Take, and the rarely seen Related product of in the market, it might even be possible to regular channel is said almost without Related product, and extremely indivedual enterprises also have text
Hat fruit leaf is processed into the sale of shiny-leaved yellowhorn Fu tea, but because price is higher, inadequate communication, causes consumer awareness not enough to wait former
Thus make a profit little.
Shiny-leaved yellowhorn seed kernel oil is rich in unrighted acid really, and can promote have brain containing rare in a vegetable oil
Nervous system is repaired, the material of regeneration function --- nervonic acid, is quality xylophyta oil higher.But currently as edible
It is ripe later pained pungent shiny-leaved yellowhorn benevolence the reason for profit that oil is sold difficult, and oil expression is edible also the sensation for making us not pleasing,
Cooking edible oil exploitation must break through these technological difficulties；In addition, compared with other commercially available edible oils, the oily cooking food compares
But greasy fragrant degree is inadequate.Therefore, although shiny-leaved yellowhorn has the advantages that many, various channel prices also all really as edible oil
It is very high, but peddle and do not draw well, and difficulty obtains consumer's accreditation, almost no sales volume.Want to make good use of the resource, create economic valency
Value, must just find a new way.
The content of the invention
In order to solve problem above, show it is an object of the present invention to provide functional effects such as a kind of anti-oxidant, antiallergy, moisturizings
Write, and pure natural, the safe shinyleaf yellowhorn oil handmade soap having no side effect and preparation method thereof.
The purpose of the present invention is achieved through the following technical solutions：
Shinyleaf yellowhorn oil handmade soap, it is characterised in that be made up of the following raw material of quality proportioning：Shiny-leaved yellowhorn seed kernel oil 50-80
Part, 20-50 parts of conventional substrate oil, shinyleaf yellowhorn shell 10-15 parts, highly basic 2-6 parts and additive 1-3 parts.
Preferably, the conventional substrate oil is the one of which or several such as coconut oil, olive oil, corn oil.
Preferably, the highly basic is one or more in NaOH or potassium hydroxide.
Preferably, additive is Chinese medical extract, activated carbon, shiny-leaved yellowhorn alcohol extracts from the leaves, shiny-leaved yellowhorn leaf polyose, shinyleaf yellowhorn shell
The one of which or several such as extract, shiny-leaved yellowhorn flower, shiny-leaved yellowhorn protein powder, acetum pyrolignosum rectificatum liquid, plant pollen, plants essential oil
Kind.
It is further preferred that shiny-leaved yellowhorn alcohol extracts from the leaves is made according to the following steps：The shiny-leaved yellowhorn leaf that October is plucked is dried
Crush, add 10 times of 95% ethanol of amount, heating and refluxing extraction three times, concentration and recovery solvent, medicinal extract frozen drying, powder
It is broken, obtain final product.
It is further preferred that shiny-leaved yellowhorn leaf polyose is made according to the following steps：The shiny-leaved yellowhorn leaf xeraphium that October is plucked
It is broken, 10 times of water of amount are added, extracting in boiling water three times is concentrated into paste, adds absolute ethyl alcohol to polysaccharide no longer to separate out, cooling and standings
Overnight, suction filtration, will crush after solid polysaccharide freeze-drying, obtain final product.
It is further preferred that shinyleaf yellowhorn shell extract is made according to the following steps：Dry shinyleaf yellowhorn shell is crushed, 10 are added
70% ethanol of amount, heating and refluxing extraction three times, concentration and recovery solvent, crush after medicinal extract frozen drying again, obtain final product.
It is further preferred that shiny-leaved yellowhorn protein powder is made according to the following steps：The shiny-leaved yellowhorn benevolence egg of oil will be extracted
White enzymolysis, concentration is crushed after freeze-drying, is obtained final product.
It is further preferred that shiny-leaved yellowhorn flower after the shiny-leaved yellowhorn flower freeze-drying of May full-bloom stage obtained by crushing.
Meanwhile, the preparation method of above-mentioned shinyleaf yellowhorn oil handmade soap is disclosed, comprise the following steps：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with conventional substrate oil, heats compound lard；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shiny-leaved yellowhorn
Shell concentrate, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, slow after being completely dissolved
Be heated to miscella identical temperature in step (1), obtain alkali lye；
(3) in additive and step (2) gained alkali lye being added into the compound lard of step (1), and insulated and stirred 5h obtains soap
Change reactant；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storage
It is 7 to hide room and be fully aged to pH value, and digestion time is no less than 3 months, obtains final product handmade soap.
Preferably, heating-up temperature is 40-45 DEG C in above-mentioned steps (1).
Beneficial effects of the present invention：
At present numerous enterprises for being engaged in the industry and individual all publicize the seeds be all from head to foot precious, with exploitation very high
Value, the slogan of publicity is all that " shinyleaf yellowhorn oil is the high edible oil of nutritive value, shiny-leaved yellowhorn leaf can be with tea making, shinyleaf yellowhorn shell
Activated carbon and furfural can be prepared ", and finally almost but all only moved towards same approach --- squeeze seed kernel oil and work as edible oil
Sell, finally have been found that difficulty obtains income.The present invention first using shinyleaf yellowhorn oil as soapmaking raw material, obtained handmade soap its antioxygen
The functional effects such as change, antiallergy, moisturizing are significantly better than commercially available traditional-handwork soap.
(2) the present invention uses shinyleaf yellowhorn shell water cooking liquid to concentrate as saponification liquor, makes obtained handmade soap artificial without adding again
Foaming ingredient just can be good foaming effect, while seminar's research is it has also been found that shinyleaf yellowhorn shell aqueous extract also has whitening, anti-
Solarization, antipruritic, antiallergy, anti-oxidant, health care are waited for a long time function and effect.
(3) shinyleaf yellowhorn oil handmade soap foaming of the invention is abundant, does not hurt hands, non-stimulated, is the exploitation of shiny-leaved yellowhorn Resource industrialization
There is provided new direction and thinking, also for the exploitation of daily chemical product that is safer, having no side effect provides new raw material sources.
(4) the present invention is found by lot of experiments and filters out shinyleaf yellowhorn shell extract, shiny-leaved yellowhorn flower, shiny-leaved yellowhorn alcohol extracts from the leaves
And shiny-leaved yellowhorn leaf polyose isoreactivity position, and continuously attempt to screen the suitable proportioning of these compositions and preparation method, it is obtained by hand
Soap has degerming quick, and cleaning capacity is strong, does not hurt hands, non-stimulated to wait remarkable result.
Part screening test result
1st, shiny-leaved yellowhorn alcohol extracts from the leaves antioxidation activity position the selection result：
Experimental result shows, active site water extract part (A), 30% ethanol extract part from shiny-leaved yellowhorn leaf
(B), 50% ethanol extract part (C), 70% ethanol extract part (D), 95% ethanol extract part (E), to DPPH freedom
Base has certain scavenging capacity, wherein 95% ethanol extract part (E) free radical scavenging is most strong, is in concentration
To DPPH free radical scavenging activities up to 85.78% during 0.2mg/ml.
2nd, shiny-leaved yellowhorn leaf polyose has stronger scavenging capacity the selection result to DPPH free radicals：
Experimental result shows that shiny-leaved yellowhorn leaf polyose has stronger scavenging capacity to DPPH free radicals, and is closed with dose-effect
System, when concentration is 0.2mg/ml to DPPH free radical scavenging activities just up to 90.78%.
3rd, shinyleaf yellowhorn shell antioxidation activity position the selection result：
Experimental result shows that six different extract parts of shinyleaf yellowhorn shell have certain antioxidation activity, wherein position D
The antioxidation activity of (extraction of 70% ethanol) is most strong, and Scavenging activity and sample concentration are in dose-effect relationship, when concentration is 0.2mg/
During ml, its clearance rate can reach 70.82%.
Brief description of the drawings
Fig. 1 shinyleaf yellowhorn oil handmade soap samples
Fig. 2 shiny-leaved yellowhorn alcohol extracts from the leaves antioxidation activities position the selection result
Fig. 3 shiny-leaved yellowhorns leaf polyose has stronger scavenging capacity the selection result to DPPH free radicals
Fig. 4 shinyleaf yellowhorn shell antioxidation activities position the selection result
Specific embodiment
The present invention is described in further details below by example, these examples are only used for illustrating the present invention, do not limit
The scope of the present invention processed.
The shinyleaf yellowhorn oil handmade soap of embodiment 1
Raw material：
Matched by following mass fractions：80 parts of shiny-leaved yellowhorn seed kernel oil, 20 parts of olive oil, 10 parts of shinyleaf yellowhorn shell, NaOH 2
Part, 1 part of shiny-leaved yellowhorn alcohol extracts from the leaves, 2 parts of shinyleaf yellowhorn shell extract.
Shiny-leaved yellowhorn alcohol extracts from the leaves is obtained according to the following steps：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, adds 10 times
95% ethanol of amount, heating and refluxing extraction three times, concentration and recovery solvent, medicinal extract frozen drying, crushing are obtained final product.
Shinyleaf yellowhorn shell extract is obtained according to the following steps：Dry shinyleaf yellowhorn shell is crushed, 10 times of 70% second of amount are added
Alcohol, heating and refluxing extraction three times, concentration and recovery solvent is crushed after medicinal extract frozen drying, is obtained final product.
Preparation method：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with olive oil, heats compound lard；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shiny-leaved yellowhorn
Shell concentrate, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, slow after being completely dissolved
Be heated to miscella identical temperature in step (1), obtain alkali lye；
(3) shiny-leaved yellowhorn leaf extract and shinyleaf yellowhorn shell extract and step (2) gained alkali lye are added the mixing of step (1)
In grease, and insulated and stirred 5h, obtain saponification thing；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storage
It is 7 to hide room and be fully aged to pH value, and digestion time is no less than 3 months, obtains final product handmade soap.
The shinyleaf yellowhorn oil handmade soap of embodiment 2
Raw material：
Matched by following mass fractions：50 parts of shiny-leaved yellowhorn seed kernel oil, 50 parts of coconut oil, 15 parts of shinyleaf yellowhorn shell, potassium hydroxide 6
Part, 2 parts of shiny-leaved yellowhorn protein powder, shiny-leaved yellowhorn spends 1 part.
Shiny-leaved yellowhorn protein powder is obtained according to the following steps：The shiny-leaved yellowhorn protein enzymolysis of oil will be extracted, concentration is cold
Freeze crushed after being dried, obtain final product.
Shiny-leaved yellowhorn flower after the shiny-leaved yellowhorn flower freeze-drying of May full-bloom stage obtained by crushing.
Preparation method：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with coconut oil, heats compound lard, temperature control is at 40-45 DEG C；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shiny-leaved yellowhorn
Shell concentrate, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, slow after being completely dissolved
Be heated to miscella identical temperature in step (1), obtain alkali lye；
(3) shiny-leaved yellowhorn protein powder and shiny-leaved yellowhorn flower and step (2) gained alkali lye are added the compound lard of step (1)
In, and insulated and stirred 5h, obtain saponification thing；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storage
It is 7 to hide room and be fully aged to pH value, and digestion time is no less than 3 months, obtains final product handmade soap.
The shinyleaf yellowhorn oil handmade soap of embodiment 3
Raw material：
Matched by following mass fractions：70 parts of shiny-leaved yellowhorn seed kernel oil, 30 parts of corn oil, 13 parts of shinyleaf yellowhorn shell, NaOH 4
Part, 2 parts of shiny-leaved yellowhorn leaf polyose, shiny-leaved yellowhorn spends 1 part.
Shiny-leaved yellowhorn leaf polyose following steps are obtained：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, 10 times of amounts of addition
Water, extracting in boiling water three times is concentrated into paste, adds absolute ethyl alcohol to polysaccharide no longer to separate out, and overnight, suction filtration will be solid for cooling and standings
Crushed after body polysaccharide freeze-drying, obtained final product.
Shiny-leaved yellowhorn flower after the shiny-leaved yellowhorn flower freeze-drying of May full-bloom stage obtained by crushing.
Preparation method：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with corn oil, heats compound lard, temperature control is at 40-45 DEG C；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shiny-leaved yellowhorn
Shell concentrate, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, slow after being completely dissolved
Be heated to miscella identical temperature in step (1), obtain alkali lye；
(3) in the compound lard by shiny-leaved yellowhorn leaf polyose and shiny-leaved yellowhorn flower with step (2) gained alkali lye addition step (1),
And insulated and stirred 5h, obtain saponification thing；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storage
It is 7 to hide room and be fully aged to pH value, and digestion time is no less than 3 months, obtains final product handmade soap.
The shinyleaf yellowhorn oil handmade soap of embodiment 4
Raw material：
Matched by following mass fractions：60 parts of shiny-leaved yellowhorn seed kernel oil, 15 parts of olive oil, 15 parts of coconut oil, 10 parts of corn oil,
14 parts of shinyleaf yellowhorn shell, 4 parts of NaOH, 1 part of shiny-leaved yellowhorn alcohol extracts from the leaves, 1 part of shiny-leaved yellowhorn leaf polyose, shiny-leaved yellowhorn spends 1 part.
Shiny-leaved yellowhorn alcohol extracts from the leaves is obtained according to the following steps：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, adds 10 times
95% ethanol of amount, heating and refluxing extraction three times, concentration and recovery solvent, medicinal extract frozen drying, crushing are obtained final product.
Shiny-leaved yellowhorn leaf polyose following steps are obtained：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, 10 times of amounts of addition
Water, extracting in boiling water three times is concentrated into paste, adds absolute ethyl alcohol to polysaccharide no longer to separate out, and overnight, suction filtration will be solid for cooling and standings
Crushed after body polysaccharide freeze-drying, obtained final product.
Shiny-leaved yellowhorn flower after the shiny-leaved yellowhorn flower freeze-drying of May full-bloom stage obtained by crushing.
Preparation method：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with olive oil, coconut oil and corn oil, heats compound lard, temperature
Control is at 40-45 DEG C；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shiny-leaved yellowhorn
Shell concentrate, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, slow after being completely dissolved
Be heated to miscella identical temperature in step (1), obtain alkali lye；
(3) shiny-leaved yellowhorn alcohol extracts from the leaves, shiny-leaved yellowhorn leaf polyose and shiny-leaved yellowhorn flower and step (2) gained alkali lye are added into step
(1) in compound lard, and insulated and stirred 5h, obtain saponification thing；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storage
It is 7 to hide room and be fully aged to pH value, and digestion time is no less than 3 months, obtains final product handmade soap.
The handmade soap trial effect of embodiment 5 is investigated
Inventor randomly selects the trier 100 of different age group, different sexes, continuous on probation by the raw material of embodiment 4
And finished product handmade soap 3 months obtained in method, trier is paid a return visit, as a result collect and be shown in Table 1 (before reference is trier
Used handmade soap)：
Using effect feedback result (the unit of table 1：People)
| Highly significant | Significantly | Typically | It is not notable | It is very not notable | |
| Foaming effect | 86 | 12 | 1 | 1 | 0 |
| Cleaning effect | 95 | 4 | 1 | 0 | 0 |
| Antiallergic effect | 90 | 5 | 3 | 2 | 0 |
| Moistening effect | 92 | 7 | 1 | 0 | 0 |
| Excitant | 0 | 0 | 1 | 2 | 97 |
The above, is only presently preferred embodiments of the present invention, and any formal limitation is not made to the present invention, though
So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, not departing from the technology of the present invention side's scope, when making a little change using the technology contents of the disclosure above or be modified to
The Equivalent embodiments of equivalent variations, as long as being the content without departing from technical solution of the present invention, according to technical spirit pair of the invention
Any simple modification, equivalent variations and modification that above example is made, still fall within the range of technical solution of the present invention.
Claims (11)
1. a kind of shinyleaf yellowhorn oil handmade soap, it is characterised in that be made up of the following raw material of quality proportioning：Shiny-leaved yellowhorn seed kernel oil 50-80
Part, 20-50 parts of conventional substrate oil, shinyleaf yellowhorn shell 10-15 parts, highly basic 2-6 parts and additive 1-3 parts.
2. shinyleaf yellowhorn oil handmade soap according to claim 1, it is characterised in that the conventional substrate oil is coconut oil, olive
The one of which or several such as olive oil, corn oil.
3. shinyleaf yellowhorn oil handmade soap according to claim 2, it is characterised in that the highly basic is NaOH or hydroxide
One or more in potassium.
4. shinyleaf yellowhorn oil handmade soap according to claim 3, it is characterised in that additive be Chinese medical extract, activated carbon,
Shiny-leaved yellowhorn alcohol extracts from the leaves, shiny-leaved yellowhorn leaf polyose, shinyleaf yellowhorn shell extract, shiny-leaved yellowhorn flower, shiny-leaved yellowhorn protein powder, acetum pyrolignosum rectificatum
The one of which such as liquid, plant pollen, plants essential oil are several.
5. shinyleaf yellowhorn oil handmade soap according to claim 4, it is characterised in that shiny-leaved yellowhorn alcohol extracts from the leaves is made according to the following steps
Into：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, adds 10 times of 95% ethanol of amount, heating and refluxing extraction three times, concentration
Recycling design, medicinal extract frozen drying, crushing, obtains final product.
6. shinyleaf yellowhorn oil handmade soap according to claim 4, it is characterised in that shiny-leaved yellowhorn leaf polyose is made according to the following steps
Into：The shiny-leaved yellowhorn leaf drying and crushing that October is plucked, adds 10 times of water of amount, and extracting in boiling water three times is concentrated into paste, adds
Absolute ethyl alcohol to polysaccharide is no longer separated out, and overnight, suction filtration will be crushed after solid polysaccharide freeze-drying, be obtained final product for cooling and standings.
7. shinyleaf yellowhorn oil handmade soap according to claim 4, it is characterised in that shinyleaf yellowhorn shell extract is made according to the following steps
Into：Dry shinyleaf yellowhorn shell is crushed, 10 times of 70% ethanol of amount, heating and refluxing extraction three times, concentration and recovery solvent, leaching is added
Crushed after cream frozen drying, obtained final product.
8. shinyleaf yellowhorn oil handmade soap according to claim 4, it is characterised in that shiny-leaved yellowhorn protein powder is according to the following steps
It is made：The shiny-leaved yellowhorn protein enzymolysis of oil will be extracted, concentration is crushed after freeze-drying, obtained final product.
9. shinyleaf yellowhorn oil handmade soap according to claim 4, it is characterised in that shiny-leaved yellowhorn flower is the text of May full-bloom stage
Gained is crushed after hat fruit flower freeze-drying.
10. the preparation method of any shinyleaf yellowhorn oil handmade soaps of 1-9 is required according to power, it is characterised in that comprised the following steps：
(1) shiny-leaved yellowhorn seed kernel oil is mixed in proportion with conventional substrate oil, heats compound lard；
(2) shinyleaf yellowhorn shell crushing will be dried, 10 times of water of amount will be added, is boiled and is concentrated into 1/5th volumes, obtain shinyleaf yellowhorn shell dense
Contracting liquid, after after the cooling of shinyleaf yellowhorn shell concentrate, stirs being added by the highly basic of accurate amount of calculation, is slowly heated after being completely dissolved
To with miscella identical temperature in step (1), obtain alkali lye；
(3) in additive and step (2) gained alkali lye being added into the compound lard of step (1), and insulated and stirred 5h obtains saponification anti-
Answer thing；
(4) saponification thing in step (3) is fallen in mould, is cooled down and sufficient standing, coagulation forming；
(5) treat that the product of coagulation forming in step (4) is removed from the molds, be cut to suitable size and shape, be placed in storeroom
Fully ageing to pH value is 7, and digestion time is no less than 3 months, obtains final product handmade soap.
The preparation method of 11. shinyleaf yellowhorn oil handmade soaps according to claim 10, it is characterised in that heating in step (1)
Temperature is 40-45 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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| CN108048265A (en) * | 2017-12-31 | 2018-05-18 | 跨越生物科技（滁州）有限公司 | A kind of preparation method of safe and non-toxic environmental-friendly Antibacterial soaps |
| CN108277110A (en) * | 2018-02-05 | 2018-07-13 | 刘丹赤 | A kind of handmade soap and preparation method |
| CN110747077A (en) * | 2019-11-22 | 2020-02-04 | 付锦洋 | Whitening and skin moistening soap and preparation method thereof |
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