CN104644528B - A kind of preparation method and application of edible moisture-keeping nutrient ointment - Google Patents
A kind of preparation method and application of edible moisture-keeping nutrient ointment Download PDFInfo
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Abstract
A kind of preparation method and application of edible moisture-keeping nutrient ointment, belong to cosmetics processing technique field, including okra treatment, the treatment of propolis, it is prepared by licorice, the extraction of ginko leaves flavone, the preparation of fibroin albumen, it is prepared by perilla herb oil, it is prepared by the preparation of pine-seed oil and emulsifying agent, it is basic emulsus material with the milk, add deionized water, after being sufficiently stirred for, 1%~5% volume okra refinishing polyose product of addition, 0.1%~1.0% volume propolis clayey, 0.1%~1.0% volume licorice, 0.1%~1.0% volume ginko leaves flavone and 0.1%~2.0% volume fibroin albumen, obtain moisture-keeping nutrient ointment.The present invention produces safety, edible moisturizing ointment using okra, propolis, Radix Glycyrrhizae, ginkgo leaf, fibroin and perilla herb oil, maize germ, wheat germ oil, pine-seed oil etc., is suitably applied the exposed skin of easy contacting foodstuff.
Description
Technical field
The invention belongs to cosmetics processing technique field, more particularly to a kind of method for preparing edible moisturizing ointment and
Its concrete application.
Background technology
Skin is the vitals for maintaining people's life and health, is made up of collagen, elastin laminin, and the state of skin takes
The ability of cell synthetic protein certainly in the loss of protein and skin.And growth to Skin Cell, be metabolized decision and make
The cell factor for be albumen, special enzyme, playing regulatory role.It can be seen that, protein serves very important in skin
Effect.Supplement protein, can improve skin elasticity, absorption of the enhancing skin to protein.The present invention is using okra, honeybee
Glue, Radix Glycyrrhizae, ginkgo leaf, fibroin and edible vegetable oil (perilla herb oil, maize germ, wheat germ oil) etc., addition food emulsification
Agent (mono-fatty acid glyceride, diglycerine fatty acid ester, D-sorbite, polyglyceryl fatty acid ester, propane diols, potassium stearate, sucrose
Fatty acid ester etc.), prepare edible Novel moisturizing nutritional ointment.
Contain various nutritional ingredients in above-mentioned plant, wherein also contain special functional components, with exfoliating, tightly
The effects such as skin, anti-aging, whitening, anti-oxidant, moisturizing, anti-inflammatory.Edible plants raw material used includes：It is okra, propolis, sweet
Grass, ginkgo leaf, fibroin and edible vegetable oil (perilla herb oil, maize germ, wheat germ oil)：
1st, okra
Okra fruit is rich in protein, fat, carbohydrate, vitamin, mineral matter and dietary fiber, while also richness
Containing compositions such as flavones, polysaccharide.Contain a kind of special mucus in fruit, this rare emplastic is also referred to as okra food
With glue, wherein main component is pectin, viscous glycoprotein etc., be the polysaccharide that is made up of arabinose, galactolipin, rhamnose etc. with
The covalent complex that protein is formed.The colloid has that viscosity is high, emulsibility strong, moisture retention and the suspension stability spy such as preferably
Point, can be used in food industry as preferable natural additive for foodstuff.
(1) protein content in setose abelmoschus seed is about 23%-25%, total reducing sugar 19.92%, polysaccharide 2.00%, fat
9.40%, flavones 2.56%.Gumbo seed protein contains 18 kinds of amino acid HJ, including 8 kinds of amino acid needed by human and other paddy
The limiting amino acid of thing --- lysine.Additionally, also containing sticking glycoprotein in tender okra pod.Viscous glycoprotein is
A kind of polysaccharide, protein mixture by collagen and mucopolysaccharide material composition, can strengthen the resistance of body, promote courage
The excretion of sterol material, also protects stomach, liver, skin and mucous membrane, strengthens the effect of skin elasticity.
(2) okra is rich in zinc, selenium and other trace elements, can strengthen human body cancer-resisting ability.Plus containing abundant Vc
And Soluble Fiber, it is with health role to skin, skin-whitening, delicacy can be made, prevent black.
(3) gum components extracted in okra, are a kind of water miscible polysaccharide, mainly containing rhamnose, arabinose, half
The polysaccharide such as lactose and a small amount of glycoprotein.It is hydrophilic colloid, contains a large amount of hydrophilic hydroxy groups, the cosmetics and skincare product energy being produced
Good emulsibility, water imbibition, high viscosity and moulding property are enough shown, the improvement colour of skin, anti-aging, the work(of efficient moisture-retention is can reach
Energy.Due to the important composition composition in polysaccharide inherently skin, mainly there are hyaluronic acid, chondroitin sulfate and heparin etc., join
With the various vital movements of cell.Therefore active polysaccharide has a extensive future in effect type cosmetics and skincare product.Can in food
As thickener, emulsifying agent and stabilizer, not only with viscosity it is high, stability is strong, suspension is good the features such as, and colloid is also
With various drug effects and healthcare function；
2nd, propolis
Propolis (propolis) is honeybee herborization bud core, the secretion of the viscose glue on trunk and itself upper palatine gland and honeybee
The complex compound that wax etc. is mixed and processed.Its chemical composition is considerably complicated, mainly resinae, Polyphenols, polysaccharide
With the mixture of beeswax.Separated measure, propolis contain flavone compound (more than 20 plant), acid, alcohol, phenol, aldehyde, ester and alkene, hydrocarbon,
Terpene, steroid, also contain vitamin B1, vitamin A, several amino acids, enzyme and 20 various trace elements etc..Can recognize
To contain most of material necessary to biological existence in propolis.
Propolis has broad-spectrum antibacterial action, and it can suppress and kill 100 various bacterias, and living organism can also be promoted to protect
Ability, improves blood circulation, promotes granulation to grow, accelerating wound healing, and with the function such as moist, antipruritic, deodorant, sun-proof.
In cosmetics, propolis has a wide range of applications, and can be added in the products such as cream, emulsion, hair-cream, shampoo, hair lotion, makes up
Mostly in product is using the ethanol extract of propolis.
3rd, Radix Glycyrrhizae
Licorice, is the composition for having medical value extracted from Radix Glycyrrhizae.Licorice is generally comprised：Glycyrrhizin
Element, glycyrrhizic acid, liquiritin, flavonoids of Glycyrrhiza, rear curtain are than wingceltis element, formoononetin, Quercetin etc..Wherein：Glycyrrhizin 6%~
14%th, glycyrrhizin calcium sylvite, Radix Glycyrrhizae hardship tongue etc., also contain sucrose 2.4%~6.5%, glucose 3.5%~4.0%, sweet dew
Sugar alcohol and aspartic acid 2%~4%.Licorice be used as cosmetic additive agent, its effect is anti-inflammatory, preventing and treating rhagadia manus et pedis and
Frostbite, can be used in the cosmetics such as cream, milk.Radix Glycyrrhizae in middle polar solvent (ethyl acetate, chloroform, ether) solubility
Composition has hair care, the remarkable result of hair care.
4th, ginkgo leaf
(1) whitening aspect：The increase at age and influenceed by external environment, internal oxygen radical can gradually increase,
Superoxide dismutase (SOD) can be made not enough, cause excessive oxygen radical that the reaction of oxidation is produced with corium confluent monolayer cells, caused
Chloasma or cyasma.Contained flavone component can hinder formation and calmness of the pigment in skin corium in ginkgo leaf, reach
To skin whitening and the effect for preventing and treating pigment patch.In addition to flavones, the zinc in ginkgo leaf, manganese, the trace element such as molybdenum also can
Remove free radical and suppress and pigment growth.
(2) smoothing wrinkle aspect：The skin of human body updates completely once to be needed to last 3 months or so, there is small microgroove, reason on the face
Be, the neonatal cell that skin corium is formed when not arriving at also to skin surface just by excessive free-radical oxidation, when
It already belongs to aged cells when arriving to epidermis.Glycosides displayed and flavonols in ginkgo leaf are all cleaning the street for free radical
Husband, can protect corium confluent monolayer cells, improve blood circulation, prevent cell to be oxidized to wrinkle.
5th, fibroin
Fibroin, also known as silk powder, is that one kind that chemical treatment of selected silkworm (such as silkworm) silk through relaxing is processed is white
Powdered hmw protein, maintains the prototype structure and chemical composition of silk.Its exquisiteness is smooth, good permeability, adhesive force
By force, with the change of temperature and humidity, moisture can be absorbed or discharge, also with the ability of unique retention oil.The master of fibroin
It is silk-fibroin and sericin to want composition, and sericin contains largely various amino acid necessary to formation cells, can adjust
The content of lipid in sebum, increases the lipid of Dry, is especially suitable for the relatively dry old women of skin.And silk-fibroin is
Fibrous protein, molecular structure is similar to the collagen of skin, it is easy to absorb, and can improve skin elasticity, in cosmetics, silk
The much more plain raw material as cosmetics (such as lipstick, muffin, eye cosmetic), it is nontoxic to human body, have no side effect, to skin
Skin is nonirritant, has good moisture-retaining capacity to the moisture of keratoderma, moreover it is possible to absorb ultraviolet, with resisting solar radiation
Effect.When fibroin is used for cosmetics with mica powder as matrix, help to reduce reflected light, be color it is more true to nature,
It is more natural.Fibroin has good heat endurance, and the consumption in this kind of silty cosmetics may be up to 20%, make product
Smear is improved, and feels more comfortable.
6th, perilla herb oil
Perilla seed is the seed of labiate purple perilla.Seed oil yield is up to 45% or so, and leukotrienes is accounted in oil
62.73%, linoleic acid accounts for 15.43%, and oleic acid accounts for 12.01%.Protein content is up to 25% in seed, containing 18 kinds of amino acid,
Wherein lysine, methionine content it is higher.Also contain oryzanol, vitamin E, B1, sterol, phosphatide etc..
(1) perilla herb oil contains alpha-linolenic acid；ω-3.There is good affinity to skin, can collect wet and increase profit, clinical research table
Bright, the curative effect of many anaphylaxis dermatosis of perilla herb oil and chapped skin is very notable.
(2) perilla herb oil has broad-spectrum antibacterial action, to staphylococcus aureus, dark green bar containing compositions such as perillaldehyde, limonenes
The common pathogenic bacteria for contaminating skin such as bacterium and Epidermophvton tinea have obvious inhibitory action, and this antibacterial action extremely low
Just can be shown under concentration, the characteristic of this efficiently anti-invasive organism of purple perilla volatile oil, to it as cosmetics function raw material
For, it is extremely advantageous condition.
(3) perilla herb oil has good surface-active, refers to a kind of drier oil, and viscosity is low, skin surface is formed breathable films,
So as to, skin dehydration and the dip-dye of microorganism are prevented, make skin smooth and illegal viscous, it is a kind of film forming day of organic high value
Right additive.
7th, maize germ, wheat germ oil
Main component is fat, protein, cellulose, gamma oryzanol and carbohydrate, and active component has riboflavin,
Sterol compound, thiamine and a small amount of mineral matter etc..Plumule has very strong antibiotic property, can suppress to be invaded in bacterium.Containing embryo oil
Cosmetics have obvious curative effects to common skin diseases such as chronic eczema, blackspot, skin agings.Gamma oryzanol in embryo oil can increase
Strong skin internal system function, adjusts sebum secretion, stimulates circulation.This agent is with embryo oil, apricot kernel oil and SP etc.
Raw material is formulated, and has preferable moisten effect to eye part skin, particularly has good elimination to act on to crow's foot；
8th, pine-seed oil
Containing other plant oil without Pi Nuolin acid with the little several 20 carbons unrighted acids of content.These
Unrighted acid is composition necessary to cell membrane lipid albumen, and the integrality for being also to maintain skin barrier effect is indispensable
Part.Unrighted acid may also suppress the aging of skin, lacks unrighted acid and causes skin exfoliation, moisture loss
Increase.
Also contain natural vitamin A in pine-seed oil, help to maintain skin emolliency and plentiful, improve skin and keep moisture
Function, prevents damage of the ultraviolet to skin.Vitamin E is natural, is most widely used composition in cosmetics, it
With anti-oxidant and removing free radical effect, suppress infringement of the free radical to skin, and UV-induced skin can be prevented
It is aging.
At present, using okra, propolis, Radix Glycyrrhizae, ginkgo leaf, fibroin and edible perilla herb oil, maize germ, wheat
Oil, pine-seed oil, add food-grade emulsifying agent (including：It is mono-fatty acid glyceride, diglycerine fatty acid ester, D-sorbite, poly- sweet
Oil and fat acid esters, propane diols, potassium stearate, sucrose fatty ester etc.), (cosmetics are led to prepare edible moisture-keeping nutrient ointment
Domain) have no report.Therefore, needed badly in the middle of prior art and want a kind of new technical scheme to solve this problem.
The content of the invention
The technical problems to be solved by the invention are：A kind of preparation of edible Novel moisturizing nutritional ointment is provided and is answered
With using the production such as okra, propolis, Radix Glycyrrhizae, ginkgo leaf, fibroin and perilla herb oil, maize germ, wheat germ oil, pine-seed oil
Go out safety, edible Novel moisturizing ointment, be suitably applied the exposed skin of easy contacting foodstuff.
A kind of preparation of edible Novel moisturizing nutritional ointment, it is characterized in that：Comprise the following steps,
Step one, okra treatment
Take fresh okra pod to shred and stir, be beaten, the slurries of acquisition carry out centrifugation removal after being extracted with water
Insoluble composition in slurries, obtains centrifugation solution；
Centrifugation solution is filtered, the ethanol solution for adding concentration to be 25%~50% is precipitated, obtaining content is
70%~80% okra viscose glue precipitation, by centrifugation, vacuum drying, obtains the okra jelly of brown；
Okra jelly is dissolved in cold water, dialysis 1 day~3 is carried out in 15 times~25 times distilled water of volume
My god, liquid is changed daily 3 times or 4 times, freeze-drying obtains Thick many candies；Thick many candies are dissolved in distilled water, add tannic acid to remove egg
In vain, it is 15%~20%H to add concentration202It is that concentrate after 0.5%~1% activated carbon is decolourized is splined on again with concentration
Microcrystalline cellulose post, adds distillation water elution, and volume ratio 1 is added after wash-out：4 water and ethanol is recrystallized, and is obtained after drying
Obtain the okra refinishing polyose product of white powder；
The treatment of step 2, propolis
Take propolis raw material 10g~50g to crush, be put into 1000ml conical flasks, add 95% ethanol solution to be put into ultrasonic wave
Inside dissolve it, then rinsed to propolis in ultrasonic wave with 95% ethanol solution and be completely dissolved, will again be moved into after supernatant liquid filtering
Solution is evaporated in revolving bottle, remaining liq is poured into evaporating dish, is put into vacuum drying chamber, and residual ethanol is removed completely,
Obtain propolis clayey standby；
It is prepared by step 3, licorice
Extracting liquorice is crushed, and is extracted using extraction and ultrasonic assistant method, in Radix Glycyrrhizae after being pulverized
The ethanol water that ethanol content is 40%~60% is added, Radix Glycyrrhizae is 1 with the volume ratio of ethanol water:15；40 DEG C~
60 DEG C, and ultrasonic power is under the conditions of 75W~85W, extraction 1 hour under these conditions, is repeated 2 times or 3 times, is obtained
It is standby to licorice；
The extraction of step 4, ginko leaves flavone
Ginkgo leaf is taken, using alcohol extraction procedure, ginkgo leaf is dried and 45 mesh~55 mesh, silver after being pulverized are crushed to
The ethanol water that concentration of alcohol is 50%~70% is added in apricot leaf, ginkgo leaf is 1 with the volume ratio of ethanol water:15；
Under conditions of 75 DEG C~85 DEG C, 2h~4h is extracted, under these conditions, repeat 2 times or 3 times to activated carbon decolorizing, obtained
To ginko leaves flavone extract；
The preparation of step 5, fibroin albumen
Silk cocoon is taken, degumming operation is carried out, the macromolecular fibroin albumen obtained after degumming adds Na2CO3Solution is refined twice,
After refining terminates, CaCl is added2Dissolving fibroin, desalination degraded is carried out using the deionized water of flowing, obtains the polypeptide of small molecule
And amino acid；
It is prepared by step 6, perilla herb oil
Choosing purple perilla seed carries out selection by winnowing, magnetic separation, sieving and removal of impurities, is rinsed with circulating water, under conditions of 35 DEG C,
Forced air drying is carried out, purple perilla seed of the water content less than 8% is obtained standby；
Dried purple perilla seed is carried out into oil expression treatment, oil expression temperature is 40 DEG C~50 DEG C, oil expression pressure for 2Mpa~
10Mpa, the perilla herb oil of acquisition carries out decolourizing and deodorization treatment again, obtains the excellent perilla herb oil of oil, and the Residual oil of purple perilla oil meal contains
Measure is 4%~8%；
The preparation of step 7, pine-seed oil
Take pine nut to be screened by screening machine, soaked with clear water, and it is totally smooth to be polishing to surface, 90 DEG C~120
Under conditions of DEG C, boiling 30min~60min carries out sterilization treatment, and the pine nut after sterilizing manually strips SEMEN PINI KORAIENSIS；
By 1:1 ratio takes SEMEN PINI KORAIENSIS and No. 6 Extraction solvent oil, and 50 DEG C~55 DEG C of heating water bath leaches 40min, will be mixed
Original solvent naphtha is released in compound, continuously adds No. 6 Extraction solvent oil equal with discharging amount, extracts 30min, then will mixing
Original solvent naphtha is released in thing, repeats aforesaid operations, extracts 20min；By by three mixtures of extraction, it is put into rotation and steams
Hair device precipitation, at 75 DEG C~80 DEG C, pressure is 0.08MP~0.10MP to control temperature, obtains the pine-seed oil of concentration；
Under conditions of 5 DEG C~15 DEG C, alkali lye is added in the pine-seed oil of concentration, need to all be added in 5min~10min,
Add alkali lye during, be stirred with the speed of 60r/min, in 30min by oil temperature rise to 60 DEG C~65 DEG C, mixing speed
30r/min is down to, continues to stir 10min~20min, static 6h~8h, after removing the edible vegetable oil on upper strata, then add pine nut weight of oil
10%~15% water is cleaned；The charcoal absorption that pine-seed oil after cleaning adds pine nut weight of oil 1% is decolourized, 75
DEG C~85 DEG C under conditions of, stirring 15min~20min after filter；Under vacuum >=0.07MP and 85 DEG C~95 DEG C of constant temperature,
Dehydration 0.3h~0.6h；100 DEG C of steam 3h are passed through, 180 DEG C, under conditions of vacuum >=0.07MP are reached in pine nut oil temperature,
Deodorization refining is carried out, the antioxidant tertiary butyl hydroquinone of pine nut weight of oil 0.02% is added, pine-seed oil is obtained standby；
It is prepared by step 8, emulsifying agent
Take deionized water, the mono-fatty acid glyceride or diglycerine fatty of 10%~40% volume of 20%~50% volume
Acid esters, the sucrose fatty ester of 10%~30% volume, the D-sorbite of 10%~30% volume, 10%~20% volume it is poly-
The potassium stearate of fatty acid glyceride, the propane diols of 3%~10% volume and 0.2%~1.0% volume is merged, fully
Stirring obtains milk；
It is basic emulsus material with the milk, adds deionized water, emulsus material is 1 with the mass ratio of deionized water：0.5
~1:2.5, after being sufficiently stirred for, addition 1%~5% volume described in step one obtain okra refinishing polyose product, 0.1%~
Described in 1.0% volume step 2 obtain propolis clayey, described in 0.1%~1.0% volume step 3 obtain licorice,
The ginko leaves flavone and step 5 described in 0.1%~2.0% volume that step 4 described in 0.1%~1.0% volume is obtained are obtained
Fibroin albumen, obtain moisture-keeping nutrient ointment.
Okra Thick many candies in the step one contain 35%~40% galactolipin, 25%~30% rhamnose, 20%
~25% galacturonic acid and 3%~5% protein.
Can be added in the step 8 perilla herb oil of 1%~3% volume, the maize germ of 1%~3% volume, 1%~
The pine-seed oil of the wheat germ oil of 3% volume or 1%~3% volume.
The edible moisture-keeping nutrient ointment is used to produce lip film, hand lotion or spats frost.
By above-mentioned design, the present invention can bring following beneficial effect：A kind of edible Novel moisturizing nutrition
The preparation and application of ointment, using okra, propolis, Radix Glycyrrhizae, ginkgo leaf, fibroin and perilla herb oil, maize germ, wheat
Oil, pine-seed oil etc. produce safety, edible Novel moisturizing ointment, are suitably applied the exposed skin of easy contacting foodstuff.System
The raw material for making moisture-keeping nutrient ointment is food-grade, and security is good and with edibility；As lip film, hand lotion, spats
Frost, and the exposure limb part of contacting foodstuff can be smeared, high safety；Aqueous and water retention property is strong, is applied to skin
Surface, moistening effect is good；Containing a large amount of nutritional ingredients, regeneration and repairing to skin tissue cell have good action, while
Volume nutrient needed for skin can be supplemented.
Brief description of the drawings
Below in conjunction with the drawings and specific embodiments, the present invention is further illustrated：
Fig. 1 is a kind of preparation method and application schematic process flow diagram of edible moisture-keeping nutrient ointment of the present invention.
Fig. 2 be a kind of edible moisture-keeping nutrient ointment of the present invention preparation and application in okra polysaccharide preparation flow show
Meaning block diagram.
Fig. 3 is that pine-seed oil preparation flow shows in a kind of preparation method and application of edible moisture-keeping nutrient ointment of the present invention
Meaning block diagram.
Fig. 4 is that perilla herb oil preparation flow shows in a kind of preparation method and application of edible moisture-keeping nutrient ointment of the present invention
Meaning block diagram.
Specific embodiment
A kind of preparation method of edible moisture-keeping nutrient ointment, as shown in figure 1, comprise the following steps,
Step one, okra treatment
As shown in Fig. 2 take fresh okra pod and shredding and stirring, it is beaten, the slurries of acquisition extract laggard with water
Insoluble composition in row centrifugation removal slurries, obtains centrifugation solution；
Centrifugation solution is filtered, the ethanol solution for adding concentration to be 25%~50% is precipitated, obtaining content is
70%~80% okra viscose glue precipitation, by centrifugation, vacuum drying, obtains the okra jelly of brown；
Okra jelly is dissolved in cold water, dialysis 1 day~3 is carried out in 15 times~25 times distilled water of volume
My god, liquid is changed daily 3 times or 4 times, freeze-drying obtains Thick many candies；Thick many candies are dissolved in distilled water, add tannic acid to remove egg
In vain, it is 15%~20%H to add concentration202It is that concentrate after 0.5%~1% activated carbon is decolourized is splined on again with concentration
Microcrystalline cellulose post, adds distillation water elution, and volume ratio 1 is added after wash-out：4 water and ethanol is recrystallized, and is obtained after drying
Obtain the okra refinishing polyose product of white powder；
The treatment of step 2, propolis
Take propolis raw material 10g~50g to crush, be put into 1000ml conical flasks, add 95% ethanol solution to be put into ultrasonic wave
Inside dissolve it, then rinsed to propolis in ultrasonic wave with 95% ethanol solution and be completely dissolved, will again be moved into after supernatant liquid filtering
Solution is evaporated in revolving bottle, remaining liq is poured into evaporating dish, is put into vacuum drying chamber, and residual ethanol is removed completely,
Obtain propolis clayey standby；
It is prepared by step 3, licorice
Extracting liquorice is crushed, and is extracted using extraction and ultrasonic assistant method, in Radix Glycyrrhizae after being pulverized
The ethanol water that ethanol content is 40%~60% is added, Radix Glycyrrhizae is 1 with the volume ratio of ethanol water:15；40 DEG C~
60 DEG C, and ultrasonic power is under the conditions of 75W~85W, extraction 1 hour under these conditions, is repeated 2 times or 3 times, is obtained
It is standby to licorice；
The extraction of step 4, ginko leaves flavone
Ginkgo leaf is taken, using alcohol extraction procedure, ginkgo leaf is dried and 45 mesh~55 mesh, silver after being pulverized are crushed to
The ethanol water that concentration of alcohol is 50%~70% is added in apricot leaf, ginkgo leaf is 1 with the volume ratio of ethanol water:15；
Under conditions of 75 DEG C~85 DEG C, 2h~4h is extracted, under these conditions, repeat 2 times or 3 times to activated carbon decolorizing, obtained
To ginko leaves flavone extract；
The preparation of step 5, fibroin albumen
Silk cocoon is taken, degumming operation is carried out, the macromolecular fibroin albumen obtained after degumming adds Na2CO3Solution is refined twice,
After refining terminates, CaCl is added2Dissolving fibroin, desalination degraded is carried out using the deionized water of flowing, obtains the polypeptide of small molecule
And amino acid；
It is prepared by step 6, perilla herb oil
As shown in figure 4, choosing purple perilla seed carries out selection by winnowing, magnetic separation, sieving and removal of impurities, it is rinsed with circulating water, 35
Under conditions of DEG C, forced air drying is carried out, obtain purple perilla seed of the water content less than 8% standby；
Dried purple perilla seed is carried out into oil expression treatment, oil expression temperature is 40 DEG C~50 DEG C, oil expression pressure for 2Mpa~
10Mpa, the perilla herb oil of acquisition carries out decolourizing and deodorization treatment again, obtains the excellent perilla herb oil of oil, and the Residual oil of purple perilla oil meal contains
Measure is 4%~8%；
The preparation of step 7, pine-seed oil
As shown in figure 3, take pine nut screened by screening machine, soaked with clear water, and it is totally smooth to be polishing to surface,
Under conditions of 90 DEG C~120 DEG C, boiling 30min~60min carries out sterilization treatment, and the pine nut after sterilizing manually strips SEMEN PINI KORAIENSIS；
By 1:1 ratio takes SEMEN PINI KORAIENSIS and No. 6 Extraction solvent oil, and 50 DEG C~55 DEG C of heating water bath leaches 40min, will be mixed
Original solvent naphtha is released in compound, continuously adds No. 6 Extraction solvent oil equal with discharging amount, extracts 30min, then will mixing
Original solvent naphtha is released in thing, repeats aforesaid operations, extracts 20min；By by three mixtures of extraction, it is put into rotation and steams
Hair device precipitation, at 75 DEG C~80 DEG C, pressure is 0.08MP~0.10MP to control temperature, obtains the pine-seed oil of concentration；
Under conditions of 5 DEG C~15 DEG C, alkali lye is added in the pine-seed oil of concentration, need to all be added in 5min~10min,
Add alkali lye during, be stirred with the speed of 60r/min, in 30min by oil temperature rise to 60 DEG C~65 DEG C, mixing speed
30r/min is down to, continues to stir 10min~20min, static 6h~8h, after removing the edible vegetable oil on upper strata, then add pine nut weight of oil
10%~15% water is cleaned；The charcoal absorption that pine-seed oil after cleaning adds pine nut weight of oil 1% is decolourized, 75
DEG C~85 DEG C under conditions of, stirring 15min~20min after filter；Under vacuum >=0.07MP and 85 DEG C~95 DEG C of constant temperature,
Dehydration 0.3h~0.6h；100 DEG C of steam 3h are passed through, 180 DEG C, under conditions of vacuum >=0.07MP are reached in pine nut oil temperature,
Deodorization refining is carried out, the antioxidant tertiary butyl hydroquinone of pine nut weight of oil 0.02% is added, pine-seed oil is obtained standby；
It is prepared by step 8, emulsifying agent
Take deionized water, the mono-fatty acid glyceride or diglycerine fatty of 10%~40% volume of 20%~50% volume
Acid esters, the sucrose fatty ester of 10%~30% volume, the D-sorbite of 10%~30% volume, 10%~20% volume it is poly-
The potassium stearate of fatty acid glyceride, the propane diols of 3%~10% volume and 0.2%~1.0% volume is merged, fully
Stirring obtains milk；
It is basic emulsus material with the milk, adds deionized water, emulsus material is 1 with the mass ratio of deionized water：0.5
~1:2.5, after being sufficiently stirred for, addition 1%~5% volume described in step one obtain okra refinishing polyose product, 0.1%~
Described in 1.0% volume step 2 obtain propolis clayey, described in 0.1%~1.0% volume step 3 obtain licorice,
The ginko leaves flavone and step 5 described in 0.1%~2.0% volume that step 4 described in 0.1%~1.0% volume is obtained are obtained
Fibroin albumen, obtain moisture-keeping nutrient ointment.
Okra Thick many candies in the step one contain 35%~40% galactolipin, 25%~30% rhamnose, 20%
~25% galacturonic acid and 3%~5% protein.
Can be added in the step 8 perilla herb oil of 1%~3% volume, the maize germ of 1%~3% volume, 1%~
The pine-seed oil of the wheat germ oil of 3% volume or 1%~3% volume, produces lip film, hand lotion or spats frost.
Emulsifying agent dispensing (single, double fatty acid glyceride 10%~40%, sucrose fatty ester 10%~30%, sorbose
Alcohol 10%~30%, polyglyceryl fatty acid ester 10%~20%, propane diols 3%~10%, potassium stearate 0.2%~1.0%),
The heat fusion of deionized water 20%~50% is added, is sufficiently stirred for, cooled down, be made emulsifiable paste standby.
It is 6~8 as basic emulsus material that above-mentioned emulsifiable paste is adjusted pH value, adds plus deionized water adjusts viscosity.Emulsifying agent base
Material：Plus deionized water=1：0.5~2.5, it is sufficiently stirred for standby.
In above-mentioned emulsifiable paste, nutritional ingredient is separately added into (okra polysaccharide 1%~5%, propolis 0.1%~1.0%, sweet
Careless extract 0.1%~1.0%, ginko leaves flavone 0.1%~1.0%, fibroin albumen 0.1%~2.0%) (it is emulsus material
Volume ratio after adding water), stir standby by colloid mill.
In above-mentioned colloid mill compound, can be according to product requirement characteristic and (purple with oil phase is optionally added respectively
Soviet Union's oil 1%~3%, maize germ 1%~3%, wheat germ oil 1%~3%, pine-seed oil 1%~3%).50 DEG C~55 DEG C of heating
Emulsifying, is cooled to normal temperature, packing, finished product.
Cosmetics of the invention, according to the different additive of addition, prepare serial edible moisture-keeping nutrient ointment.
It is prepared by embodiment 1, emulsifying agent base-material
Compound method：Emulsifying agent base-material is first prepared, after the mixture of above-mentioned dispensing is mixed, is stirred, emulsification is obtained
Agent base-material.Oil phase and water are mutually mixed respectively, and are heated to 80 DEG C, then water is added in oil phase with stirring, emulsification is uniform,
Be cooled to 30 DEG C~35 DEG C it is standby.
(1) embodiment 2, hand lotion is formulated
Compound method：In emulsifying agent base-material, deionized water is added, 30 DEG C~35 DEG C condition mixing are stirred by colloid mill,
Add perilla herb oil, spices, Preservative qs, emulsifying, finished product.
(2) embodiment 3, hand lotion is formulated
Compound method：In emulsifying agent base-material, add deionized water, 30 DEG C~35 DEG C conditions add okra polysaccharide, propolis,
Licorice mixes, and is stirred by colloid mill, adds maize germ, wheat germ oil, spices, Preservative qs, homogenized milk
Change, finished product.
(3) embodiment 4, hand lotion is formulated
Compound method：In emulsifying agent base-material, deionized water, 30 DEG C~35 DEG C conditions is added to add okra polysaccharide, propolis
Mixing, is stirred by colloid mill, adds pine-seed oil, spices, Preservative qs, emulsifying, finished product.
Embodiment 5, (colourless) lipstick formula
Compound method：In emulsifying agent base-material, deionized water, 30 DEG C~35 DEG C conditions is added to add okra polysaccharide, honeybee
Glue, ginko leaves flavone, fibroin albumen mixing, by colloid mill stir, add maize germ, wheat germ oil, spices, anti-corrosion
Appropriate agent, emulsifying, finished product.
Embodiment 6, foot moisturizing ointment formula
Compound method：In emulsifying agent base-material, add deionized water, 30 DEG C~35 DEG C conditions add okra polysaccharide, propolis,
Licorice mix, by colloid mill stir, add maize germ, wheat germ oil and perilla herb oil, pine-seed oil, spices,
Preservative qs, emulsifying, finished product.
Claims (4)
1. a kind of preparation method of edible moisture-keeping nutrient ointment, it is characterized in that：Comprise the following steps,
Step one, okra treatment
Take fresh okra pod to shred and stir, be beaten, the slurries of acquisition carry out centrifugation removal slurries after being extracted with water
Interior insoluble composition, obtains centrifugation solution；
Centrifugation solution is filtered, the ethanol solution for adding concentration to be 25%~50% is precipitated, it is 70% to obtain content
~80% okra viscose glue precipitation, by centrifugation, vacuum drying, obtains the okra jelly of brown；
Okra jelly is dissolved in cold water, dialysis 1 day~3 days is carried out in 15 times~25 times distilled water of volume, often
It changes liquid 3 times or 4 times, and freeze-drying obtains Thick many candies；Thick many candies are dissolved in distilled water, add tannic acid to remove deproteinized, added
Concentration is 15%~20%H202It is that concentrate after 0.5%~1% activated carbon is decolourized is splined on microcrystalline cellulose again with concentration
Plain post, adds distillation water elution, and volume ratio 1 is added after wash-out：4 water and ethanol is recrystallized, and white powder is obtained after drying
The okra refinishing polyose product of last shape；
The treatment of step 2, propolis
Take propolis raw material 10g~50g to crush, be put into 1000ml conical flasks, adding 95% ethanol solution to be put into ultrasonic wave makes
Its dissolving, then rinsed to propolis in ultrasonic wave with 95% ethanol solution and be completely dissolved, rotation will be again moved into after supernatant liquid filtering
Solution is evaporated in bottle, remaining liq is poured into evaporating dish, is put into vacuum drying chamber, and residual ethanol is removed completely, is obtained
Propolis clayey is standby；
It is prepared by step 3, licorice
Extracting liquorice is crushed, and is extracted using extraction and ultrasonic assistant method, is added in Radix Glycyrrhizae after being pulverized
Ethanol content is 40%~60% ethanol water, and Radix Glycyrrhizae is 1 with the volume ratio of ethanol water:15；At 40 DEG C~60 DEG C,
With ultrasonic power under the conditions of 75W~85W, to extract 1 hour, under these conditions, repeat 2 times or 3 times, obtain Radix Glycyrrhizae
Extract is standby；
The extraction of step 4, ginko leaves flavone
Ginkgo leaf is taken, using alcohol extraction procedure, ginkgo leaf is dried and 45 mesh~55 mesh, ginkgo leaf after being pulverized are crushed to
Middle to add the ethanol water that concentration of alcohol is 50%~70%, ginkgo leaf is 1 with the volume ratio of ethanol water:15；75
DEG C~85 DEG C under conditions of, extract 2h~4h, under these conditions, repeat 2 times or 3 times to activated carbon decolorizing, obtain silver
Apricot leaf flavone extract；
The preparation of step 5, fibroin albumen
Silk cocoon is taken, degumming operation is carried out, the macromolecular fibroin albumen obtained after degumming adds Na2CO3Solution is refined twice, refining
After end, CaCl is added2Dissolving fibroin, desalination degraded is carried out using the deionized water of flowing, obtains the polypeptide and ammonia of small molecule
Base acid；
It is prepared by step 6, perilla herb oil
Choosing purple perilla seed carries out selection by winnowing, magnetic separation, sieving and removal of impurities, is rinsed with circulating water, under conditions of 35 DEG C, carries out
Forced air drying, obtains purple perilla seed of the water content less than 8% standby；
Dried purple perilla seed is carried out into oil expression treatment, oil expression temperature is 40 DEG C~50 DEG C, and oil expression pressure is 2Mpa~10Mpa,
The perilla herb oil of acquisition carries out decolourizing and deodorization treatment again, obtains the excellent perilla herb oil of oil, and the residua content of purple perilla oil meal is 4%
~8%；
The preparation of step 7, pine-seed oil
Take pine nut to be screened by screening machine, soaked with clear water, and be polishing to that surface is totally smooth, at 90 DEG C~120 DEG C
Under the conditions of, boiling 30min~60min carries out sterilization treatment, and the pine nut after sterilizing manually strips SEMEN PINI KORAIENSIS；
By 1:1 ratio takes SEMEN PINI KORAIENSIS and No. 6 Extraction solvent oil, and 50 DEG C~55 DEG C of heating water bath leaches 40min, by mixture
Interior original solvent naphtha is released, and continuously adds No. 6 Extraction solvent oil equal with discharging amount, extracts 30min, then by mixture
Original solvent naphtha is released, and repeats aforesaid operations, extracts 20min；By by three mixtures of extraction, rotary evaporator is put into
Precipitation, at 75 DEG C~80 DEG C, pressure is 0.08MP~0.10MP to control temperature, obtains the pine-seed oil of concentration；
Under conditions of 5 DEG C~15 DEG C, alkali lye is added in the pine-seed oil of concentration, need to all be added in 5min~10min, added
During alkali lye, it is stirred with the speed of 60r/min, oil temperature is risen to 60 DEG C~65 DEG C in 30min, mixing speed is down to
30r/min, continues to stir 10min~20min, static 6h~8h, after removing the edible vegetable oil on upper strata, then adds pine nut weight of oil 10%
~15% water is cleaned；The charcoal absorption that pine-seed oil after cleaning adds pine nut weight of oil 1% is decolourized, 75 DEG C~
Under conditions of 85 DEG C, filtered after stirring 15min~20min；Under vacuum >=0.07MP and 85 DEG C~95 DEG C of constant temperature, dehydration
0.3h~0.6h；100 DEG C of steam 3h are passed through, 180 DEG C, under conditions of vacuum >=0.07MP are reached in pine nut oil temperature, carried out
Deodorization is refined, and adds the antioxidant tertiary butyl hydroquinone of pine nut weight of oil 0.02%, obtains pine-seed oil standby；
It is prepared by step 8, emulsifying agent
Take deionized water, the mono-fatty acid glyceride of 10%~40% volume or the diglycerine fatty acid of 20%~50% volume
Ester, the sucrose fatty ester of 10%~30% volume, the D-sorbite of 10%~30% volume, 10%~20% volume it is poly- sweet
The potassium stearate of oil and fat acid esters, the propane diols of 3%~10% volume and 0.2%~1.0% volume is merged, and is fully stirred
Mix acquisition milk；
It is basic emulsus material with the milk, adds deionized water, emulsus material is 1 with the mass ratio of deionized water：0.5~1:
2.5, after being sufficiently stirred for, okra refinishing polyose product, 0.1%~1.0% that step one described in 1%~5% volume of addition is obtained
Propolis clayey, licorice, 0.1% of step 3 acquisition described in 0.1%~1.0% volume that step 2 described in volume is obtained
The fibroin that the ginko leaves flavone and step 5 described in 0.1%~2.0% volume that step 4 described in~1.0% volume is obtained are obtained
Albumen, obtains moisture-keeping nutrient ointment.
2. the preparation method of a kind of edible moisture-keeping nutrient ointment according to claim 1, it is characterized in that：The step
Okra Thick many candies in one contain 35%~40% galactolipin, 25%~30% rhamnose, 20%~25% galacturonic acid
And 3%~5% protein.
3. the preparation method of a kind of edible moisture-keeping nutrient ointment according to claim 1, it is characterized in that：The step
Added in eight the perilla herb oil of 1%~3% volume, the maize germ of 1%~3% volume, the wheat germ oil of 1%~3% volume or
The pine-seed oil of 1%~3% volume, produces lip film, hand lotion or spats frost.
4. a kind of application of edible moisture-keeping nutrient ointment, it is characterized in that：The moisture-keeping nutrient that will be eaten described in claim 1
Ointment is used to produce lip film, hand lotion or spats frost.
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| CN105878057B (en) * | 2016-06-01 | 2019-01-08 | 宁波工程学院 | A kind of preparation method of food-grade hand lotion |
| CN106420540A (en) * | 2016-12-12 | 2017-02-22 | 紫花（广州）药业有限公司 | Ointment for relieving and moisturizing skins |
| CN108078063A (en) * | 2017-11-18 | 2018-05-29 | 肖本燕 | Okra pieces of old cloth or rags production method |
| CN108703930A (en) * | 2018-08-26 | 2018-10-26 | 福建乐伴护理用品有限公司 | A kind of moisturiser and preparation method thereof containing Abelmoschus Esculentus Linn extract |
| CN111732672B (en) * | 2020-07-22 | 2020-12-18 | 广东省生物工程研究所（广州甘蔗糖业研究所） | Okra polygalacturonic acid with uric acid reducing effect and preparation method and application thereof |
| CN116999484A (en) * | 2023-10-07 | 2023-11-07 | 云南英格生物技术有限公司 | Application of perilla seed oil meal extract in preparation of 5 alpha-reductase inhibitor |
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| CN101443364A (en) * | 2006-05-10 | 2009-05-27 | 博胡斯生物科技股份公司 | Pectic polysaccharides isolated from fruit pods of okra |
| CN102670467A (en) * | 2012-05-31 | 2012-09-19 | 南通恒隆化工有限公司 | Antibiosis hand cream |
| KR20130138550A (en) * | 2012-06-11 | 2013-12-19 | 한국콜마주식회사 | Cosmetic compositions for moisturizing lips |
| CN103816105A (en) * | 2014-03-12 | 2014-05-28 | 西南大学 | Complete multifunctional hand cream and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101443364A (en) * | 2006-05-10 | 2009-05-27 | 博胡斯生物科技股份公司 | Pectic polysaccharides isolated from fruit pods of okra |
| CN102670467A (en) * | 2012-05-31 | 2012-09-19 | 南通恒隆化工有限公司 | Antibiosis hand cream |
| KR20130138550A (en) * | 2012-06-11 | 2013-12-19 | 한국콜마주식회사 | Cosmetic compositions for moisturizing lips |
| CN103816105A (en) * | 2014-03-12 | 2014-05-28 | 西南大学 | Complete multifunctional hand cream and preparation method thereof |
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