KR101245034B1 - Functional soap containing rose petal extract and manufacturing method of the same - Google Patents

Functional soap containing rose petal extract and manufacturing method of the same Download PDF

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KR101245034B1
KR101245034B1 KR1020110013584A KR20110013584A KR101245034B1 KR 101245034 B1 KR101245034 B1 KR 101245034B1 KR 1020110013584 A KR1020110013584 A KR 1020110013584A KR 20110013584 A KR20110013584 A KR 20110013584A KR 101245034 B1 KR101245034 B1 KR 101245034B1
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최주순
유명림
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients

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Abstract

본 발명은 장미추출물이 함유된 기능성 비누의 제조방법에 관한 것으로, 더욱 상세하게는 포화지방산에 불포화지방산 및 유화수를 혼합하는 비누화단계, 전술한 비누화단계를 통해 제조된 비누원료에 용제를 혼합하는 용제혼합단계, 용제가 혼합되어 용해된 비누원료에 장미추출물을 첨가하는 첨가제혼합단계 및 첨가제가 혼합된 비누원료를 경화시키는 경화단계를 포함하여 이루어진다.
전술한 장미추출물이 함유된 기능성 비누는 장미향을 방출하며, 미백 및 피부노폐물을 제거효과가 탁월하다.
The present invention relates to a method for producing a functional soap containing a rose extract, and more particularly, a saponification step of mixing unsaturated fatty acids and emulsified water to saturated fatty acids, and mixing the solvent in the soap raw material prepared through the saponification step described above. It comprises a solvent mixing step, an additive mixing step of adding the rose extract to the soap material dissolved in the solvent is mixed and a curing step of curing the soap material mixed with the additive.
Functional soap containing the above-mentioned rose extract releases rose fragrance and is excellent in removing whitening and skin waste.

Description

장미추출물이 함유된 기능성 비누의 제조방법 {FUNCTIONAL SOAP CONTAINING ROSE PETAL EXTRACT AND MANUFACTURING METHOD OF THE SAME }Manufacturing method of functional soap containing rose extract {FUNCTIONAL SOAP CONTAINING ROSE PETAL EXTRACT AND MANUFACTURING METHOD OF THE SAME}

본 발명은 장미추출물이 함유된 기능성 비누의 제조방법에 관한 것으로, 더욱 상세하게는 비누화단계, 용제혼합단계, 첨가제혼합단계 및 경화단계를 포함한다.
The present invention relates to a method for producing a functional soap containing a rose extract, and more particularly includes a saponification step, a solvent mixing step, an additive mixing step and a curing step.

본 발명은 장미추출물이 함유된 기능성 비누의 제조방법에 관한 것으로, 더욱 상세하게는 비누화단계, 용제혼합단계, 첨가제혼합단계 및 경화단계를 포함한다.The present invention relates to a method for producing a functional soap containing a rose extract, and more particularly includes a saponification step, a solvent mixing step, an additive mixing step and a curing step.

종래에 사용되던 일반비누는 유지(우지, 돈지, 양지 등)와 야자유를 적량 배합하여 60 내지 70℃의 온도로 가열 용해한 후 수산화나트륨(NaOH)을 첨가하여 비누화 반응을 실시하고, 상층에 뜬 비누로부터 하층에 가라앉는 비누화 반응의 부산물인 물, 미반응 수산화나트륨, 글리세린 층 등을 분리 제거한 다음, 진한 소금물을 1 내지 2회 가하여 비누속에 있는 잔류 글리세린과 수산화나트륨 등을 제거하여 통상의 비누 층을 얻고, 이를 진공 건조하여 수분을 13% 정도 함유한 상태로 제조된다. 이와 같이 제조된 비누에 소량의 산화 방지제, 보색제, 지방산 향료 또는 식물성 향료 등을 배합하여 성형 제조하여 완성된다.Conventional soaps used in the prior art are formulated with a proper amount of fats and oils (Uji, pork, sunny), palm oil and dissolved at a temperature of 60 to 70 ℃, followed by saponification by adding sodium hydroxide (NaOH), and soap Water, unreacted sodium hydroxide, glycerin layer, etc., which are by-products of the saponification reaction sinking to the lower layer, are separated and then concentrated brine is added once or twice to remove residual glycerin and sodium hydroxide in the soap, thereby removing ordinary soap layers. It is obtained, and vacuum dried to prepare a state containing about 13% moisture. A small amount of antioxidants, complementary agents, fatty acid flavors or vegetable flavors and the like are added to the soaps thus prepared to form a molded product.

또한, 최근에는 여러 가지 과일이나, 꽃의 향을 나타내는 첨가제를 혼합하는 기능성 비누가 제조되고 있으나, 전술한 종래에 기능성 비누는 화학성분을 합성하여 인공적인 향을 방출하도록 한 것으로, 통상적인 청결성 유지와 향을 방출하는 것 말고는 피부에 별다른 기능성을 나타내지 못하는 문제점이 있었다.
In addition, in recent years, functional soaps have been prepared for mixing various fruit or flower flavor additives, but in the above-described conventional functional soaps to synthesize artificial ingredients to release artificial flavors, maintaining normal cleanliness Except for releasing the fragrance and there was a problem that does not show any functional on the skin.

본 발명의 목적은 장미추출물이 함유되어 장미향을 방출하고, 피부 독성제거 및 미백효과가 탁월한 기능성 비누를 제공하는 장미추출물을 함유한 기능성 비누의 제조방법을 제공하는 것이다.
An object of the present invention is to provide a method for producing a functional soap containing a rose extract containing a rose extract to release the fragrance of roses, providing a functional soap with excellent skin toxicity removal and whitening effect.

본 발명의 목적은 포화지방산에 불포화지방산 및 유화수를 혼합하는 비누화단계, 상기 비누화단계를 통해 제조된 비누원료에 용제를 혼합하는 용제혼합단계, 용제가 혼합되어 용해된 비누원료에 장미추출물을 첨가하는 첨가제혼합단계 및 첨가제가 혼합된 비누원료를 경화시키는 경화단계를 포함하는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법을 제공함에 의해 달성된다.An object of the present invention is a saponification step of mixing unsaturated fatty acid and emulsified water to saturated fatty acid, a solvent mixing step of mixing a solvent in the soap raw material prepared through the saponification step, the solvent is mixed and the rose extract is added to the dissolved soap raw material It is achieved by providing a method for producing a functional soap containing a rose extract, characterized in that it comprises an additive mixing step and a curing step of curing the soap material mixed with the additive.

본 발명의 바람직한 특징에 따르면, 상기 비누화단계는 포화지방산 160 내지 280 중량부에 불포화지방산 10 내지 30 중량부 및 유화수 10 내지 15 중량부를 혼합하고, 45 내지 75℃의 온도로 가열하여 이루어지는 것으로 한다.According to a preferred feature of the invention, the saponification step is to be made by mixing 10 to 30 parts by weight of unsaturated fatty acid and 10 to 15 parts by weight of emulsified water to 160 to 280 parts by weight of saturated fatty acid, and heated to a temperature of 45 to 75 ℃ .

본 발명의 더 바람직한 특징에 따르면, 상기 포화지방산은 스테아린산 100 중량부, 팔미트산 20 내지 60 중량부, 미리스트산 20 내지 60 중량부 및 라우르산 20 내지 60 중량부를 포함하는 것으로 한다.According to a more preferred feature of the invention, the saturated fatty acid is to include 100 parts by weight of stearic acid, 20 to 60 parts by weight of palmitic acid, 20 to 60 parts by weight of myristic acid and 20 to 60 parts by weight of lauric acid.

본 발명의 더욱 바람직한 특징에 따르면, 상기 불포화지방산은 코코넛오일 5 내지 10 중량부, 올리브유 3 내지 7 중량부, 피마자오일 5 내지 7 중량부 및 시어버터오일 0.5 내지 1.5 중량부를 포함하는 것으로 한다.According to a more preferred feature of the present invention, the unsaturated fatty acid is 5 to 10 parts by weight of coconut oil, 3 to 7 parts by weight of olive oil, 5 to 7 parts by weight of castor oil and 0.5 to 1.5 parts by weight of shea butter oil.

본 발명의 더욱 더 바람직한 특징에 따르면, 상기 용제혼합단계는 비누원료 100 중량부에 용제 60 내지 200 중량부를 혼합하여 이루어지는 것으로 한다.According to a further preferred feature of the invention, the solvent mixing step is to be made by mixing 60 to 200 parts by weight of the solvent to 100 parts by weight of the soap raw material.

본 발명의 더욱 더 바람직한 특징에 따르면, 상기 용제는 솔비톨 20 내지 70 중량부, 에탄올 10 내지 60 중량부, 트리에탄올아민 10 내지 40 중량부 및 글리세린 20 내지 70 중량부를 포함하는 것으로 한다.According to a still more preferred feature of the present invention, the solvent comprises 20 to 70 parts by weight of sorbitol, 10 to 60 parts by weight of ethanol, 10 to 40 parts by weight of triethanolamine and 20 to 70 parts by weight of glycerin.

본 발명의 더욱 더 바람직한 특징에 따르면, 상기 첨가제 혼합단계는 용제가 혼합되어 용해된 비누원료 100 중량부에 장미추출물 2 내지 3 중량부를 혼합하여 이루어지는 것으로 한다.According to a further preferred feature of the present invention, the additive mixing step is to be made by mixing 2 to 3 parts by weight of the rose extract to 100 parts by weight of the dissolved soap material mixed with the solvent.

본 발명의 더욱 더 바람직한 특징에 따르면, 상기 장미추출물은 장미꽃잎 100 중량부와 정제수 1000 중량부를 중탕기에 넣고, 상기 중탕기를 100 내지 110℃의 온도로 3시간 동안 가동하여 추출되는 것으로 한다.According to a still more preferred feature of the present invention, the rose extract is put into 100 parts by weight of rose petals and 1000 parts by weight of purified water in a water bath, it is to be extracted by operating the water bath at a temperature of 100 to 110 ℃ for 3 hours.

본 발명의 더욱 더 바람직한 특징에 따르면, 상기 장미추출물은 장미꽃잎 100 중량부와 설탕물 100 중량부를 밀폐용기에 넣고 80 내지 100일 동안 발효한 후에 여과하여 추출되는 것으로 한다.
According to an even more preferred feature of the present invention, the rose extract is 100 parts by weight of rose petals and 100 parts by weight of sugar water is put into a sealed container and fermented for 80 to 100 days and then filtered.

본 발명에 따른 장미추출물을 함유한 기능성 비누의 제조방법은 장미추출물이 함유되어 장미향을 방출하고, 피부 독성제거 및 미백효과가 탁월한 기능성 비누를 제공하는 효과를 나타낸다.
The manufacturing method of the functional soap containing the rose extract according to the present invention has the effect of providing a functional soap containing the rose extract to release the fragrance of roses, excellent skin removal and whitening effect.

도 1은 본 발명에 따른 장미추출물을 함유한 기능성 비누의 제조방법을 나타낸 순서도이다.1 is a flow chart showing a method for producing a functional soap containing a rose extract according to the present invention.

이하에는, 본 발명의 바람직한 실시예와 각 성분의 물성을 상세하게 설명하되, 이는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 발명을 용이하게 실시할 수 있을 정도로 상세하게 설명하기 위한 것이지, 이로 인해 본 발명의 기술적인 사상 및 범주가 한정되는 것을 의미하지는 않는다.
Hereinafter, preferred embodiments of the present invention and physical properties of the respective components will be described in detail with reference to the accompanying drawings. However, the present invention is not limited thereto, And this does not mean that the technical idea and scope of the present invention are limited.

본 발명에 따른 장미추출물이 함유된 기능성 비누의 제조방법은 포화지방산에 불포화지방산 및 유화수를 혼합하는 비누화단계(S101), 전술한 비누화단계(S101)를 통해 제조된 비누원료에 용제를 혼합하는 용제혼합단계(S103), 용제가 혼합되어 용해된 비누원료에 장미추출물을 첨가하는 첨가제혼합단계(S105) 및 첨가제가 혼합된 비누원료를 경화시키는 경화단계(S107)를 포함하여 이루어진다.
The method for producing a functional soap containing a rose extract according to the present invention is a saponification step of mixing unsaturated fatty acid and emulsified water in saturated fatty acid (S101), by mixing the solvent in the soap raw material prepared through the above-described saponification step (S101) It includes a solvent mixing step (S103), an additive mixing step (S105) of adding a rose extract to a soap material in which the solvent is dissolved and a curing step (S107) of curing the soap material in which the additive is mixed.

전술한 비누화단계(S101)는 포화지방산에 불포화지방산 및 유화수를 혼합하는 단계로, 포화지방산 160 내지 280 중량부에 불포화지방산 10 내지 30 중량부 및 유화수 10 내지 15 중량부를 혼합하고, 45 내지 75℃의 온도로 가열하여 비누화된 비누원료를 제조한다.The above saponification step (S101) is a step of mixing unsaturated fatty acid and emulsified water with saturated fatty acid, 160 to 280 parts by weight of saturated fatty acid, 10 to 30 parts by weight of unsaturated fatty acid and 10 to 15 parts by weight of emulsified water, and 45 to Heated to a temperature of 75 ℃ to prepare a saponified soap raw material.

이때, 전술한 포화지방산은 스테아린산 100 중량부, 팔미트산 20 내지 60 중량부, 미리스트산 20 내지 60 중량부 및 라우르산 20 내지 60 중량부를 포함하여 이루어지며, 전술한 불포화지방산은 동백유 5 내지 10 중량부, 포도씨유 3 내지 7 중량부, 피마자오일 5 내지 7 중량부를 포함하여 이루어지고, 전술한 유화수는 10 내지 15 중량부가 첨가되는데, 수산화나트륨으로 이루어진 가성소다를 대신하여 사용되는 강염기성의 물질로 비누제조에 사용되는 대표적인 반응제다.At this time, the above-mentioned saturated fatty acid comprises 100 parts by weight of stearic acid, 20 to 60 parts by weight of palmitic acid, 20 to 60 parts by weight of myristic acid and 20 to 60 parts by weight of lauric acid, the above-mentioned unsaturated fatty acid is camellia oil 5 It comprises 10 to 10 parts by weight, grape seed oil 3 to 7 parts by weight, castor oil 5 to 7 parts by weight, the above-mentioned emulsified water is added 10 to 15 parts by weight, a strong base used in place of caustic soda made of sodium hydroxide It is a typical substance used in soap production.

수산화나트륨을 사용하여 비누를 제조하게 되면 50일 이상이 경과 한 후에 수소이온수치가 낮아져 피부에 비누를 사용할 수 있으나, 유화수는 전술한 지방산 또는 불포화지방산과 반응한 후에 곧바로 피부에 사용할 수 있는 장점이 있다.When soap is manufactured using sodium hydroxide, the hydrogen ion level is lowered after 50 days or more, and soap can be used on the skin. However, emulsified water can be used on the skin immediately after reacting with the aforementioned fatty acid or unsaturated fatty acid. There is this.

전술한 스테아린산은 비누의 경화성을 향상시키고, 전술한 팔미트산은 보습효과가 우수하며, 전술한 미리스트산은 잔거품의 발생을 유도하고, 전술한 라우르산은 굵은거품의 발생을 유도한다.The stearic acid described above improves the curability of the soap, the palmitic acid described above is excellent in the moisturizing effect, the above-mentioned myristic acid induces the generation of residual bubbles, the lauric acid induces the generation of coarse bubbles.

또한, 전술한 동백유 및 포도씨유는 클렌징효과가 우수하며, 전술한 피마자오일은 우수한 보습효과를 나타낸다.In addition, the above-mentioned camellia oil and grape seed oil have an excellent cleansing effect, the above-mentioned castor oil shows an excellent moisturizing effect.

전술한 스테아린산의 용융온도는 71 내지 71.5℃이며, 전술한 팔미트산의 용융온도는 62.6℃이고, 전술한 미리스트산의 용융온도는 58.8℃이며, 전술한 라우르산의 용융온도는 43.5℃를 나타내기 때문에, 전술한 비누화단계는 45 내지 75℃의 온도로 가열하는 것이 바람직하며, 70 내지 75℃로 가열하는 것이 더욱 바람직하다.
The above-mentioned melting temperature of stearic acid is 71 to 71.5 ° C, the above-mentioned melting temperature of palmitic acid is 62.6 ° C, the above-mentioned melting temperature of myristic acid is 58.8 ° C, and the above-mentioned melting temperature of lauric acid is 43.5 ° C. Since the saponification step described above is preferably heated to a temperature of 45 to 75 ℃, it is more preferable to heat to 70 to 75 ℃.

전술한 용제혼합단계(S103)는 전술한 비누화단계(S101)를 통해 제조된 비누원료에 용제를 혼합하는 단계로, 비누원료 100 중량부에 용제 60 내지 200 중량부를 혼합하여 이루어지는데, 전술한 용제는 전술한 비누원료를 용해시켜, 전술한 장미추출물과 비누원료가 고르게 혼합될 수 있도록 하는 역할을 한다.The above-described solvent mixing step (S103) is a step of mixing the solvent in the soap raw material prepared through the saponification step (S101) described above, it is made by mixing 60 to 200 parts by weight of the solvent to 100 parts by weight of the soap raw material, the solvent Dissolves the above-described soap raw material, and serves to allow the above-mentioned rose extract and soap raw material to be evenly mixed.

이때, 전술한 용제는 솔비톨 20 내지 70 중량부, 에탄올 10 내지 60 중량부, 트리에탄올아민 10 내지 40 중량부 및 글리세린 20 내지 70 중량부를 혼합하여 이루어지는데, 전술한 용제혼합단계(S103)는 비누원료를 80 내지 90℃의 온도로 가열하면서 용제를 혼합하고 교반하여 이루어지며, 더욱 바람직하게는 글리세린과 에탄올을 비누원료에 첨가한 후에 80℃의 온도로 가열하여 혼합물이 일정부분 용융되면, 솔비톨 및 트리에탄올아민을 첨가하고 90℃의 온도로 가열하면서 저어주어 혼합한다.At this time, the above-described solvent is made by mixing 20 to 70 parts by weight of sorbitol, 10 to 60 parts by weight of ethanol, 10 to 40 parts by weight of triethanolamine and 20 to 70 parts by weight of glycerin, the above-described solvent mixing step (S103) is a soap raw material It is made by mixing and stirring the solvent while heating to a temperature of 80 to 90 ℃, more preferably, glycerol and ethanol is added to the soap raw material and then heated to a temperature of 80 ℃ when the mixture is partially melted, sorbitol and triethanol Add amine and stir while heating to 90 ° C. and mix.

전술한 글리세린은 글리세롤이라고도 하는데, 천연보습제이며, 피부에 보습효과를 부여하여 화장품에 널리 사용되고 있으며, 전술한 솔비톨은 흡습성이 강하고 물과 에탄올 등에 잘 용해되어 화장용 크림이나 로션 등에 주로 사용된다.
Glycerol, also referred to as glycerol, is a natural moisturizer and is widely used in cosmetics by imparting a moisturizing effect to the skin. The aforementioned sorbitol is strongly hygroscopic and well dissolved in water and ethanol, and is mainly used in cosmetic creams or lotions.

전술한 첨가제혼합단계(S105)는 전술한 용제가 혼합되어 용해된 비누원료에 장미추출물을 첨가하는 단계로, 용제가 혼합되어 용해된 비누원료 100 중량부에 장미추출물 2 내지 3 중량부를 혼합하여 이루어지는데, 전술한 장미추출물은 장미향을 방출하고, 피부의 독성을 제거할 뿐만 아니라, 탁월한 미백효과를 나타내는 기능성 비누를 제공할 수 있도록 하는 역할을 한다.The above-described additive mixing step (S105) is a step of adding a rose extract to a soap material in which the aforementioned solvent is mixed and dissolved, by mixing 2 to 3 parts by weight of a rose extract to 100 parts by weight of the dissolved soap material. The rose extract described above serves to release the fragrance of roses, remove the toxicity of the skin, and provide a functional soap that exhibits an excellent whitening effect.

이때, 전술한 장미추출물은 장미꽃잎 100 중량부와 정제수 1000 중량부를 중탕기에 넣고, 전술한 중탕기를 100 내지 110℃의 온도로 3시간 동안 가동하여 추출된 것이 사용되는데, 더욱 바람직하게는, 생장미의 꽃송이가 80% 정도 개화 상태일 때, 장미꽃잎을 채취하고, 채취한 장미꽃잎 100 중량부와 정제수 1000 중량부를 중탕기에 넣고 107℃의 온도로 3시간 동안 중탕한 후에 농축된 농축액과 중탕과정에서 증류된 증류액을 다시 혼합하여 제조된 장미추출물이 사용된다.At this time, the above-mentioned rose extract is used to put 100 parts by weight of rose petals and 1000 parts by weight of purified water in a water bath, and the extract is operated by running the above-described water bath at a temperature of 100 to 110 ℃ for 3 hours, more preferably, the growing rice When the blossoms of the plant are about 80% blooming, the rose petals are collected, 100 parts by weight of the collected rose petals and 1000 parts by weight of purified water are placed in a water bath, and the mixture is bathed at a temperature of 107 ° C. for 3 hours. Rose extract prepared by mixing the distilled distillate again is used.

또한, 전술한 장미추출물은 장미꽃잎 100 중량부와 설탕물 100 중량부를 밀폐용기에 넣고 80 내지 100일 동안 발효한 후에 여과하여 추출된 것이 사용될 수도 있는데, 더욱 바람직하게는 생장미의 꽃송이가 80% 정도 개화 상태일 때, 장미꽃잎을 채취하고 설탕과 물이 1:1의 비율로 혼합된 설탕물이 담긴 용기에 전술한 장미꽃잎을 넣어 밀봉하고 90일 동안 발효시킨 후에 발효된 혼합물을 필터로 걸러서 제조되는 장미추출물이 사용된다.In addition, the rose extract described above may be used to extract 100 parts by weight of rose petals and 100 parts by weight of sugar water in an airtight container and fermented for 80 to 100 days, followed by filtration. When it is in full bloom, the rose petals are collected and sealed in a container containing sugar water in which sugar and water are mixed at a ratio of 1: 1. After sealing, the fermented mixture is filtered through a filter. Prepared rose extracts are used.

전술한 경화단계(S105)는 첨가제가 혼합된 비누원료를 경화시키는 단계로, 첨가제가 혼합된 비누원료를 원하는 형태로 형성된 용기에 담은 후에 상온으로 냉각하고, 20 내지 30 시간 동안 건조한 후에 용기를 제거하여 비누로 제조하는 단계다.
The above-mentioned curing step (S105) is a step of curing the soap material mixed with the additives, the soap material mixed with the additives in a container formed in the desired form, then cooled to room temperature, dried for 20 to 30 hours and then removed the container To prepare a soap.

전술한 것처럼 본 발명에 따른, 장미추출물이 함유된 기능성 비누의 제조방법은 포화지방산에 불포화지방산을 혼합하는 비누화단계(S101), 전술한 비누화단계(S101)를 통해 제조된 비누원료에 용제를 혼합하는 용제혼합단계(S103), 용제가 혼합되어 용해된 비누원료에 장미추출물을 첨가하는 첨가제혼합단계(S105) 및 첨가제가 혼합된 비누원료를 경화시키는 경화단계(S107)를 포함하는 이루어지며, 장미추출물이 함유되어 장미향을 방출하고, 피부 독성제거 및 미백효과가 탁월한 기능성 비누를 제공한다.
As described above, according to the present invention, a method for preparing a functional soap containing a rose extract is a saponification step of mixing unsaturated fatty acids with saturated fatty acids (S101), mixing the solvent in the soap raw materials prepared through the above-mentioned saponification step (S101). To the solvent mixing step (S103), the solvent is mixed, the additive mixture step of adding the rose extract to the dissolved soap material (S105) and the curing agent comprises a curing step (S107) to cure the mixed soap material is made, Contains extract to release rose fragrance and provides functional soap with excellent skin toxicity removal and whitening effect.

S101 ; 비누화단계
S103 ; 용제혼합단계
S105 ; 첨가제혼합단계
S107 ; 경화단계
S101; Saponification Step
S103; Solvent Mixing Step
S105; Additive Mixing Step
S107; Curing step

Claims (9)

포화지방산에 불포화지방산 및 유화수를 혼합하는 비누화단계;
상기 비누화단계를 통해 제조된 비누원료에 용제를 혼합하는 용제혼합단계;
용제가 혼합되어 용해된 비누원료 100 중량부에 장미추출물 2 내지 3 중량부를 첨가하는 첨가제혼합단계; 및
첨가제가 혼합된 비누원료를 경화시키는 경화단계;를 포함하며,
상기 장미추출물은 장미꽃잎 100 중량부와 설탕물 100 중량부를 밀폐용기에 넣고 80 내지 100일 동안 발효한 후에 여과하여 추출되는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
Saponification step of mixing unsaturated fatty acid and emulsified water to saturated fatty acid;
A solvent mixing step of mixing a solvent in the soap raw material manufactured through the saponification step;
An additive mixing step of adding 2 to 3 parts by weight of a rose extract to 100 parts by weight of a dissolved soap material mixed with a solvent; And
It includes; a curing step of curing the soap material mixed with the additive;
The rose extract is 100 parts by weight of rose petals and 100 parts by weight of sugar water in a sealed container and fermented for 80 to 100 days, and then filtered and extracted.
청구항 1에 있어서,
상기 비누화단계는 포화지방산 160 내지 280 중량부에 불포화지방산 10 내지 30 중량부 및 유화수 10 내지 15 중량부를 혼합하고, 45 내지 75℃의 온도로 가열하여 이루어지는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
The method according to claim 1,
The saponification step is a mixture containing 10 to 30 parts by weight of unsaturated fatty acid and 10 to 15 parts by weight of emulsified water in 160 to 280 parts by weight of saturated fatty acid, and functionalized containing rose extract, characterized in that the heating is carried out at a temperature of 45 to 75 ℃ Method of Making Soap.
청구항 2에 있어서,
상기 포화지방산은 스테아린산 100 중량부, 팔미트산 20 내지 60 중량부, 미리스트산 20 내지 60 중량부 및 라우르산 20 내지 60 중량부를 포함하는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
The method according to claim 2,
The saturated fatty acid is 100 parts by weight of stearic acid, 20 to 60 parts by weight of palmitic acid, 20 to 60 parts by weight of myristic acid and 20 to 60 parts by weight of lauric acid to prepare a functional extract containing a rose extract Way.
청구항 2에 있어서,
상기 불포화지방산은 코코넛오일 5 내지 10 중량부, 올리브유 3 내지 7 중량부, 피마자오일 5 내지 7 중량부 및 시어버터오일 0.5 내지 1.5 중량부를 포함하는 것 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
The method according to claim 2,
The unsaturated fatty acid is prepared from 5 to 10 parts by weight of coconut oil, 3 to 7 parts by weight of olive oil, 5 to 7 parts by weight of castor oil, and 0.5 to 1.5 parts by weight of shea butter oil. Way.
청구항 1에 있어서,
상기 용제혼합단계는 비누원료 100 중량부에 용제 60 내지 200 중량부를 혼합하여 이루어지는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
The method according to claim 1,
The solvent mixing step is a method of producing a functional soap containing a rose extract, characterized in that by mixing 60 to 200 parts by weight of a solvent to 100 parts by weight of soap raw material.
청구항 5에 있어서,
상기 용제는 솔비톨 20 내지 70 중량부, 에탄올 10 내지 60 중량부, 트리에탄올아민 10 내지 40 중량부 및 글리세린 20 내지 70 중량부를 포함하는 것을 특징으로 하는 장미추출물이 함유된 기능성 비누의 제조방법.
The method according to claim 5,
The solvent is 20 to 70 parts by weight of sorbitol, 10 to 60 parts by weight of ethanol, 10 to 40 parts by weight of triethanolamine and 20 to 70 parts by weight of glycerin, the method of producing a functional soap containing a rose extract.
삭제delete 삭제delete 삭제delete
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KR20060101096A (en) * 2005-03-19 2006-09-22 정세영 Rose extract with skin wrinkle improvement effect
KR100893622B1 (en) 2008-07-10 2009-04-20 신영수 Soap and it's making method for smell clearance using salicornia herbacea and white lotus
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020062513A (en) * 2001-01-22 2002-07-26 한국화장품주식회사 rose petal extract with skin whitening function and skin whitening cosmetic composition containg the same
KR20060101096A (en) * 2005-03-19 2006-09-22 정세영 Rose extract with skin wrinkle improvement effect
KR100893622B1 (en) 2008-07-10 2009-04-20 신영수 Soap and it's making method for smell clearance using salicornia herbacea and white lotus
KR20090093920A (en) * 2009-08-13 2009-09-02 정동명 Separatea type manufactured material for natural soap

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