KR20080072122A - The cosmetic composition and its manufacturing method including flower petal - Google Patents

The cosmetic composition and its manufacturing method including flower petal Download PDF

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KR20080072122A
KR20080072122A KR1020070010400A KR20070010400A KR20080072122A KR 20080072122 A KR20080072122 A KR 20080072122A KR 1020070010400 A KR1020070010400 A KR 1020070010400A KR 20070010400 A KR20070010400 A KR 20070010400A KR 20080072122 A KR20080072122 A KR 20080072122A
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petals
cosmetic composition
solution
softening
petal
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KR1020070010400A
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Korean (ko)
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KR101425454B1 (en
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오주영
최수규
이정래
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주식회사 엘지생활건강
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
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  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

A cosmetic composition comprising petals is provided to show skin beauty effect of moisturizing, whitening, and anti-wrinkling due to the petals and beauty ingredients eluted therefrom and provide visual satisfaction by maintaining a shape of petals as it is in the cosmetic. A cosmetic composition comprises softened and decolored petals, ingredients eluted therefrom, a solvent for softening and decoloring, a polyacrylic based polymer and a polyol. A method for preparing the cosmetic composition comprises the steps of: (a) extracting dried petals with a solution where a ratio of ethanol and water is 1:2-2:1 at room temperature for 12-48 hours to prepare a solution including the petals; and (b) mixing the solution with a base solution. Further, the decolored petals are selected from rose, chrysanthemum and marigold.

Description

꽃잎이 함유된 화장료 조성물 및 이의 제조방법 {The cosmetic composition and its manufacturing method including flower petal}Cosmetic composition containing petals and a method for producing the same {The cosmetic composition and its manufacturing method including flower petal}

본 발명은 다양한 꽃잎 및 그로부터 용출된 미용성분을 그대로 함유하는 화장료조성물 및 이의 제조방법에 관한 것이다.The present invention relates to a cosmetic composition containing a variety of petals and cosmetic ingredients eluted therefrom and a method for producing the same.

꽃잎(Flower Petal)은 장미, 국화, 연, 마리골드, 카모마일, 금잔화, 개나리, 난초, 동백, 데이지, 라일락, 목련, 무궁화, 민들레, 백합, 봉선화, 수련, 수선화, 아네모네, 아이리스, 옥잠화, 월계수, 제라늄, 자스민, 카네이션, 칸나, 튜울립, 팬지, 프리지하, 해바라기, 하이신스 등이 이용될 수 있으며, 건조가 가능하고 건조 후에도 고유의 꽃잎 색깔을 어느정도 유지하고 미용성분을 포함하고 있는 것이라면 모두 사용가능하다.Flower Petal is rose, chrysanthemum, lotus, marigold, chamomile, marigold, forsythia, orchid, camellia, daisy, lilac, magnolia, rose of sharon, dandelion, lily, balsam, water lily, narcissus, anemone, iris, daylily, laurel , Geranium, Jasmine, Carnation, Canna, Tulip, Pansy, Freeze, Sunflower, High Synth, etc. can be used, and if it is dry and maintains its original petal color to some extent and contains beauty ingredients It is possible.

예를 들면, 장미꽃에는 비타민류, 니코틴산, 유기산, 탄닌이 풍부하여 미백, 항염 효과가 좋은 것으로 알려져 있다. 꽃잎은 필요시 편리한 사용을 위하여 건조하여 사용하는 것이 바람직한데, 냉동건조 또는 가열건조 후 적절한 보관에 의해 빨간색, 노란색, 흰색 등 본래의 장미꽃 종류에 따라 그 고유의 색깔과 향을 간직하고 있다.For example, rose flowers are rich in vitamins, nicotinic acid, organic acids, and tannins, and are known to have good whitening and anti-inflammatory effects. Petals are preferably dried and used for convenient use. They retain their unique color and scent according to the original rose type such as red, yellow, and white by appropriate storage after freeze drying or heat drying.

이러한 건조꽃잎을 화장료에 그대로 넣거나, 분쇄하여 넣음으로써 시각 차별화를 꾀하는 화장료들이 있으나, 몇가지 문제점들이 있다. 예를들면, 건조 꽃잎을 화장료에 그대로 적용시, 연화되지 않아 딱딱하여 제조가 어렵고, 사용 품질이 나빠 제품적으로도 가치가 적었다. 또한, 제품 내에서 꽃잎 색소인 안토시아닌, 카로티노이드 등 색소성분이 시간이 지남에 따라 탈색되는데, 화장료 내에서 색소농도의 분포가 달라져 시각적으로 좋지 못하다는 단점이 있다.There are some cosmetics for visual differentiation by putting these dried petals in cosmetics or by crushing them, but there are some problems. For example, when dried petals are applied to cosmetics as they are, they are not softened because they do not soften and are difficult to manufacture. In addition, the pigment components such as anthocyanin, carotenoids, such as petal pigments in the product is discolored over time, there is a disadvantage that the distribution of pigment concentration in the cosmetics is not good visually.

이외에, 꽃잎을 과산화수소 등 탈색제를 이용하여 단시간 내에 탈색시킨 후, 원하는 인공색소를 가미하여 꽃잎의 색상을 인위적으로 재생하여 방향제, 악세사리 등에 활용하는 생활용품 및 잡기류가 있으나, 꽃잎의 고유한 성분을 함유하지 못하며, 탈색된 꽃잎의 표면이 상하고 거칠어 자연적이지 못하다는 단점이 있다. In addition, there are daily necessities and catches that decolorize the petals in a short time by using a bleaching agent such as hydrogen peroxide, and artificially reproduce the color of the petals by adding a desired artificial pigment to utilize fragrances and accessories. It does not contain and has the disadvantage that the surface of the discolored petal is damaged and rough and not natural.

따라서, 본 발명이 이루고자 하는 기술적 과제는 건조 꽃잎을 꽃잎 모양 그대로 연화, 탈색시키고 이를 위해 사용된 용매 성분 및 꽃잎으로부터 용출된 성분을 모두 포함시켜 화장료에 적용함으로써, 사용된 꽃잎의 피부 미용 효과를 기대할 수 있으며 연화된 꽃잎이 손의 힘으로 뭉게져 피부에 흡수되며 내용물이 투명상이고 마사지감이 우수하여 시각적, 감촉적으로 차별화된 사용감을 갖는 화장료 조성물을 제공하는데 그 목적이 있다.Therefore, the technical problem to be achieved by the present invention is to soften and decolorize the dry petals as the petal shape, and to apply to the cosmetic by including both the solvent component and the components eluted from the petals, the skin beauty effect of the petals used can be expected And softened petals are aggregated by the power of the hand is absorbed into the skin, the contents are transparent and excellent massage feeling is to provide a cosmetic composition having a visual, feel differentiating feeling.

상기 기술적 과제를 달성하기 위하여, 건조 꽃잎을 자연스럽게 연화, 탈색시키고, 연화, 탈색을 위하여 사용된 용매와 이로부터 용출된 성분을 모두 포함시키 는 것을 특징으로 한다.In order to achieve the above technical problem, the dried petals are naturally softened, decolorized, characterized in that it comprises both the solvent used for softening, decolorization and components eluted therefrom.

보다 상세하게, 본 발명은 열풍 건조, 냉동 건조 후 마른 상태로 잘 보관된 꽃잎을 에탄올과 물의 비율이 1:2 내지 2:1인 용매에 상온에서 12시간 내지 48시간 담가둔다. 담가두는 시간은 건조 꽃잎의 종류 및 건조 상태에 달라질 수 있으며 침적 동안 꽃잎의 부패를 방지하고 투명상의 화장료를 제조하기 위해 방부제나 가용화제를 상기 용출 용매에 미리 녹여 함께 사용할 수 있으며, 용출 속도를 조절하고 충분한 침적량을 확보하기 위해 화장료에 사용되는 폴리올을 사용할 수 있다. 이럴 경우 꽃잎이 연화되고 꽃잎에 들어있는 천연색소와 미용 성분들이 사용된 용매에 용출되며, 꽃잎 본래의 외관을 그대로 유지할 수 있다.More specifically, the present invention is soaked in a dry state after hot air drying, freeze-drying petals soaked in a solvent with a ratio of ethanol and water of 1: 2 to 2: 1 12 hours to 48 hours at room temperature. The soaking time may vary depending on the type and dry condition of the dried petals, and pre-dissolved preservatives or solubilizers can be used together in the elution solvent to prevent decay of the petals during deposition and to prepare a transparent cosmetic, and to control the dissolution rate. And polyols used in cosmetics may be used to ensure sufficient deposition amount. In this case, the petals are softened, and the natural pigments and cosmetic ingredients contained in the petals are eluted in the solvent used, and the original appearance of the petals can be maintained.

본 발명에서 사용되는 건조 꽃잎은 장미, 국화, 연, 마리골드, 카모마일, 금잔화, 개나리, 난초, 동백, 데이지, 라일락, 목련, 무궁화, 민들레, 백합, 봉선화, 수련, 수선화, 아네모네, 아이리스, 옥잠화, 월계수, 제라늄, 자스민, 카네이션, 칸나, 튜울립, 팬지, 프리지하, 해바라기, 하이신스 등이 선택될 수 있으며 그 크기 및 색깔은 구애받지 않으나 장미, 국화, 마리골드 등이 보다 바람직하며, 미리 분쇄나 절단되지 않아 꽃잎 그대로의 모양을 간직하고 있는 꽃잎을 사용하는 것이 바람직히다.The dried petals used in the present invention are roses, chrysanthemums, lotuses, marigolds, chamomiles, marigolds, forsythias, orchids, camellia, daisies, lilacs, magnolias, rose of sharon, dandelions, lilies, balsams, water lilies, narcissus, anemone, iris, daylily , Laurel, geranium, jasmine, carnation, canna, tulip, pansy, freesia, sunflower, high-synth, etc. can be selected, regardless of the size and color, but more preferably roses, chrysanthemum, marigold, etc. It is advisable to use petals that are not cut and retain their shape.

본 발명에서 사용되는 건조 꽃잎의 양은 화장료 조성물 총량의 0.1 내지 5 중량%가 바람직하며, 연화 및 용출에 필요한 용매의 총량은 1 내지 30 중량%가 바람직하다.The amount of dry petal used in the present invention is preferably 0.1 to 5% by weight of the total amount of the cosmetic composition, and the total amount of the solvent required for softening and dissolution is preferably 1 to 30% by weight.

본 발명은 화장료 조성물로써, 사용된 꽃잎을 외관적으로 쉽게 확인할 수 있 는 심미적 특성 및 좋은 마사지감 등의 사용감을 위하여 투명 외관 및 손의 놀림에 알맞은 점탄성 특성을 갖도록 하는 것이 중요한데, 이를 위하여 알킬(alkyl)기와 같이 친유성의 작용기가 부가되지 않은, 친수기만으로 구성된 폴리아크릴산으로부터 유도된 고분자들과 폴리올을 함께 사용하여 화장료 제형을 만드는 것이 바람직하다.The present invention is a cosmetic composition, it is important to have a viscoelastic property suitable for the transparent appearance and hand teasing for aesthetic properties and good massage feeling such that the used petals can be easily seen in appearance, for this purpose, alkyl ( It is preferable to make a cosmetic formulation using a polyol together with polymers derived from polyacrylic acid consisting only of hydrophilic groups, to which no lipophilic functional groups are added, such as alkyl).

본 발명에 사용가능한 폴리아크릴산계 고분자로는 카보머, 글리세릴 아크릴레이트/아크릴릭애씨드 코폴리머, 소듐 폴리아크릴레이트로부터 선택된 고분자를 조성물 전체중량 대비 0.1 내지 3 중량% 함유하는 것이 바람직한데, 이들의 분자 구조내에 반드시 친수성기만 포함하여야 하며 중량평균 분자량이 수만 내지 수백만 이하인 것이 바람직하다.The polyacrylic acid polymers usable in the present invention preferably contain 0.1 to 3% by weight of a polymer selected from carbomer, glyceryl acrylate / acrylic acid copolymer, and sodium polyacrylate, based on the total weight of the composition. It is desirable to include only hydrophilic groups in the structure and preferably have a weight average molecular weight of tens of thousands to millions or less.

또한, 본 발명은 5 내지 50 중량%의 폴리올을 포함하며, 구체적으로는 글리세린, 솔비톨, 폴리에틸렌글리콜, 프로필렌글리콜, 디프로필렌글리콜, 부틸렌글로콜로부터 선택되어진다.In addition, the present invention includes 5 to 50% by weight of polyol, and is specifically selected from glycerin, sorbitol, polyethylene glycol, propylene glycol, dipropylene glycol, butylene glycol.

이하, 꽃잎과 그로부터 용출된 모든 성분을 함유하는 본 발명의 화장료 조성물 및 이의 제조방법에 대해 보다 구체적으로 설명한다.Hereinafter, the cosmetic composition of the present invention containing the petals and all the components eluted therefrom and the preparation method thereof will be described in more detail.

본 발명자들은 꽃잎을 이용한 화장료를 연구하던 중, 건조 꽃잎을 수화시켜 쉽게 연화, 탈색시키고 이를 화장료에 그대로 적용할 수 있음을 확인하고 실험한 결과, 피부미용효과, 안정성 및 피부안전성에 문제점이 없음을 확인하고, 이를 토대로 본 발명을 완성하게 되었다.The inventors of the present invention, while researching cosmetics using petals, confirmed that the dried petals can be easily softened and discolored by applying hydration and applied to the cosmetics as a result, and there is no problem in skin beauty effect, stability and skin safety. After confirming this, the present invention was completed.

이하 실시예 및 비교예에 따라 자세히 설명하면 다음과 같다. 그러나, 하기 의 실시예들은 본 발명을 보다 쉽게 이해하기 위하여 제공되는 것일 뿐 본 발명이 하기의 실시예에 한정되는 것은 아니다.When described in detail according to the Examples and Comparative Examples as follows. However, the following examples are merely provided to more easily understand the present invention, and the present invention is not limited to the following examples.

실시예Example 1 내지 2 및  1 and 2 and 비교예Comparative example 1 내지 4 1 to 4

실시예 1 내지 2 및 비교예 1 내지 4 에 기재된 용매를 이용하여 연화/탈색 과정을 수행한 후, 건조 꽃잎의 연화와 탈색 정도, 꽃잎 상태 및 향기를 표1에 비교하였다. 실시예 1 내지 2 및 비교예 1 내지 4는 건조된 적색 건조 장미꽃잎을 사용하였으며, 상온에서 24시간 침출하였다. 연화정도는 꽃잎을 만져보아 그 단단함을 척도로 하였으며, 탈색정도는 꽃잎의 색깔과 용출된 용매의 색깔로 판단하였으며, 꽃잎의 상태는 표면 거칠기와 외관으로, 향기는 건조 꽃잎과 각각 비교하였다. 단위는 모두 그램(gram)이다.After performing the softening / decolorization process using the solvents described in Examples 1 and 2 and Comparative Examples 1 to 4, the softening and decolorization degree of the dried petals, petal state and fragrance were compared to Table 1. Examples 1 to 2 and Comparative Examples 1 to 4 used dried red rose petals, and were leached at room temperature for 24 hours. The degree of softening was measured by touching the petals, and the degree of decolorization was judged by the color of the petals and the color of the eluted solvent. The condition of the petals was surface roughness and appearance, and the fragrance was compared with the dry petals. The units are all grams.

실시예 1Example 1 실시예 2Example 2 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4 정제수Purified water 55 33 55 -- -- -- 에탄올ethanol 55 33 -- 55 -- -- 과산화수소수(30%)Hydrogen peroxide (30%) -- -- -- -- 1010 -- 글리세린glycerin -- 44 55 -- -- 55 프로필렌글리콜Propylene glycol -- -- -- 55 -- 55 건조장미꽃잎Dried rose petals 1One 1One 1One 1One 1One 1One

실시예 1Example 1 실시예 2Example 2 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4 연화정도Softening degree 많이 연화Much softening 많이 연화Much softening 적게 연화Less softening 보통 연화Normal softening 완전 연화Complete softening 적게 연화Less softening 탈색정도Decolorization 많이 탈색A lot of discoloration 많이 탈색A lot of discoloration 적게 탈색Less discoloration 적게 탈색Less discoloration 완전 탈색Complete discoloration 적게 탈색Less discoloration 꽃잎상태Petal 본래 유지Maintaining original 본래 유지Maintaining original 본래 유지Maintaining original 본래 유지Maintaining original 외관 변형Appearance deformation 외관 변형Appearance deformation 향취Aroma 본래 유지Maintaining original 본래 유지Maintaining original 본래 유지Maintaining original 본래 유지Maintaining original 변취Deodorant 본래 유지Maintaining original

본 발명에서와 같이 건조 꽃잎의 연화 및 탈색을 위하여 알코올과 정제수를 섞어쓰는 것이 바람직하며 폴리올을 일부 포함시키는 것도 가능함을 알 수 있다. 과산화수소수를 사용할 경우, 꽃잎의 연화 및 탈색이 가장 우수하나 꽃잎의 외관이 스웰링(swelling)에 의해 본래의 모습을 유지하지 못하였고 표면이 거칠었으며, 과산화수소수의 냄새 및 피부 부작용이 우려되어 수세, 건조 등의 부가적인 작업이 필요한데 이럴 경우 꽃잎으로부터 용출되는 미용성분이 모두 제거되어 본 발명의 취지에 맞지 않았다. 또한, 정제수, 에탄올, 폴리올만으로 각각 연화, 탈색시킬 경우 탈색이 부족하거나, 연화가 부족하거나 연화와 탈색이 모두 부족한 단점이 있었다.As in the present invention, it is preferable to mix alcohol and purified water for softening and decolorizing dry petals, and it is also possible to include some polyol. When hydrogen peroxide solution is used, the softening and discoloration of the petals is the best, but the appearance of the petals is not maintained by the swelling, the surface is rough, and the surface is rough. Additional work such as drying is required, in which case all of the cosmetic ingredients eluted from the petals are removed, which does not fit the purpose of the present invention. In addition, when softening and decolorizing only purified water, ethanol, and polyol, respectively, decolorization is insufficient, softening is insufficient, or both softening and decolorization are insufficient.

다음으로, 꽃잎 용액을 베이스(Base) 용액에 포함시키는 화장물 조성물에 대하여 다음의 실시예 및 비교예를 제조하였다. 꽃잎 용액은 상온에서 24시간 침출시켜 제조하였고, 베이스 용액은 별도로 상온에서 제조한 후 꽃잎 용액과 혼합하여 호모 믹서로 섞어 제조하였다.Next, the following examples and comparative examples were prepared for the cosmetic composition including the petal solution in the base solution. The petal solution was prepared by leaching at room temperature for 24 hours, and the base solution was prepared separately at room temperature, and then mixed with the petal solution and mixed with a homo mixer.

실시예Example 3 내지 5 및  3 to 5 and 비교예Comparative example 5 내지 8 5 to 8

실시예 3 내지 5 및 비교예 5 내지 8에 따라 만든 후, 화장료의 투명도, 보습력, 사용감 및 꽃잎에 의한 마사지감 등을 비교하였다. 투명도는 베이스가 투명하여 꽃잎이 잘 보이는가를 기준으로 판단하였으며, 보습력은 각질층의 수분보유량을 측정하여 평가하였다. 이때 측정기기는 스키콘(Skicon) 200을 사용하였고, 시험은 25℃, 상대습도 50%의 항온 항습실에서 실시하여 사용전의 수분보유량과 사용 후 2시간 후의 수분보유량을 수학식 1에 따라 수분보유율을 산출하였으며, 수치가 클수록 보습력이 우수함을 의미한다.After making according to Examples 3 to 5 and Comparative Examples 5 to 8, the transparency, moisturizing power, feeling of use and massage feeling by the petals and the like were compared. Transparency was judged based on whether the base was transparent and the petals were seen well. Moisturizing power was evaluated by measuring the moisture content of the stratum corneum. At this time, the measuring device was used skicon (Skicon) 200, the test was carried out in a constant temperature and humidity room of 25 ℃, relative humidity 50% to determine the water retention before use and the water retention after 2 hours after use according to equation (1). The higher the value, the better the moisturizing power.

Figure 112007009761891-PAT00001
Figure 112007009761891-PAT00001

또한, 사용감은 20명의 소비자로 하여금 5점 척도로 마사지감, 밀착감, 부드러움 등을 종합평가하여 얻었으며, 5점에 가까울수록 좋음을 의미한다.In addition, the feeling of use was obtained by a comprehensive evaluation of massage feeling, fit, and softness by 20 consumers on a five-point scale, the closer to five points means better.

꽃잎의 연화는 피부에 문지를시 꽃잎이 얼마나 잘 뭉게져 부드럽게 발리나를 5점 척도로 평가한 것이다.The softening of the petals is a measure of how well the petals clump when rubbed on the skin, and gently evaluates Ballina on a 5-point scale.

실시예 3Example 3 실시예 4Example 4 실시예 5Example 5 비교예 5Comparative Example 5 비교예 6Comparative Example 6 비교예 7Comparative Example 7 비교예 8Comparative Example 8 가)꽃잎용액A) petal solution 정제수Purified water 55 55 33 55 55 33 55 에탄올ethanol 55 33 33 55 55 33 55 글리세린glycerin -- 33 -- -- 55 -- 건조장미꽃잎Dried rose petals 1One -- 0.50.5 1One 1One 0.50.5 1One 건조마리골드꽃잎Dried Marigold Petals -- 0.50.5 -- -- -- -- 나) 베이스용액B) Base solution 카보머Carbomer 0.50.5 -- 0.30.3 -- -- 0.30.3 0.50.5 소듐 카보머Sodium carbomer -- 0.30.3 -- -- -- -- -- 글리세릴아크릴레이트/ 아크릴릭애씨드코폴리머Glyceryl Acrylate / Acrylic Acid Copolymer -- 0.50.5 0.30.3 -- 0.50.5 0.30.3 -- 아크릴레이트/C10-30 알킬 아크릴레이트 코폴리머Acrylate / C10-30 Alkyl Acrylate Copolymer -- -- -- 0.50.5 0.30.3 -- -- 글리세린glycerin 1515 1010 1010 1515 1010 -- 1515 부틸렌글리콜Butylene glycol 1010 1010 1010 1010 1010 -- 1010 수첨케스터오일Hydrogenated Castor Oil 0.20.2 0.20.2 0.20.2 0.20.2 0.20.2 0.20.2 0.20.2 트리에탄올아민Triethanolamine 0.50.5 -- 0.20.2 0.50.5 0.50.5 0.30.3 0.50.5 향료Spices 적량Quantity 적량Quantity 적량Quantity 적량Quantity 적량Quantity 적량Quantity 적량Quantity 에탄올ethanol -- -- -- -- -- -- 55 정제수Purified water To 100To 100 To 100To 100 To 100To 100 To 100To 100 To 100To 100 To 100To 100 To 100To 100 다. 제조방법All. Manufacturing method 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)를 나)에 모두 넣고 제조A) Put it all in b) 가)에서 꽃잎만을 분리하여 나)에 넣고제조Separate only petals from a) and put them in b)

실시예 3Example 3 실시예 4Example 4 실시예 5Example 5 비교예 5Comparative Example 5 비교예 6Comparative Example 6 비교예 7Comparative Example 7 비교예 8Comparative Example 8 투명도transparency 투명Transparency 투명Transparency 불투명opacity 불투명opacity 불투명opacity 투명Transparency 투명Transparency 수분증가율Moisture growth rate 5555 5050 5252 5050 4545 1616 3838 사용감Feeling 4.24.2 4.04.0 4.04.0 3.83.8 3.53.5 3.03.0 3.63.6 꽃잎연화Petal softening 3.83.8 3.73.7 4.04.0 3.33.3 3.23.2 3.03.0 3.53.5

실시예 3 내지 5 및 비교예 5 내지 8에 따르면, 꽃잎 및 사용된 용매, 용출된 미용성분을 모두 포함시킬 경우, 용매 및 용출된 미용성분을 제거한 것과 비교하여 수분증가율, 사용감, 꽃잎연화에서 우수하였으며, 알킬기를 포함하지 않는 폴리아크릴산 및 그 염을 포함하였을 경우, 투명도가 우수하여 심미적으로 미려하였다. 또한, 폴리올을 다량 함유시킬 경우, 사용감 및 보습력이 우수하였다.According to Examples 3 to 5 and Comparative Examples 5 to 8, when both the petal and the solvent used and the eluted cosmetic ingredients are included, the moisture increase rate, feeling, and softening of the petals are superior to those of removing the solvent and the eluted cosmetic ingredients. When polyacrylic acid and salts thereof do not include an alkyl group, the transparency was excellent and the aesthetic beauty. Moreover, when a large amount of polyol was contained, the usability and moisture retention power were excellent.

본 발명에 따른 꽃잎이 함유된 화장료 조성물은, 꽃잎에 함유되어 있는 여러 가지 미용성분 및 꽃잎을 그대로 화장료에 포함시키고 적절한 폴리아크릴산계 고분자와 폴리올을 함유시킴으로써, 함유된 꽃잎 및 그로부터 용출된 미용성분으로 인한 피부효과를 기대할 수 있으며, 꽃잎의 모양을 미려한 상태로 보존시킴으로써 시각적인 만족감을 얻을 수 있으며, 우수한 사용감을 얻을 수 있다.Cosmetic composition containing petals according to the present invention, by including the various cosmetic ingredients and petals contained in the cosmetics in the cosmetics as it is, and containing the appropriate polyacrylic acid-based polymer and polyol, as the contained petals and the cosmetic components eluted therefrom Due to the skin effect can be expected, by visually preserving the shape of the petals can obtain a visual satisfaction, and excellent usability can be obtained.

Claims (6)

연화 탈색된 꽃잎 및 이로 부터 용출된 성분, 연화 탈색을 위한 용매, 폴리아크릴산계고분자, 폴리올을 포함하는 꽃잎이 함유된 화장료 조성물.A cosmetic composition comprising a petal comprising softened and decolorized petals and components eluted therefrom, a solvent for softening and decolorizing, a polyacrylic acid-based polymer, and a polyol. 제1항에 있어서, 연화 탈색을 위한 용매는 에탄올과 물의 비율이 1:2 내지 2:1인 용액이며, 조성물 전체중량 대비 1 내지 30 중량% 함유하는 것을 특징으로 하는 꽃잎이 함유된 화장료 조성물.The method of claim 1, wherein the solvent for softening bleaching is a solution of 1: 2 to 2: 1 ratio of ethanol and water, the cosmetic composition containing petals, characterized in that containing 1 to 30% by weight based on the total weight of the composition. 제1항에 있어서, 연화 탈색된 꽃잎은 장미, 국화, 마리골드 중에서 선택되는 꽃잎이며, 조성물 전체중량 대비 0.1 내지 5 중량 % 함유하는 것을 특징으로 하는 꽃잎이 함유된 화장료 조성물.The cosmetic composition of claim 1, wherein the softened and decolorized petals are petals selected from roses, chrysanthemums, marigolds, and contain 0.1 to 5% by weight based on the total weight of the composition. 제1항에 있어서, 폴리아크릴산계 고분자는 카보머, 글리세릴 아크릴레이트/아크릴릭애씨드 코폴리머, 폴리아크릴릭에씨드 및 그들의 염으로부터 선택되며, 조성물 전체중량 대비 0.1 내지 3 중량% 함유하는 것을 특징으로 하는 꽃잎이 함유된 화장료 조성물.The method of claim 1, wherein the polyacrylic acid polymer is selected from carbomer, glyceryl acrylate / acrylic acid copolymer, polyacrylic acid and salts thereof, characterized in that it contains 0.1 to 3% by weight relative to the total weight of the composition. Cosmetic composition containing petals. 제1항에 있어서, 폴리올은 글리세린, 솔비톨, 폴리에틸렌글리콜, 프로필렌글리콜, 디프로필렌글리콜, 부틸렌글리콜 중에서 선택되며, 조성물 전체중량 대비 5 내지 50 중량% 함유하는 것을 특징으로 하는 꽃잎이 함유된 화장료 조성물.The cosmetic composition according to claim 1, wherein the polyol is selected from glycerin, sorbitol, polyethylene glycol, propylene glycol, dipropylene glycol, butylene glycol, and contains 5 to 50 wt% of the total weight of the composition. . 에탄올과 물의 비율이 1:2 내지 2:1의 용액에 건조 꽃잎을 담가 12 시간 내지 48 시간 동안 상온에서 침출 시킨, 꽃잎을 포함한 용액을 베이스 용액과 혼합하는 것을 특징으로 하는 꽃잎이 함유된 화장료 조성물의 제조방법.Cosmetic composition containing a petal, characterized in that the mixture of ethanol and water is mixed with the base solution, the solution containing the petals, immersed dry petals in a solution of 1: 2 to 2: 1 and leached at room temperature for 12 to 48 hours Manufacturing method.
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WO2015163528A1 (en) * 2013-06-07 2015-10-29 충북대학교 산학협력단 Cosmetic composition for skin whitening and wrinkle alleviation, containing, as active ingredients, white rose extract and gartanin derivative compound isolated therefrom
US10842727B2 (en) 2013-06-07 2020-11-24 Gangneung-Wongju National University Industry Academy Cooperation Group Cosmetic composition comprising white rose flower extract for skin whitening and improving skin wrinkle
WO2019107866A1 (en) * 2017-11-30 2019-06-06 주식회사 라피끄 Cosmetic comprising softened natural plant body and method for producing same
WO2019107865A1 (en) * 2017-11-30 2019-06-06 주식회사 라피끄 Method for producing cosmetic composition comprising natural plant, and cosmetic composition produced thereby
CN110582267A (en) * 2017-11-30 2019-12-17 拉菲克化妆品株式会社 Method for preparing cosmetic composition containing natural plant and cosmetic composition prepared by the same
KR20200085068A (en) * 2019-01-04 2020-07-14 (주)이미인 Oil-in-water type cosmetic composition comprising petal
CN109820783A (en) * 2019-03-22 2019-05-31 云南省农业科学院花卉研究所 A kind of discoloration method of plant petals
KR102320428B1 (en) * 2021-04-08 2021-11-04 (주)나우코스 Moisture-enhancing transparent cosmetic composition not having surfactant and oil
CN114392220A (en) * 2022-02-10 2022-04-26 银谷芳香科技有限公司 Production process of colorless Damascus rose dry petals
CN114392220B (en) * 2022-02-10 2024-02-13 银谷芳香科技有限公司 Production process of colorless dried rosa damascena petals

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