CN107468576A - A kind of composition containing burdock extract and its application in cosmetics - Google Patents

A kind of composition containing burdock extract and its application in cosmetics Download PDF

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Publication number
CN107468576A
CN107468576A CN201710763382.7A CN201710763382A CN107468576A CN 107468576 A CN107468576 A CN 107468576A CN 201710763382 A CN201710763382 A CN 201710763382A CN 107468576 A CN107468576 A CN 107468576A
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extract
burdock
burdock extract
composition
composition containing
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章苏宁
姜姗姗
朱玉英
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Shanghai Institute of Technology
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Shanghai Institute of Technology
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/005—Preparations for sensitive skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82—Preparation or application process involves sonication or ultrasonication
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of composition containing burdock extract, it is made up of burdock extract and chrysanthemum potato extract, the mass ratio of described burdock extract and chrysanthemum potato extract is 1：1.Present invention also offers a kind of application of the above-mentioned composition containing burdock extract in cosmetics.Weight of the burdock extract in cosmetics is than being 1% 10% for 1% 10%, weight ratio of the chrysanthemum potato extract in cosmetics.The composition of the present invention has the cooperative effect such as releive, repair, and its application in cosmetics is mainly applied in the skin-protection products such as face cream, elite breast, the skin of gained apply some make up it is simple with preparation technology, it is feasible, it is naturally safe the characteristics of.

Description

A kind of composition containing burdock extract and its application in cosmetics
Technical field
The invention belongs to chemical field, is related to a kind of cosmetics, specifically a kind of composition containing burdock extract and Its application in cosmetics.
Background technology
Burdock, be the biennial rhizome vegetable of composite family, containing various active material, including water-soluble dietary fiber, Synanthrin, carotenoid, burdock oligosaccharide, burdock seed oil, chlorogenic acid etc..Contain a large amount of flavones ingredients, this composition tool in burdock There is anti-oxidation function, research shows, flavone compound can terminate free radical chain reactionses chain, so as to reach anti-oxidant effect Fruit.Wherein lignan component also has certain anti-oxidation efficacy, and it can protect the damage of free radical, and it can mainly press down It the formation of superoxide anion processed and hydroxy radical, can also increase internal antioxidase, so as to reach antioxidant effect.Ox Burdock whole plant contains antimicrobial component.Its chlorogenic acid contained can suppress Escherichia coli, staphylococcus aureus, bacillus and Micrococcus luteus；Polyacetylene material in radix bardanae has more preferable antibacterial action.
Chrysanthemum potato (Smallanthus sonchifolius), also known as ten thousand sweet potatos, it is a kind of composite family herbaceos perennial.It is rich Containing protein, amino acid, and the glucide such as FOS, glucose, sucrose and fructose, its main Leaf-feeding insects of chrysanthemum potato It is pure natural green health care food for root tuber, not only with refrigerant annealing, clearing heat and detoxicating, the whole intestines of stomach invigorating, the guarantor for softening blood vessel Strong effect, also with eliminating the phlegm, antibacterial promoting blood circulation, hypotensive activity effect.
Burdock and chrysanthemum potato all have certain medical value and health-care effect, but at present for burdock and chrysanthemum potato in cosmetics In application be also rarely reported, particularly both compositions to skin releive and repair is there is not yet relevant report.
The content of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of composition containing burdock extract and its Application in cosmetics, described this composition containing burdock extract and its application in cosmetics will solve prior art The technical problem that middle burdock and chrysanthemum potato are not effectively applied in cosmetics.
The invention provides a kind of composition containing burdock extract, it is made up of burdock extract and chrysanthemum potato extract, it is described Burdock extract and chrysanthemum potato extract mass ratio be 1：1；
Described burdock extract is prepared via a method which to form：
(1) burdock is cleaned up；
(2) burdock cleaned up in step (1) is subjected to pulverization process with pulverizer；
(3) by the burdock crushed as 40 DEG C of baking oven freeze-day with constant temperature to constant weight；
(4) ethanol water that mass percent concentration is 40% will be added in burdock powder dried in step (3) Carry out immersion treatment；
(5) it is 40 DEG C, power 150W the mixed solution obtained by step (4) to be controlled into temperature, and frequency is the super of 40KHz Ultrasonic 30min under the conditions of sound, filtration treatment then is carried out with 0.45 μm of membrane filtration of micropore 3, and collect gained filtrate；
(6) filtrate obtained by step (5) is controlled and carries out vacuum rotation under conditions of vacuum is 0.094-0.096MPa Turn evaporation, obtain burdock extract concentrate, control temperature to be freeze-dried for -55 DEG C, produce burdock extract；
Described chrysanthemum potato extract is prepared via a method which to form：
(1) chrysanthemum potato is cleaned up；
(2) the chrysanthemum potato cleaned up in step (1) is subjected to pulverization process with pulverizer；
(3) by the chrysanthemum potato crushed as 40 DEG C of baking oven freeze-day with constant temperature to constant weight；
(4) ethanol water that mass percent concentration is 50% will be added in chrysanthemum potato powder dried in step (3) Carry out immersion treatment；
(5) it is 50 DEG C, power 150W the mixed solution obtained by step (4) to be controlled into temperature, and frequency is the super of 40KHz Ultrasonic 20min under the conditions of sound, filtration treatment then is carried out with 0.45 μm of miillpore filter, and collect gained filtrate；
(6) filtrate obtained by step (5) is controlled and carries out vacuum rotation under conditions of vacuum is 0.094-0.096MPa Turn evaporation, obtain chrysanthemum potato extract concentrated solution, control temperature to be freeze-dried for -55 DEG C, produce chrysanthemum potato extract.
Present invention also offers a kind of application of the above-mentioned composition containing burdock extract in cosmetics.
Further, above-mentioned application, apply in face cream or toner.
Further, above-mentioned application, weight ratio of the burdock extract in cosmetics are 1%-10%, chrysanthemum potato extract Weight ratio in cosmetics is 1%-10%.
Present invention also offers a kind of face cream of above-mentioned composition containing burdock extract, calculate by mass percentage, The content and composition of its raw material are as follows：
The 2%-20% of composition containing burdock extract
Mineral grease 1-5%
Synthetic Oil 1-4%
Vegetable fat 1-5%
Animal fat 0-2%
Emulsifying agent 2-6%
NMF 2-10%
Preservative 0.05-0.2%
Antioxidant 0.01-0.1%
Surplus is deionized water；
Described mineral grease is the mixture that stearic acid and white oil form, and is calculated in mass ratio, i.e. stearic acid：White oil is 4：1；
Described Synthetic Oil is the mixing of isobutyl palmitate, glycerin monostearate and dimethyl siloxane composition Thing, calculate in mass ratio, i.e. isobutyl palmitate：Glycerin monostearate is：Dimethyl siloxane 6：1：2；
Described vegetable fat is the mixture that Sweet Almond Oil and olive oil form, and is calculated in mass ratio, i.e. Sweet Almond Oil： Olive oil is 1：2；
Described emulsifying agent is the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21), match Bick 305 emulsify The mixture of agent composition, is calculated, i.e. polyoxyethylene (2) stearic alcohol ether in mass ratio：Polyoxyethylene (21) stearic alcohol ether：Match Bick 305 emulsifying agents are 2：3：3；
Described NMF is the mixture that glycerine and butanediol form, and is calculated in mass ratio, i.e. glycerine：Butanediol is 1: 3；
Described preservative is the mixture that methyl hydroxybenzoate and propylben form, and is calculated in mass ratio, i.e. Ni Bo Tortoise beetle ester：Propylben is 2：1；
Described antioxidant is 2,6- di-tert-butyl hydroxy toluenes.
Present invention also offers a kind of preparation method of above-mentioned face cream containing the composition containing burdock extract, including Following steps：
(1) by the oil phase 1 of mineral grease, Synthetic Oil, match Bick 305 emulsifying agent composition, to be heated to 65-90 DEG C of stirring molten Solution is used as A1 phases；
(2) vegetable fat, the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21), antioxidant are formed Oil phase 2 is heated to 65-90 DEG C of stirring and dissolving as A2 phases；
(3) composition containing burdock extract is dissolved in 5~30% deionized water and is heated to 50-70 DEG C of insulation Aqueous phase 1 be used as B1 phases；
(4) NMF is dissolved in balance deionized water, and heating stirring is completely dispersed the uniform conduct of aqueous phase 2 to 65-90 DEG C B2 phases；
(5) temperature is controlled to be mixed and stirred for the A1 phases obtained by step (1) and step (2) with A2 phases at 70-85 DEG C Uniformly, total oil phase is made as A phases；
(6) controlling temperature, mixer mixing speed is 500-700rpm/min, by step (4) and step at 70-85 DEG C (5) the B2 phases obtained by with A phases be mixed and stirred for uniformly；
(7) it is 500-700rpm/min, to control mixer mixing speed, and the mixture obtained by step (6) is cooled to 50-70 DEG C, then mixed with the B1 obtained by step (3)；
(8) under the conditions of controlling homogenizer rotating speed to be 10000-20000rpm/min, by the mixing obtained by step (7) Thing thing is uniformly dispersed；
(9) after step (8) is well mixed, when being naturally cooling to 45 DEG C, preservative is added, continues mechanical agitation to mixing Uniformly, speed of agitator 100-500rpm/min；And stop stirring after naturally cooling to room temperature, discharging, produce a kind of contain The face cream of burdock extract composition.
Present invention also offers a kind of above-mentioned toner containing the composition containing burdock extract, by quality hundred Divide than calculating, the content and composition of its raw material are as follows：
The 2%-20% of composition containing burdock extract
Solubilizer 0.5-2%
Rheology control agent 0.05-0.5%
Preservative 0.05-0.2%
Essence 0.01-0.05%
Surplus is deionized water；
Described solubilizer is rilanit special；
Described rheology control agent is hydroxyethyl cellulose；
Described preservative is the mixture of hydroxyphenyl methyl esters and hydroxyphenyl propyl ester composition, is calculated in mass ratio, i.e. oxybenzene Base methyl esters：Hydroxyphenyl propyl ester is 2：1.
Present invention also offers a kind of preparation method of the toner of above-mentioned described composition containing burdock extract, bag Include following steps：
(1) deionized water is added in a container, starts agitator, rheology control agent is slowly poured into described container In, rheology control agent add finish continue stir 15-20min it is standby；
(2) essence, solubilizer and preservative Hybrid Heating are heated to 45 DEG C as oil phase and obtain oil phase；
(3) will be added to containing composition containing burdock extract in the deionized water of step (1) uniform as Aqueous dispersions It is heated to 50 DEG C and obtains aqueous phase；
(4) aqueous phase obtained by step (3) is cooled to 45 DEG C, then the oil phase obtained by step (2) is added to step (3) institute In the aqueous phase obtained, while mixer is opened, it is 300-500rpm/min to control mixing speed, carries out scattered 10min, mechanical agitation Stop stirring to being well mixed and naturally cooling to after room temperature, discharging, produce a kind of refreshing containing the composition containing burdock extract Skin water.
The present invention one kind composition containing burdock extract, releive and repair functional component as sensitive skin, its Application in cosmetics is mainly applied in the skin-protection products such as face cream, elite breast, and contains burdock extract using above-mentioned The skin of composition apply some make up it is simple with preparation technology, it is feasible, it is natural safe the characteristics of, suitable for industrialized production.
Brief description of the drawings
Fig. 1 is the left and right arm ferroheme numerical value of different time.
Embodiment
The present invention is expanded on further by way of example and in conjunction with the accompanying drawings, but is not intended to limit the present invention.
Embodiment 1
A kind of burdock extract, is prepared via a method which：
(1) burdock is cleaned up；
(2) burdock cleaned up in step (1) is subjected to pulverization process with pulverizer；
(3) by the burdock crushed as 40 DEG C of baking oven freeze-day with constant temperature to constant weight；
(4) burdock powder 1g dried in step (3) is taken, 40% ethanol solution for then taking 20ml with graduated cylinder is soaked Bubble processing；
(5) it is 40 DEG C, power 150W the mixed solution obtained by step (4) to be controlled into temperature, and frequency is the super of 40KHz Ultrasonic 30min under the conditions of sound, filtration treatment then is carried out with 0.45 μm of filtering with microporous membrane, and collect gained filtrate；
(6) filtrate obtained by step (5) is controlled and carries out vacuum rotation under conditions of vacuum is 0.094-0.096MPa Turn evaporation, obtain burdock extract concentrate, control temperature to be freeze-dried for -55 DEG C, produce burdock extract.
Embodiment 2
(1) chrysanthemum potato is cleaned up；
(2) the chrysanthemum potato cleaned up in step (1) is subjected to pulverization process with pulverizer；
(3) by the chrysanthemum potato crushed as 40 DEG C of baking oven freeze-day with constant temperature to constant weight；
(4) chrysanthemum potato powder 1g dried in step (3) is taken, 50% ethanol solution for then taking 20ml with graduated cylinder is soaked Bubble processing；
(5) it is 50 DEG C, power 150W the mixed solution obtained by step (4) to be controlled into temperature, and frequency is the super of 40KHz Ultrasonic 20min under the conditions of sound, filtration treatment then is carried out with 0.45 μm of miillpore filter, and collect gained filtrate；
(6) filtrate obtained by step (5) is controlled and carries out vacuum rotation under conditions of vacuum is 0.094-0.096MPa Turn evaporation, obtain chrysanthemum potato extract concentrated solution, control temperature to be freeze-dried for -55 DEG C, produce chrysanthemum potato extract.
By the extract of embodiment 1 and embodiment 2 with 1：1 mass ratio mixing, produces burdock extract composition
Application Example 1
The burdock extract composition of the gained of embodiment 1,2 is releived as skin, anti-sensitizer, applied in face cream, I.e. a kind of face cream containing burdock extract composition, is calculated by mass percentage, and the content and composition of its raw material are as follows：
Described solid grease is the mixture that cetostearyl alcohol and glycerin monostearate form, and is calculated in mass ratio, That is cetostearyl alcohol：Glycerin monostearate is 4：1；
Described liquid fat is the mixture of white oil, dimethicone and jojoba oil composition, is calculated in mass ratio, i.e., White oil：Dimethicone：Jojoba oil is 1：2：1；
Described emulsifying agent is the mixture of polyoxyethylene (2) stearic alcohol ether alcohol ether composition stearic with polyoxyethylene (21), Calculate in mass ratio, i.e. polyoxyethylene (2) stearic alcohol ether：Polyoxyethylene (21) stearic alcohol ether is 1.5：2；
Described preservative is the mixture that hydroxyphenyl methyl esters and hydroxyphenyl propyl ester form, and is calculated in mass ratio, i.e. oxybenzene Base methyl esters：Hydroxyphenyl propyl ester is 2：1；
Described antioxidant is 2,6- di-tert-butyl hydroxy toluenes.
A kind of preparation method of above-mentioned face cream containing burdock extract composition, specifically comprises the following steps：
(1) it is, 4g cetostearyl alcohol and 1g glycerin monostearate, the i.e. 2g of 8g liquid grease by 5g solid greases White oil, the jojoba oil of 4g dimethicone and 2g, 3.5g emulsifying agents are the 1.5g stearic alcohol ether of polyoxyethylene (2) and 2g The stearic alcohol ether of polyoxyethylene (21), 0.05g antioxidants are that the oil phase of 2,6- di-tert-butyl hydroxy toluenes composition is heated to 65-90 DEG C stirring and dissolving is incubated standby as A phases；
(2), the burdock extract composition obtained by 0.02g Examples 1 and 2 is dissolved in 83.13g deionized water and added Heat is standby as B phases to 65-90 DEG C of insulation；
(3), under the conditions of controlling homogenizer rotating speed to be 10000-20000rpm/min, by the B phases obtained by step (2) Control drop rate to be added it to for 50-100ml/min in the A phases obtained by step (1), while continue homogeneous with homogenizer 3min；
(4) after, step (3) homogeneous 3min terminates, 75~80 DEG C are cooled to, it is 100- to use agitator instead and control speed of agitator 500rpm/min carries out mechanical defoaming；
(5) when, being cooled to 45 DEG C after the completion of step (4) mechanical defoaming, it is 0.2g hydroxyphenyl methyl esters to add 0.3g preservatives With 0.1g hydroxyphenyl propyl ester, continue to control agitator speed to be stirred for 100-500rpm/min, it is to be cooled to be cooled to room temperature Stop stirring afterwards, discharging, produce a kind of face cream containing burdock extract composition.
The above-mentioned cream containing extractive composition is subjected to experiment investigation to palliative, dissipated using through transepidermal water (TEWL) method of testing, its specific experiment step are as follows：
In experimentation, 2cm × 2cm test zone grids are drawn on two arms of subject or so, then by hand Arm clear water is cleaned and dried, and exposure is under the present circumstances (it is required that being maintained at 20 DEG C, relative humidity 50% or so as far as possible).Then protect Hold that phychology is gentle, the basic value of two arm grid spaces is determined with measuring instrument, after this, wherein in left arm, Tu Yi Quantitative cream, it need to smear uniformly and cover whole grid spaces.Then the experiment number of half an hour, one hour and two hours are measured According to.
It is parallel to test three times under the same terms, and average.
The TEWL values of face cream containing extractive composition are as shown in table 1, as it can be seen from table 1 same left arm is applying TWEL value (base of the TEWL values after the face cream containing said composition extract compared to the arm for being not coated with any product is smeared Plinth value) have an obvious reduction, and the time under the same conditions, smeared a left side for the face cream containing said composition extract The TEWL values of arm will generally be less than the TEWL values of blank control group.Skin TEWL values are lower, and it is better just to represent skin barrier function. And this method is to utilize vapor barometric gradient, this gradient is formed in different 2 cuticula moisture losses, finally Inverse relation is presented with moisture content of skin in obtained TEWL values.This just illustrates that the face cream containing composition can play and subtracted well Slow skin barrier dehydration effect, it can be seen that the face cream containing said composition has certain moisturizing, barrier maintenance effect.
The TEWL value researchs of face cream of the table 1 containing extractive composition
Experiment investigation is carried out by the above-mentioned cream antiallergic containing extractive composition is palliative, its specific experiment step is such as Under：
In experimentation, radius is drawn on two arms of subject or so as 1cm test zones circle, then by hand Arm clear water is cleaned and dried, and exposure under the present circumstances (it is required that be maintained at 20 DEG C, relative humidity 50% or so as far as possible.Then protect Hold that phychology is gentle, the basic value and blank value of two arm grid spaces are determined with measuring instrument, after this, right arm wherein On, a certain amount of cream is applied, need to smear uniformly and cover whole grid spaces.After cream is completely dry, divide in left and right arm The histamine phosphate solution of same concentrations Di not gone up.Then the experimental data of 15 minutes, 20 minutes and 30 minutes is measured, and is observed The situation of wheal on arm.
It is parallel to test three times under the same terms, and average.
The blood red pigment value of face cream containing extractive composition is as shown in figure 1, it will be seen from figure 1 that smearing The blood red pigment value of the right arm of face cream containing said composition extract will generally be less than the blood red pigment value of blank control group. In addition, further it is observed that after histamine phosphate is added dropwise, the arm of left and right two has a wheal generation respectively, and specific data are as shown in table 2. We substantially observe, scribble the wheal that the wheal of the arm of the cream will be significantly less than on the arm for being not coated with the cream.This With regard to illustrating the cream containing said composition, there is certain antihistamine effect to skin.It can be seen that contain said composition Face cream has certain antiallergic effect.
The diameter of the different time wheal of table 2
Application Example 2
The burdock extract composition of the gained of embodiment 1,2 is releived as skin, anti-sensitizer, applied in toner, I.e. a kind of toner containing burdock extract composition, is calculated by mass percentage, and the content and composition of its raw material are as follows：
Described burdock extract composition, it is made up of burdock extract, chrysanthemum potato extract, the mass ratio of composition is 1： 1,
Described solubilizer is 0.5g rilanit specials；
Described rheology control agent is 0.5g hydroxyethyl celluloses；
Described preservative is the mixture of hydroxyphenyl methyl esters and hydroxyphenyl propyl ester composition, is calculated in mass ratio, i.e. oxybenzene Base methyl esters：Hydroxyphenyl propyl ester is 2：1, i.e. the hydroxypropyl propyl ester of 0.04g hydroxypropyls methyl esters and 0.02g.
Described essence is 0.01g commercially available essence used for cosmetic.
A kind of preparation method of described toner containing burdock extract composition, it is characterised in that specifically include as Lower step：
(1), take a certain amount of deionized water to start agitator in beaker, rheology control agent is slowly poured into beaker, flow Become conditioning agent add finish continue stir 15-20min it is standby；
(2) 0.01g essence, 0.5g solubilizer and preservative Hybrid Heating, are heated to 45 DEG C as oil phase and obtain oil Phase；
(3), will be added to containing 5g burdock extract compositions in the deionized water of step (1) uniform as Aqueous dispersions It is heated to 70 DEG C and obtains aqueous phase；
(4) aqueous phase obtained by step (3), is cooled to 45 DEG C, then the oil phase obtained by step (2) is added to step (3) In the aqueous phase of gained, while mixer is opened, it is 300-500rpm/min to control mixing speed, carries out scattered 10min, and machinery stirs Mix to well mixed and naturally cool to after room temperature and stop stirring, discharging, produce a kind of refreshing containing burdock extract composition Skin water.
The above is only the basic explanation under present inventive concept, and is made according to technical scheme any etc. Effect conversion, all should belong to protection scope of the present invention.

Claims (8)

  1. A kind of 1. composition containing burdock extract, it is characterised in that：It is made up of burdock extract and chrysanthemum potato extract, described ox The mass ratio of burdock extract and chrysanthemum potato extract is 1：1；
    Described burdock extract is prepared via a method which to form：
    (1) burdock is cleaned up；
    (2) burdock cleaned up in step (1) is subjected to pulverization process with pulverizer；
    (3) by the burdock crushed as 35-45 DEG C of baking oven freeze-day with constant temperature to constant weight；
    (4) ethanol water that mass percent concentration is 35-45% will be added in burdock powder dried in step (3) to enter Row immersion treatment；
    (5) it is 35-45 DEG C, power 140-160W, frequency 35- the mixed solution obtained by step (4) to be controlled into temperature Ultrasonic 25-35min under 45KHz ultrasound condition, then with 0.45 μm of filtering with microporous membrane 3-5 times, and collect gained filtrate；
    (6) filtrate obtained by step (5) is controlled and carries out vacuum rotating steaming under conditions of vacuum is 0.094-0.096MPa Hair, obtains burdock extract concentrate, controls temperature to be freeze-dried for -55 DEG C, produces burdock extract；
    Described chrysanthemum potato extract is prepared via a method which to form：
    (1) chrysanthemum potato is cleaned up；
    (2) the chrysanthemum potato cleaned up in step (1) is subjected to pulverization process with pulverizer；
    (3) by the chrysanthemum potato crushed as 35-45 DEG C of baking oven freeze-day with constant temperature to constant weight；
    (4) ethanol water that mass percent concentration is 45-55% will be added in chrysanthemum potato powder dried in step (3) to enter Row immersion treatment；
    (5) it is 45-55 DEG C, power 140-160W, frequency 35- the mixed solution obtained by step (4) to be controlled into temperature Ultrasonic 15-25min under 45KHz ultrasound condition, filtration treatment then is carried out with 0.45 μm of miillpore filter, and collect gained and filter Liquid；
    (6) filtrate obtained by step (5) is controlled and carries out vacuum rotating steaming under conditions of vacuum is 0.094-0.096MPa Hair, obtains chrysanthemum potato extract concentrated solution, controls temperature to be freeze-dried for less than -55 DEG C, produces chrysanthemum potato extract.
  2. A kind of 2. application of composition containing burdock extract in cosmetics described in claim 1.
  3. 3. application according to claim 2, it is characterised in that：Apply in face cream or toner.
  4. 4. application according to claim 3, it is characterised in that：Weight ratio of the burdock extract in cosmetics is 1%- 10%th, weight ratio of the chrysanthemum potato extract in cosmetics is 1%-10%.
  5. 5. a kind of face cream of the composition containing burdock extract containing described in claim 1, it is characterised in that by quality percentage Than calculating, the content and composition of its raw material are as follows：
    The 2%-20% of composition containing burdock extract
    Mineral grease 1-5%
    Synthetic Oil 1-4%
    Vegetable fat 1-5%
    Animal fat 0-2%
    Emulsifying agent 2-6%
    NMF 2-10%
    Preservative 0.05-0.2%
    Antioxidant 0.01-0.1%
    Surplus is deionized water；
    Described mineral grease is the mixture that stearic acid and white oil form, and is calculated in mass ratio, i.e. stearic acid：White oil is 4：1；
    Described Synthetic Oil is the mixture of isobutyl palmitate, glycerin monostearate and dimethyl siloxane composition, is pressed Mass ratio calculates, i.e. isobutyl palmitate：Glycerin monostearate is：Dimethyl siloxane 6：1：2；
    Described vegetable fat is the mixture that Sweet Almond Oil and olive oil form, and is calculated in mass ratio, i.e. Sweet Almond Oil：Olive Oil is 1：2；
    Described emulsifying agent is the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21), the match emulsifying agent group of Bick 305 Into mixture, calculate in mass ratio, i.e. polyoxyethylene (2) stearic alcohol ether：Polyoxyethylene (21) stearic alcohol ether：Match Bick 305 Emulsifying agent is 2：3：3；
    Described NMF is the mixture that glycerine and butanediol form, and is calculated in mass ratio, i.e. glycerine：Butanediol is 1:3；
    Described preservative is the mixture that methyl hydroxybenzoate and propylben form, and is calculated in mass ratio, i.e. Metagin Ester：Propylben is 2：1；
    Described antioxidant is 2,6- di-tert-butyl hydroxy toluenes.
  6. A kind of 6. preparation method of face cream containing the composition containing burdock extract described in claim 5, it is characterised in that Comprise the following steps：
    (1) oil phase 1 of mineral grease, Synthetic Oil, match Bick 305 emulsifying agent composition is heated to 65-90 DEG C of stirring and dissolving work For A1 phases；
    (2) oil phase for forming vegetable fat, the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21), antioxidant 2 are heated to 65-90 DEG C of stirring and dissolving as A2 phases；
    (3) composition containing burdock extract is dissolved in 5~30% deionized water and is heated to the water of 50-70 DEG C of insulation Phase 1 is used as B1 phases；
    (4) NMF is dissolved in balance deionized water, and heating stirring is completely dispersed uniform aqueous phase 2 to 65-90 DEG C and is used as B2 phases；
    (5) temperature is controlled at 70-85 DEG C, and the A1 phases obtained by step (1) and step (2) with A2 phases be mixed and stirred for It is even, total oil phase is made as A phases；
    (6) controlling temperature, mixer mixing speed is 500-700rpm/min, by step (4) and step (5) institute at 70-85 DEG C The B2 phases obtained with A phases be mixed and stirred for uniformly；
    (7) it is 500-700rpm/min, to control mixer mixing speed, and the mixture obtained by step (6) is cooled into 50-70 DEG C, then mixed with the B1 obtained by step (3)；
    (8) under the conditions of controlling homogenizer rotating speed to be 10000-20000rpm/min, by the mixture thing obtained by step (7) It is uniformly dispersed；
    (9) after step (8) is well mixed, when being naturally cooling to 45 DEG C, preservative is added, it is equal to mixing to continue mechanical agitation It is even, speed of agitator 100-500rpm/min；And stop stirring after naturally cooling to room temperature, discharging, produce one kind and contain ox The face cream of burdock extractive composition.
  7. 7. a kind of toner of the composition containing burdock extract containing described in claim 1, it is characterised in that by quality percentage Than calculating, the content and composition of its raw material are as follows：
    The 2%-20% of composition containing burdock extract
    Solubilizer 0.5-2%
    Rheology control agent 0.05-0.5%
    Preservative 0.05-0.2%
    Essence 0.01-0.05%
    Surplus is deionized water；
    Described solubilizer is rilanit special；
    Described rheology control agent is hydroxyethyl cellulose；
    Described preservative is the mixture of hydroxyphenyl methyl esters and hydroxyphenyl propyl ester composition, is calculated in mass ratio, i.e. hydroxyphenyl first Ester：Hydroxyphenyl propyl ester is 2：1.
  8. A kind of 8. preparation method of the toner of composition containing burdock extract described in claim 7, it is characterised in that including Following steps：
    (1) deionized water is added in a container, starts agitator, rheology control agent slowly poured into described container, Rheology control agent add finish continue stir 15-20min it is standby；
    (2) essence, solubilizer and preservative Hybrid Heating are heated to 45 DEG C as oil phase and obtain oil phase；
    (3) it will be added in the deionized water of step (1) containing composition containing burdock extract and uniformly heated as Aqueous dispersions Aqueous phase is obtained to 50 DEG C；
    (4) aqueous phase obtained by step (3) is cooled to 45 DEG C, then the oil phase obtained by step (2) is added to obtained by step (3) In aqueous phase, while mixer is opened, it is 300-500rpm/min to control mixing speed, carries out scattered 10min, and mechanical agitation is to mixed Close uniformly and stop stirring after naturally cooling to room temperature, discharging, produce a kind of toner containing the composition containing burdock extract.
CN201710763382.7A 2017-08-30 2017-08-30 A kind of composition containing burdock extract and its application in cosmetics Pending CN107468576A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110754609A (en) * 2019-12-11 2020-02-07 厦门闽得友食品科技有限公司 Compound color fixative for aquatic products and preparation process thereof
CN111265465A (en) * 2020-04-01 2020-06-12 广州今盛美精细化工有限公司 Cubilose extract and application thereof in preparation of cosmetics

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103599021A (en) * 2013-11-15 2014-02-26 上海应用技术学院 Roselle extract as well as preparation method thereof and application thereof in whitening skincare cosmetics
CN104940049A (en) * 2014-03-28 2015-09-30 浙江大学 Method for extracting smallanthus sonchifolius plant extract, extract and application
CN106821832A (en) * 2015-12-04 2017-06-13 上海家化联合股份有限公司 A kind of composition comprising ginseng extract and burdock extract

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103599021A (en) * 2013-11-15 2014-02-26 上海应用技术学院 Roselle extract as well as preparation method thereof and application thereof in whitening skincare cosmetics
CN104940049A (en) * 2014-03-28 2015-09-30 浙江大学 Method for extracting smallanthus sonchifolius plant extract, extract and application
CN106821832A (en) * 2015-12-04 2017-06-13 上海家化联合股份有限公司 A kind of composition comprising ginseng extract and burdock extract

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110754609A (en) * 2019-12-11 2020-02-07 厦门闽得友食品科技有限公司 Compound color fixative for aquatic products and preparation process thereof
CN111265465A (en) * 2020-04-01 2020-06-12 广州今盛美精细化工有限公司 Cubilose extract and application thereof in preparation of cosmetics

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