CN108774613A - A kind of soapberry pericarp handmade soap and preparation method thereof - Google Patents
A kind of soapberry pericarp handmade soap and preparation method thereof Download PDFInfo
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- CN108774613A CN108774613A CN201810288390.5A CN201810288390A CN108774613A CN 108774613 A CN108774613 A CN 108774613A CN 201810288390 A CN201810288390 A CN 201810288390A CN 108774613 A CN108774613 A CN 108774613A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Detergent Compositions (AREA)
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Abstract
The invention belongs to daily washing product technical field, be related to a kind of soapberry pericarp handmade soap and preparation method thereof, it is weaker which solve the handmade soap bacteria resistance function on existing market the problems such as.This handmade soap includes according to mass fraction meter:24 parts of natural soap bases, 70 portions of soapberry pericarp saponin(e concentrates, 6 parts of flavones liquid and 0.4 part of essential oil, preparation method includes the following steps:1) acquisition soapberry fruit prepares soapberry pericarp saponin(e concentrate;2) acquisition Suaeda salsa extracts flavones liquid;3) it takes in the natural soap base merging beakers of 24g, water-bath makes its thawing, and soapberry pericarp saponin(e concentrate made from 70g steps 1) is added in beaker;4) it weighs flavones liquid made from 6g steps 2) and pours into and obtain mixed liquor in beaker;5) beaker is taken out from water-bath, is stirred liquid;6) essential oil is instilled in beaker, is stirred liquid;7) mixed liquor is poured into mold cooled and solidified to get soapberry pericarp handmade soap finished product.
Description
Technical field
The invention belongs to daily washing product technical field, it is related to a kind of soapberry pericarp handmade soap and preparation method thereof.
Background technology
Current market sales of perfumed soap, most of synthesized by production of machinery, due to containing using chemical substance
Substance is learned, the natural grease on human skin can be not only washed away after use, it is also possible to can be damaged to skin.
Natural plant Chinese soapberry is known as soap tree, is rich in saponin(e in pericarp, can soapberry be directly wrapped in cotton and knit sack
Interior soaked rub with the hands is squeezed, and so that it is generated foam, is directly used in laundry, hair washing, ablution.
The sub- seedling of Suaeda salsa can cook, extracting solution include there are many minerals, dietary fiber, flavones etc. effectively at
Part, the diseases such as the carcinoma of the rectum, diabetes, hemorrhoid can be prevented.Wherein abundant flavone content, to Escherichia coli, staphylococcus aureus,
Candida albicans bacterium etc. has very strong fungistatic effect as people's health requirement is higher and higher, also occurs some now
More popular handmade soap has better moisture-keeping functions, such as since the grease after saponification in handmade soap is not pulled out
The Chinese invention patent of Patent No. CN201210228754.3《A kind of Gingko handmade soap》, the handmade soap contains:According to weight
Measure the Transparent soap base of percentages 70~99.5%, 0.05~20% ginkgo biloba extract;And 0.05~3% plants essential oil
Or essence.It adds ginkgo biloba extract in handmade soap so that handmade soap has the function of whitening, crease-resistant.In addition, also having
Sweet osmanthus handmade soap, cucumber handmade soap etc..But organic natural soap base addition saline land alkali is fabricated to the extracted object of soapberry pericarp
Fluffy sub- extracting solution has not been reported as the current country of handmade soap prepared by raw material.
Invention content
First purpose of the present invention is the presence of the above problem in view of the prior art, it is proposed that a kind of soapberry pericarp hand
Work soap, the technical problem to be solved by the present invention is to:A kind of soapberry pericarp handmade soap is provided, natural environmental-protective, low is made it have
Foam and bacteria resistance function.
Second object of the present invention is the presence of the above problem in view of the prior art, it is proposed that a kind of soapberry pericarp hand
The preparation method of work soap, the technical problem to be solved by the present invention is to:A kind of preparation method of soapberry pericarp handmade soap is provided,
Make it have natural environmental-protective, low foam and bacteria resistance function.
First purpose of the present invention can be realized by following technical proposal:
A kind of soapberry pericarp handmade soap, it is characterised in that the handmade soap includes according to mass fraction meter:24 parts natural
Soap base, 70 parts of soapberry pericarp saponin(e concentrate, 6 parts of flavones liquid and 0.4 part of essential oil.
In above-mentioned soapberry pericarp handmade soap, the soapberry pericarp saponin(e concentrate is with ripe soapberry fruit
Raw material is implemented as to be made after crushing concentration extraction.
In above-mentioned soapberry pericarp handmade soap, the flavones liquid is extracted using Suaeda salsa blades as raw material
It arrives.
In above-mentioned soapberry pericarp handmade soap, the essential oil is plant Peppermint essential oil.
Second object of the present invention can be realized by following technical proposal:
A kind of preparation method of soapberry pericarp handmade soap, it is characterised in that include the following steps:
1) the ripe soapberry fruit of acquisition obtains soapberry pericarp saponin(e concentrate after crushing concentration extraction;
2) it acquires fresh Suaeda salsa and extracts flavones liquid;
3) in the beaker for taking the natural soap base mergings of 24g clean, water-bath makes its thawing, and 70g steps 1) system is added in beaker
Soapberry pericarp saponin(e concentrate to get to soapberry pericarp soap base liquid;
4) it weighs flavones liquid made from 6g steps 2) and pours into and obtain mixed liquor in beaker;
5) beaker is taken out from water-bath, is stirred liquid until flavones liquid is completely mixed with soapberry pericarp soap base liquid
It closes;
6) by essential oil it is evenly dispersed instill in beaker, be stirred liquid until be thoroughly mixed;
7) mixed liquor in beaker is poured into mold, is put at shady and cool ventilation cooled and solidified to get soapberry pericarp hand
Work soap finished product.
In a kind of preparation method of above-mentioned soapberry pericarp handmade soap, soapberry pericarp soap is prepared in the step 1)
The detailed process of glycosides concentrate is:
A, after taking soapberry ripening fruits is clean to dry, seed in fruit is removed, by remaining pericarp, puts 120 DEG C
Drying box 2h after, temperature is adjusted to 80 DEG C and dries pericarps to being completely dried, is crushed up to spaonin powder with 200 mesh micronizers
End;
B, 100g soapberry powder is weighed, is put into enamelled cup, 500mL distilled water is added, with 100 DEG C of water-baths in water-bath
Heating decocts 3h;
C, 6 layers of filtered through gauze after cooling, obtain filtrate one and filter residue, and filter residue remains in enamelled cup, and 500mL distillations are added
Water decocts 2h;
D, it is filtered again after cooling, obtains filtrate two and filter residue, 500mL distilled water immersions 8h is added into filter residue;
E, the soapberry extract filtering for impregnating 8h is taken, filtrate three is obtained, twice with distilled water flushing filter residue, obtains filtrate four;
F, it is concentrated by evaporation:Merging filtrate one, filtrate two, filtrate three and filtrate four are concentrated by evaporation 5h for 100 DEG C with water-bath,
Obtain water extracting liquid;
G, it extracts repeatedly:Water extracting liquid is poured into separatory funnel, adds 250mL extracting n-butyl alcohols, separation upper liquid that must extract
Liquid one is taken, liquid is retained, 200mL extracting n-butyl alcohols are added in downward liquid, and it is extract liquor two to obtain upper liquid, and 200mL is added in liquid still further below
Extracting n-butyl alcohol obtains extract liquor three;
H, rotary evaporation:Combining extraction liquid one, extract liquor two and extract liquor three, with 63 revs/min, 75 DEG C of Rotary Evaporators
Rotary evaporation, recycles n-butanol, and collection obtains soapberry pericarp saponin(e concentrate.
In a kind of preparation method of above-mentioned soapberry pericarp handmade soap, extraction flavones liquid is specific in the step 2)
Process is:
A, fresh Suaeda salsa is collected;
B, the green leaves of Suaeda salsa are all removed, and is put into clean beaker and collects;
C, leaf is eluted with water, is put into alcohol and sterilizes 6 minutes, is then immersed in water, washes away alcohol;
D, Suaeda salsa blades 1g is weighed, is placed in Soxhlet extractor, 70% ethyl alcohol 100mL and a little CaCO is added3,
6-8h is extracted, extracting solution reduced pressure is poured out and boils off ethyl alcohol and obtain concentrate;
E, concentrate is washed 2-3 times in separatory funnel with the ether of same volume, obtains flavones liquid.
In a kind of preparation method of above-mentioned soapberry pericarp handmade soap, the bath temperature of the step 3) is 100 DEG C.
In a kind of preparation method of above-mentioned soapberry pericarp handmade soap, the mixing time of the step 5) is 1 minute.
In a kind of preparation method of above-mentioned soapberry pericarp handmade soap, the addition essential oil of the step 6) is 0.4 gram,
The mixing time of the step 6) is 2 minutes.
Compared with prior art, the present invention has the following advantages:
In natural plant Chinese soapberry pericarp be rich in saponin(e, can directly by soapberry be wrapped in cotton knit in sack it is soaked rub with the hands squeeze,
It is directly used in laundry, hair washing, ablution.Abundant flavone content in the sub- extracting solution of Suaeda salsa, to Escherichia coli, Staphylococcus aureus
Bacterium, candida albicans bacterium etc. have very strong fungistatic effect.Soapberry pericarp is fabricated to organic natural soap base by water extraction,
To add the natural organic component of the sub- flavone extractive of Suaeda salsa, soapberry pericarp handmade soap finished product is made.With natural environmental-protective,
The comprehensive functions such as low foam, sterilizing ability be strong.It can effectively realize resource consolidation and cycling and reutilization.
Specific implementation mode
The following is specific embodiments of the present invention, and technical scheme of the present invention will be further described, but the present invention is simultaneously
It is not limited to these embodiments.
This soapberry pericarp handmade soap includes according to mass fraction meter:24 parts of natural soap base, 70 parts of soapberry pericarp
Saponin(e concentrate, 6 parts of flavones liquid and 0.4 part of essential oil.Wherein, soapberry pericarp saponin(e concentrate is with ripe soapberry
Fruit is obtained as raw material after crushing concentration extraction, and flavones liquid is to extract to obtain as raw material using fresh Suaeda salsa.Essence
Oil is preferably plant Peppermint essential oil.
According to following data it can be found that, 24 parts of natural soap base, 70 parts of soapberry pericarp saponin(e concentrate, 6 parts
When flavones liquid and 0.4 part of essential oil, best results are made a concrete analysis of as follows:
(1) fungistatic effect:Fungistatic effect is detected using filter paper enzyme, with natural soap base, soapberry pericarp saponin(e concentrate
9 groups of contrast experiment's groups are prepared with flavones liquid, every group is separately added into 6g flavones liquid, is configured to soapberry pericarp saponin(e concentrate concentration
Respectively 10%, 20%, 30%, 40%, 50%, 60%, 70%, 80%, 90% handmade soap formula, it is found through experiment that, when
Soapberry pericarp saponin(e concentrate it is a concentration of 90% when to the fungistatic effect of staphylococcus aureus, Escherichia coli and proteus
Reach optimum value, best is reached to the fungistatic effect of Candida albicans when soapberry pericarp saponin(e concentrate concentration reaches 40%
Value.
(2) clean effect:It prepares handmade soap identical with bacteriostatic test and is formulated contrast experiment's group, be found through experiments that, when
Soapberry pericarp saponin(e concentrate concentration cleans dirt completely when reaching 70%, increases soapberry pericarp saponin(e concentrate
After concentration, cleaning capacity is constant.
Consider at above-mentioned 2 points, optimum proportioning be added in the natural soap bases of 24g 70g soapberrys pericarp saponin(e concentrate and
6g flavones liquid.
The preparation method of this soapberry pericarp handmade soap, includes the following steps:
1) acquisition soapberry ripening fruits prepares soapberry pericarp saponin(e concentrate, and the specific steps prepared include:
A, after taking soapberry ripening fruits is clean to dry, seed in fruit is removed, by remaining pericarp, puts 120 DEG C
Drying box 2h after, temperature is adjusted to 80 DEG C and dries pericarps to being completely dried, is crushed up to spaonin powder with 200 mesh micronizers
End;
B, 100g soapberry powder is weighed, is put into enamelled cup, 500mL distilled water is added, with 100 DEG C of water-baths in water-bath
Heating decocts 3h;
C, 6 layers of filtered through gauze after cooling, obtain filtrate one and filter residue, and filter residue remains in enamelled cup, and 500mL distillations are added
Water decocts 2h;
D, it is filtered again after cooling, obtains filtrate two and filter residue, 500mL distilled water immersions 8h is added into filter residue;
E, the soapberry extract filtering for impregnating 8h is taken, filtrate three is obtained, twice with distilled water flushing filter residue, obtains filtrate four;
F, it is concentrated by evaporation:Merging filtrate one, filtrate two, filtrate three and filtrate four are concentrated by evaporation 5h for 100 DEG C with water-bath,
Obtain water extracting liquid;
G, it extracts repeatedly:Water extracting liquid is poured into separatory funnel, adds 250mL extracting n-butyl alcohols, separation upper liquid that must extract
Liquid one is taken, liquid is retained, 200mL extracting n-butyl alcohols are added in downward liquid, and it is extract liquor two to obtain upper liquid, and 200mL is added in liquid still further below
Extracting n-butyl alcohol obtains extract liquor three;
H, rotary evaporation:Combining extraction liquid one, extract liquor two and extract liquor three, with 63 revs/min, 75 DEG C of Rotary Evaporators
Rotary evaporation, recycles n-butanol, and collection obtains soapberry pericarp saponin(e concentrate;
2) it acquires fresh Suaeda salsa and extracts flavones liquid, and the specific steps of its extraction include:
A, the green leaves of Suaeda salsa are all removed, and is put into clean beaker and collects;
B, leaf is eluted with water, is put into alcohol and sterilizes 6 minutes, is then immersed in water, washes away alcohol;
C, Suaeda salsa blades 1g is weighed, is placed in Soxhlet extractor, 70% ethyl alcohol 100mL and a little CaCO3 is added,
6-8h is extracted, extracting solution reduced pressure is poured out and boils off ethyl alcohol and obtain concentrate;
D, concentrate is washed 2-3 times in separatory funnel with the ether of same volume, obtains flavones liquid;
3) in the beaker for taking the natural soap base mergings of 24g clean, beaker is placed in water-bath in 100 DEG C of water-baths, until soap base is complete
It is complete to melt, soapberry pericarp saponin(e concentrate made from 70g steps 1) is added in beaker to get to soapberry pericarp soap base
Liquid;
4) it weighs flavones liquid made from 6g steps 2) and pours into and obtain mixed liquor in beaker;
5) beaker is taken out from water-bath, is stirred liquid until flavones liquid is completely mixed with soapberry pericarp soap base liquid
It closes, mixing time is preferably 1 minute;
6) by 0.4g essential oils it is evenly dispersed instill in beaker, be stirred liquid until be thoroughly mixed, mixing time is excellent
It is selected as 2 minutes;
7) mixed liquor in beaker is poured into mold, is put at shady and cool ventilation cooled and solidified to get soapberry pericarp hand
Work soap finished product.
Using handmade soap obtained above, there are the comprehensive functions such as natural environmental-protective, low foam, sterilizing ability be strong, it can be effective
Realize resource consolidation and cycling and reutilization.
Specific embodiment described herein is only an example for the spirit of the invention.Technology belonging to the present invention is led
The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Claims (10)
1. a kind of soapberry pericarp handmade soap, it is characterised in that the handmade soap includes according to mass fraction meter:24 parts of natural soap
Base, 70 parts of soapberry pericarp saponin(e concentrate, 6 parts of flavones liquid and 0.4 part of essential oil.
2. soapberry pericarp saponin(e concentrate according to claim 1, it is characterised in that:The soapberry pericarp saponin(e is dense
Contracting liquid is to be implemented as raw material with ripe soapberry fruit to be made after crushing concentration extraction.
3. flavones liquid according to claim 1, it is characterised in that:The flavones liquid is using Suaeda salsa blades as original
Material extraction obtains.
4. essential oil according to claim 1, it is characterised in that:The essential oil is plant Peppermint essential oil.
5. a kind of preparation method of soapberry pericarp handmade soap, it is characterised in that include the following steps:
1) the ripe soapberry fruit of acquisition obtains soapberry pericarp saponin(e concentrate after crushing concentration extraction;
2) it acquires fresh Suaeda salsa and extracts flavones liquid;
3) in the beaker for taking the natural soap base mergings of 24g clean, water-bath makes its thawing, and it is obtained that 70g steps 1) are added in beaker
Soapberry pericarp saponin(e concentrate is to get to soapberry pericarp soap base liquid;
4) it weighs flavones liquid made from 6g steps 2) and pours into and obtain mixed liquor in beaker;
5) beaker is taken out from water-bath, is stirred liquid until flavones liquid is thoroughly mixed with soapberry pericarp soap base liquid;
6) by essential oil it is evenly dispersed instill in beaker, be stirred liquid until be thoroughly mixed;
7) mixed liquor in beaker is poured into mold, is put at shady and cool ventilation cooled and solidified to get soapberry pericarp handmade soap
Finished product.
6. preparation method according to claim 5, it is characterised in that:The step 1) prepares the concentration of soapberry pericarp saponin(e
The detailed process of liquid is:
A, after taking soapberry ripening fruits to clean and dry, seed in fruit remove, by remaining pericarp, put 120 DEG C and do
After dry case 2h, temperature is adjusted to 80 DEG C and dries pericarp to being completely dried, is crushed up to soapberry powder with 200 mesh micronizers;
B, 100g soapberry powder is weighed, is put into enamelled cup, 500mL distilled water is added, with 100 DEG C of heating water baths in water-bath
Decoct 3h;
C, 6 layers of filtered through gauze after cooling, obtain filtrate one and filter residue, and filter residue remains in enamelled cup, and 500mL distilled water is added, and decoct
Boil 2h;
D, it is filtered again after cooling, obtains filtrate two and filter residue, 500mL distilled water immersions 8h is added into filter residue;
E, the soapberry extract filtering for impregnating 8h is taken, filtrate three is obtained, twice with distilled water flushing filter residue, obtains filtrate four;
F, it is concentrated by evaporation:Merging filtrate one, filtrate two, filtrate three and filtrate four obtain water with 100 DEG C of evaporation and concentration 5h of water-bath
Carry concentrate;
G, it extracts repeatedly:Water extracting liquid is poured into separatory funnel, 250mL extracting n-butyl alcohols, separation upper liquid is added to obtain extract liquor
One, liquid is retained, 200mL extracting n-butyl alcohols are added in downward liquid, and it is extract liquor two to obtain upper liquid, and the positive fourths of 200mL are added in liquid still further below
Alcohol extracts, and obtains extract liquor three;
H, rotary evaporation:Combining extraction liquid one, extract liquor two and extract liquor three, with 63 revs/min, 75 DEG C rotations of Rotary Evaporators
Evaporation, recycles n-butanol, and collection obtains soapberry pericarp saponin(e concentrate.
7. preparation method according to claim 5, it is characterised in that:The detailed process of step 2) the extraction flavones liquid
For:
A, fresh Suaeda salsa is collected;
B, the green leaves of Suaeda salsa are all removed, and is put into clean beaker and collects;
C, leaf is eluted with water, is put into alcohol and sterilizes 6 minutes, is then immersed in water, washes away alcohol;
D, Suaeda salsa blades 1g is weighed, is placed in Soxhlet extractor, 70% ethyl alcohol 100mL and a little CaCO3, extracting is added
6-8h pours out extracting solution reduced pressure and boils off ethyl alcohol and obtain concentrate;
E, concentrate is washed 2-3 times in separatory funnel with the ether of same volume, obtains flavones liquid.
8. preparation method according to claim 5, it is characterised in that:The bath temperature of the step 3) is 100 DEG C.
9. preparation method according to claim 5, it is characterised in that:The mixing time of the step 5) is 1 minute.
10. preparation method according to claim 5, it is characterised in that:The addition essential oil of the step 6) is 0.4 gram,
The mixing time of the step 6) is 2 minutes.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109486606A (en) * | 2018-12-26 | 2019-03-19 | 湖北工业大学 | A method of saponin(e health liquor is rich in using Stauntonia latifolia production |
CN109609299A (en) * | 2019-01-23 | 2019-04-12 | 杭州善舒生物科技有限公司 | A kind of nanometer of soapberry soap and preparation method thereof |
CN109652247A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of perfumed soap preparation process of the saponin(e containing natural plants |
CN110025498A (en) * | 2019-04-28 | 2019-07-19 | 重庆第二师范学院 | A kind of portable effervesce soap of soapberry and preparation method |
CN111826246A (en) * | 2020-07-10 | 2020-10-27 | 辽宁泓新科技成果转化服务有限公司 | Suaeda salsa perfumed soap formula and processing technology thereof |
CN113913254A (en) * | 2020-07-10 | 2022-01-11 | 辽宁泓新科技成果转化服务有限公司 | Suaeda salsa perfumed soap formula and processing technology thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN109652247A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of perfumed soap preparation process of the saponin(e containing natural plants |
CN109486606A (en) * | 2018-12-26 | 2019-03-19 | 湖北工业大学 | A method of saponin(e health liquor is rich in using Stauntonia latifolia production |
CN109609299A (en) * | 2019-01-23 | 2019-04-12 | 杭州善舒生物科技有限公司 | A kind of nanometer of soapberry soap and preparation method thereof |
CN110025498A (en) * | 2019-04-28 | 2019-07-19 | 重庆第二师范学院 | A kind of portable effervesce soap of soapberry and preparation method |
CN111826246A (en) * | 2020-07-10 | 2020-10-27 | 辽宁泓新科技成果转化服务有限公司 | Suaeda salsa perfumed soap formula and processing technology thereof |
CN113913254A (en) * | 2020-07-10 | 2022-01-11 | 辽宁泓新科技成果转化服务有限公司 | Suaeda salsa perfumed soap formula and processing technology thereof |
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