CN110755278A

CN110755278A - Facial mask and preparation method thereof

Info

Publication number: CN110755278A
Application number: CN201910902736.0A
Authority: CN
Inventors: 向文韬
Original assignee: Individual
Current assignee: Individual
Priority date: 2019-09-24
Filing date: 2019-09-24
Publication date: 2020-02-07

Abstract

The invention relates to the technical field of skin care products, and particularly discloses a facial mask and a preparation method thereof. The facial mask comprises the following components in percentage by weight: 87.06% -89.06% of water, 2% -4% of prunus humilis extractive solution, 3% of glycerol, 3% of 1, 3-butanediol, 0.99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.5% of AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol, 0.1% of chlorphenesin, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed sclerotium rolfsii gum, 0.08% of MP methyl ester, 0.02% of glycyrrhiza glabra root extract, and 0.02% of HA-T sodium hyaluronate. The facial mask disclosed by the invention takes the prunus salicina extract as an active ingredient, can be used for astringing and softening the skin, has the performances of moisturizing, diminishing inflammation and bleaching, has the effects of removing sclerosis and keratinization and improving scars, can be used for preventing small wrinkles, eye bags and skin looseness, and can be used for keeping the skin moist and delicate.

Description

Facial mask and preparation method thereof

Technical Field

The invention relates to the technical field of skin care products, and particularly relates to a facial mask and a preparation method thereof.

Background

The mask is a category of skin care products, and the most important purpose of the mask is to make up for the cleaning work of makeup removal and face washing, and realize other maintenance functions such as moisturizing, whitening, anti-aging, grease balancing and the like by matching with other essential ingredients on the basis. The principle of the facial mask is that the facial mask is covered on the face for a short time, so that outside air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, sweat gland secretion and metabolism are promoted, the oxygen content of the skin is increased, products of epidermal cell metabolism and accumulated grease substances are favorably removed from the skin, water in the facial mask permeates into the horny layer of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic.

Most of the existing facial masks adopt chemicals as active ingredients, and after long-term use, the effect is gradually deteriorated, even the skin is damaged. Therefore, it is very necessary to design a mask mainly containing plant nutrients to solve the above technical problems.

Disclosure of Invention

The invention aims to overcome the defects in the prior art and provides a facial mask and a preparation method thereof. The facial mask takes effective components extracted from the prunus salicina as main active components, and can avoid the defects that the traditional facial mask is poor in long-term use effect and easy to generate side effects on a human body.

The purpose of the invention is realized by the following technical scheme: the facial mask comprises the following components in percentage by weight: 87.06% -89.06% of water, 2% -4% of prunus salicina extract, 3% of glycerol, 3% of 1, 3-butanediol, 0, 99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.5% of AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol, 0.1% of chlorphenesin, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed micronucleus (SCLEOTIUMROLFSSI) gum, 0.08% of MP methyl ester, 0.02% of Glycyrrhiza glabra (GLYCYRRHIZAZAGLABRA) root extract, and 0.02% of HA-T sodium hyaluronate.

Preferably, the facial mask comprises the following components in percentage by weight: 89.06% water, 2% plum extract, 3% glycerin, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMROLFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhiza glabra) root extract, and 0.02% HA-T sodium hyaluronate.

Preferably, the facial mask comprises the following components in percentage by weight: 88.06% water, 3% prune extract, 3% glycerin, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMRFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhizza) root extract, and 0.02% HA-T sodium hyaluronate.

Preferably, the facial mask comprises the following components in percentage by weight: 87.06% water, 4% Prunus salicina extract, 3% glycerol, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMRFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhizza) root extract, and 0.02% HA-T sodium hyaluronate.

The crisp plum extract is prepared by the following method:

(1) selecting fruits: selecting fresh, full and juicy plums (Prunus salicina Lindl), and removing immature fruits, silt and other impurities;

(2) cleaning: washing the selected crisp plums in the step (1) with deionized water;

(3) removing kernels: cutting the cleaned crisp plums in the step (2) with a disinfected knife to remove kernels, and taking the crisp plum pulp for later use;

(4) extraction: and (4) putting the crispy plum pulp obtained in the step (3) into a centrifugal crusher to be crushed, and filtering to obtain an crispy plum extracting solution.

The pulverization condition in the step (4) is that pulverization is carried out for 10 minutes at 26000 revolutions per minute.

The preparation method of the facial mask comprises the following steps:

(1) heating 87.06% -89.06% of water to 80 ℃ for disinfection, adding 3% of 1, 3-butanediol and 0.02% of HA-T sodium hyaluronate into the disinfected water to obtain a mixed solution; homogenizing and dispersing the mixed solution at 150 revolutions per minute until the mixed solution is dissolved to obtain a material A;

(2) adding 2-4% of plum extract, 3% of glycerol, 0.99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed sclerotium rolfsii (SCLEOTIUMROLFSII) gum, 0.08% of MP methyl ester and 0.02% of Glycyrrhiza glabra (GLYCYRRHIZAGLABRA) root extract into the material A in the step (1), homogenizing and emulsifying for 5 minutes at 60 r/min, heating to 90 ℃, keeping the temperature for 25 minutes, cooling to 40 ℃, adding 0.5% of AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol and 0.1% of chlorphenesin, and stirring for 20 minutes at 40 r/min until the mixture is uniform to obtain a mask; the percentages are weight percentages.

Preferably, in the step (1),

the homogeneous dispersion is carried out in a homogenizing emulsifying machine;

the time for sterilization is 30 minutes.

Preferably, the homogenizing and emulsifying in the step (2) and the stirring are preferably performed in a homogenizing and emulsifying machine.

Compared with the prior art, the invention has the following advantages and effects: the facial mask disclosed by the invention takes the prunus salicina extract as an effective component, the prunus salicina extract contains rich components such as fruit acid, sugar, trace protein, carotene, vitamins, calcium, phosphorus, iron, asparagine, glutamine, serine, glycine, proline, threonine and alanine, and the like, so that the mask can be used for astringing and softening the skin, has the performances of moisturizing, diminishing inflammation and bleaching, has the effects of removing hardening, keratinization and improving scars, can be used for preventing small wrinkles, eye bags and skin looseness, and can be used for keeping the skin moist and delicate.

Detailed Description

The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.

Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs. The terminology used herein in the description is for the purpose of describing particular embodiments only and is not intended to be limiting of the application.

Furthermore, the terms "first," "second," "third," and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicit to a number of indicated technical features. Thus, a feature defined as "first," "second," etc. may explicitly or implicitly include at least one of the feature. In the description of the present application, "plurality" means at least two, e.g., two, three, etc., unless specifically limited otherwise.

In this application, all materials are commercially available unless otherwise specified. As used herein, unless otherwise indicated, "percent" or "%" refers to weight percent of all components.

In this application, the word "about" or "approximately" means within an acceptable range for the specified particular parameter as determined by one of ordinary skill in the art, which will depend in part on the manner in which the value is measured or determined, i.e., the limits of the measurement system. For example, "about" may refer to a range of up to 10% of a given value.

The invention completely meets all indexes in technical specifications for cosmetic safety (2015 edition) issued by the state and does not contain any potential hazard.

The facial mask disclosed by the invention comprises the following components in percentage by weight: 87.06% -89.06% of water, 2% -4% (if less than 2% the whitening effect is insufficient, if more than 4% the pH value is low, the solution is strong in acidity) of the extract of prunus salicina, 3% of glycerin, 3% of 1, 3-butylene glycol, 0.99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.5% of AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol, 0.1% of chlorphenesin, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed micronucleus (SCLEOTIUMROLFSSII) gum, 0.08% of MP methyl ester, 0.02% of extract of the root of Glycyrrhiza glabra (GLYCYRRHIZAGLABRA), and 0.02% of HA-T sodium hyaluronate.

The crisp plum extract of the embodiment of the invention is prepared by the following method:

(4) extraction: and (4) putting the prunus salicina fruit pulp obtained in the step (3) into a centrifugal grinder to be ground (the rotating speed is 26000 r/m, the time is 10 minutes), and filtering to obtain the prunus salicina extract.

Example 1

The facial mask comprises the following components in percentage by weight: 89.06% water, 2% plum extract, 3% glycerin, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMROLFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhiza glabra) root extract, and 0.02% HA-T sodium hyaluronate.

The preparation method of the facial mask comprises the following steps:

(1) heating water to 80 ℃ for disinfection (keeping the temperature for 30 minutes for disinfection), and adding 1, 3-butanediol and HA-T sodium hyaluronate into the disinfected water to obtain a mixed solution; homogenizing and dispersing the mixed solution at 150 r/min (in a homogenizing and emulsifying machine) until the mixed solution is dissolved to obtain a material A;

(2) adding the crisp plum extract, glycerol, EG-1 glyceryl polyether-26, trehalose, transparent xanthan gum, dipotassium glycyrrhizinate, HG hydrolyzed sclerotium rolfsii (SCLEOTIUMROLFSSI) gum, MP methyl ester and Glycyrrhiza glabra (GLYCYRRHIZAGLABRA) root extract into the material A in the step (1), homogenizing and emulsifying (in a homogenizing and emulsifying machine) for 5 minutes at 60 revolutions per minute, heating to 90 ℃, keeping the temperature for 25 minutes, cooling to 40 ℃, adding AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol and 0.1% of chlorphenesin, and stirring (in a homogenizing and emulsifying machine) at 40 revolutions per minute for 20 minutes to be uniform to obtain a mask essence; the percentages are weight percentages.

Example 2

The facial mask comprises the following components in percentage by weight: 88.06% water, 3% prune extract, 3% glycerin, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMRFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhizza) root extract, and 0.02% HA-T sodium hyaluronate.

The preparation method of the facial mask comprises the following steps:

(1) heating water to 80 ℃ (keeping the temperature for 30 minutes for disinfection), and adding 1, 3-butanediol and HA-T sodium hyaluronate into the disinfected water to obtain a mixed solution; homogenizing and dispersing the mixed solution at 150 r/min (in a homogenizing and emulsifying machine) until the mixed solution is dissolved to obtain a material A;

Example 3

The facial mask comprises the following components in percentage by weight: 87.06% water, 4% Prunus salicina extract, 3% glycerol, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed micronucleus (SCLEOTIUMRFSSII) gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra (Glycyrrhizza) root extract, and 0.02% HA-T sodium hyaluronate.

The preparation method of the facial mask comprises the following steps:

Effects of the embodiment

1. According to the comparative test, referring to the evaluation guideline for cosmetic moisturizing efficacy (QB/T4256-2011), after the facial mask is used by a volunteer in a constant-temperature and constant-humidity environment for a single time, the moisturizing effect of the facial mask within 6 hours is evaluated in a non-invasive manner by using an instrument. During the test, the test face masks and the blank control were randomly distributed on the inner sides of the left and right forearm of the subject. The product is used for a single time, and the application time is 20 minutes. The stratum corneum moisture content was measured using a skin moisture tester (Corneometer) on the product application zone and the placebo zone before and after 0.5, 1,2, 4, and 6 hours of product application, respectively. Each face film sample had 24 ginseng samples and the test was completed.

The short-term moisturizing effect after the use is obviously different. Four (one commercially available mask, mask from examples 1-3) samples all showed an increase in skin moisture when tested in the second half hour of use. However, the difference in moisturizing effect between the four samples was significant. (group A is a commercial mask, group B is the mask of example 1, group C is the mask of example 2, and group D is the mask of example 3). The detailed results are shown in table 1.

Table 1 moisturizing effect test results of commercially available masks and masks of examples 1 to 3

From the above results, it can be seen that the increase in skin moisture content gradually decreased with time after application, and that the skin moisture increase values of samples A, B, C, and D were more than 10 units when tested 0.5 hours after application of the face mask; after 2 hours after use, the skin moisture content increase value of samples A, B, C and D is more than 10 units; after 6 hours, only C, D samples had an increase in skin moisture content of greater than 10 units.

2. In the comparative test, the PH value of the facial mask of the embodiment 1-3 is tested and the heat and cold resistance is tested for 48 hours by referring to QB/T2872-2017. The results are shown in Table 2. As can be seen from table 2, the mask pack of example 3 had the best stability, that is, the mask pack containing 4% of the prune extract had the best stability.

Table 2 results of the effect test of the masks of examples 1 to 3

The mask prepared by the healthy and harmless prunus salicina extractive solution has no side effect on a human body, and has more remarkable whitening and skin-care effects.

The invention tries to prepare the crisp plum extract into the facial mask for the first time, wherein the crisp plum extract contains sugar, trace protein, carotene, vitamin, calcium, phosphorus, iron, asparagines, glutamine, serine, glycine, proline, threonine, alanine and other components. Has astringent, softening, moisturizing, antiinflammatory, and bleaching effects. It also has effects in relieving sclerosis and keratinization, improving scar, preventing wrinkle, pouch and cutis laxa, and keeping skin moist and tender.

The facial mask disclosed by the invention takes the prunus salicina extract as an effective component, the prunus salicina extract contains rich components such as fruit acid, sugar, trace protein, carotene, vitamins, calcium, phosphorus, iron, asparagine, glutamine, serine, glycine, proline, threonine and alanine, and the like, so that the mask can be used for astringing and softening the skin, has the performances of moisturizing, diminishing inflammation and bleaching, has the effects of removing hardening, keratinization and improving scars, can be used for preventing small wrinkles, eye bags and skin looseness, and can be used for keeping the skin moist and delicate.

The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims

1. The facial mask is characterized by comprising the following components in percentage by weight: 87.06% -89.06% of water, 2% -4% of prunus humilis extractive solution, 3% of glycerol, 3% of 1, 3-butanediol, 0.99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.5% of AJIDEWNL-50, 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol, 0.1% of chlorphenesin, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed sclerotium rolfsii gum, 0.08% of MP methyl ester, 0.02% of glycyrrhiza glabra root extract, and 0.02% of HA-T sodium hyaluronate.

2. The mask pack according to claim 1, wherein the mask pack comprises the following components in percentage by weight: 89.06% water, 2% plum extract, 3% glycerin, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed sclerotium rolfsii gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra root extract, and 0.02% HA-T sodium hyaluronate.

3. The mask pack according to claim 1, wherein the mask pack comprises the following components in percentage by weight: 88.06% water, 3% prune extract, 3% glycerol, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed sclerotium rolfsii gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra root extract, and 0.02% HA-T sodium hyaluronate.

4. The mask pack according to claim 1, wherein the mask pack comprises the following components in percentage by weight: 87.06% water, 4% prune extract, 3% glycerol, 3% 1, 3-butylene glycol, 0.99% EG-1 glyceryl polyether-26, 0.5% trehalose, 0.5% AJIDEWNL-50, 0.15% 1, 2-hexanediol, 0.15% phenoxyethanol, 0.1% chlorphenesin, 0.25% transparent xanthan gum, 0.09% dipotassium glycyrrhizinate, 0.09% HG hydrolyzed sclerotium rolfsii gum, 0.08% MP methyl ester, 0.02% Glycyrrhiza glabra root extract, and 0.02% HA-T sodium hyaluronate.

5. The mask pack according to any one of claims 1 to 4, wherein the extract of prunus salicina is prepared by the following method:

(1) selecting fruits: selecting fresh, full and juicy crispy plums, and removing immature fruits, silt and other impurities;

6. The mask according to claim 5, wherein the pulverization in the step (4) is carried out under a condition of pulverization at 26000 rpm for 10 minutes.

7. A method for preparing the mask pack according to any one of claims 1 to 4, comprising the steps of:

(2) adding 2% -4% of plum extract, 3% of glycerol, 0.99% of EG-1 glyceryl polyether-26, 0.5% of trehalose, 0.25% of transparent xanthan gum, 0.09% of dipotassium glycyrrhizinate, 0.09% of HG hydrolyzed sclerotium rolfsii gum, 0.08% of MP methyl ester and 0.02% of glycyrrhiza glabra root extract into the material A in the step (1), homogenizing and emulsifying for 5 minutes at 60 revolutions per minute, heating to 90 ℃, keeping the temperature for 25 minutes, cooling to 40 ℃, adding 0.5% of AJIDEWNL-50 and 0.15% of 1, 2-hexanediol, 0.15% of phenoxyethanol and 0.1% of chlorphenesin, and then stirring for 20 minutes at 40 revolutions per minute until the mixture is uniform to obtain the mask; the percentages are weight percentages.

8. The method for preparing a facial mask according to claim 7, wherein the homogeneous dispersion in the step (1) is performed in a homogenizing and emulsifying machine; the time for sterilization is 30 minutes.

9. The method for preparing a facial mask pack according to claim 7, wherein the homogenizing emulsification in the step (2) and the stirring are performed in a homogenizing emulsifier.