CN104428344B - 生产聚醚多元醇的方法 - Google Patents

生产聚醚多元醇的方法 Download PDF

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Publication number
CN104428344B
CN104428344B CN201380028753.7A CN201380028753A CN104428344B CN 104428344 B CN104428344 B CN 104428344B CN 201380028753 A CN201380028753 A CN 201380028753A CN 104428344 B CN104428344 B CN 104428344B
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China
Prior art keywords
polyether polyol
water
polyol mixture
neutralized
mixture
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CN201380028753.7A
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Chinese (zh)
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CN104428344A (zh
Inventor
R·登希坦
P·A·特莫舒伊泽恩
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Huntsman International LLC
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Huntsman International LLC
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01Preparation of ethers
    • C07C41/34Separation; Purification; Stabilisation; Use of additives
    • C07C41/44Separation; Purification; Stabilisation; Use of additives by treatments giving rise to a chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01Preparation of ethers
    • C07C41/34Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30Post-polymerisation treatment, e.g. recovery, purification, drying

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN201380028753.7A 2012-05-29 2013-04-25 生产聚醚多元醇的方法 Active CN104428344B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12169832.8A EP2669312A1 (en) 2012-05-29 2012-05-29 Process for the production of polyether polyols
EP12169832.8 2012-05-29
PCT/EP2013/058599 WO2013178410A1 (en) 2012-05-29 2013-04-25 Process for the production of polyether polyols

Publications (2)

Publication Number Publication Date
CN104428344A CN104428344A (zh) 2015-03-18
CN104428344B true CN104428344B (zh) 2016-11-02

Family

ID=48227253

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380028753.7A Active CN104428344B (zh) 2012-05-29 2013-04-25 生产聚醚多元醇的方法

Country Status (7)

Country Link
US (1) US9353039B2 (enExample)
EP (2) EP2669312A1 (enExample)
CN (1) CN104428344B (enExample)
ES (1) ES2566330T3 (enExample)
IN (1) IN2014DN09290A (enExample)
RU (1) RU2625310C2 (enExample)
WO (1) WO2013178410A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10150837B2 (en) * 2016-06-23 2018-12-11 Covestro Llc Processes for removing water from a polyether polyol
WO2018005191A1 (en) * 2016-06-30 2018-01-04 Covestro Llc Processes and systems for removing water and salt from a neutralized polyether polyol
CN108341942B (zh) * 2017-01-22 2020-05-26 山东蓝星东大化工有限责任公司 用于碱金属催化合成的聚醚多元醇的精制方法
RU2751516C2 (ru) * 2017-01-25 2021-07-14 ХАНТСМЭН ИНТЕРНЭШНЛ ЭлЭлСи Способ получения полиэфирполиолов
CN109054012B (zh) * 2018-07-17 2020-12-01 上海邦高化学有限公司 一种聚乙二醇的合成工艺
CN109575268A (zh) * 2018-11-02 2019-04-05 佳化化学(滨州)有限公司 一种聚醚多元醇的精制方法及精制装置
CN110330640B (zh) * 2019-07-15 2022-02-18 万华化学集团股份有限公司 一种高分子量烃基封端聚醚的精制方法
US11572440B2 (en) 2020-02-18 2023-02-07 Covestro Llc Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content
CN114149578A (zh) * 2021-12-29 2022-03-08 滨化集团股份有限公司 一种聚醚多元醇中钾钠离子脱除方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0982341A2 (de) * 1998-08-21 2000-03-01 Basf Aktiengesellschaft Verfahren zur Herstellung von Polyetherpolyolen
WO2001088015A1 (en) * 2000-05-15 2001-11-22 Shell Internationale Research Maatschappij B.V. Process for the preparation of polyether polyols
WO2004000914A1 (de) * 2002-06-20 2003-12-31 Basf Aktiengesellschaft Verfahren zur aufarbeitung von polyetheralkoholen
WO2010145899A1 (en) * 2009-06-18 2010-12-23 Huntsman International Llc A process for neutralizing an unneutralised polyether polyol

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US3823145A (en) 1968-07-26 1974-07-09 Basf Wyandotte Corp Removal of impurities from polyols
US3582491A (en) 1969-06-12 1971-06-01 Wyandotte Chemicals Corp Removal of inorganic catalysts from polyols
US3715402A (en) 1969-08-08 1973-02-06 Basf Wyandotte Corp Removal of catalysts from polyols
BE795455A (fr) 1972-02-24 1973-08-16 Basf Ag Procede de preparation de polyalkylene-ethers purs
SU546627A1 (ru) * 1975-07-09 1977-02-15 Предприятие П/Я Г-4059 Способ очистки щелочных полиоксиалкиленполиолов
US4254287A (en) * 1979-07-05 1981-03-03 Conoco, Inc. Removal of catalyst from ethoxylates by centrifugation
DE3016113A1 (de) 1980-04-25 1981-10-29 Bayer Ag, 5090 Leverkusen Verfahren zur aufarbeitung von polyetherpolyolen
JPS5770124A (en) 1980-10-20 1982-04-30 Dai Ichi Kogyo Seiyaku Co Ltd Purification of polyether-polyol
DD155428B1 (de) 1980-12-18 1987-02-04 Renate Marquardt Verfahren zur stufenweisen reinigung von inhibitoren fuer die galvanotechnik
DE3229216A1 (de) 1982-08-05 1984-02-09 Basf Ag, 6700 Ludwigshafen Verfahren zur reinigung von rohen polyether-polyolen
US4985551A (en) 1988-12-29 1991-01-15 Basf Corporation Process for purification of catalysts from polyols using ion exchange resins
DE3907911A1 (de) * 1989-03-11 1990-09-13 Bayer Ag Verfahren zur entfernung von katalysatoren aus polyether-polyolen
JPH05111602A (ja) 1991-10-22 1993-05-07 Nikko Kyodo Co Ltd 晶析装置およびその方法
IS4687A (is) 1998-03-13 1998-04-06 Shell Internationale Research Maatschappij B.V. Aðferð við framleiðslu á lyktarlitlum pólýeter pólýólum
JP2009511449A (ja) 2005-10-06 2009-03-19 イナート・ファルマ 有機塩基のリン酸化抗原塩およびその結晶化方法
RU2008143136A (ru) * 2008-10-30 2010-05-10 Открытое акционерное общество "Нижнекамскнефтехим" (RU) Способ получения простых полиэфиров
BR112013015393A2 (pt) * 2010-12-20 2016-09-20 Bayer Ip Gmbh método para a preparação de poliéter polióis
CN102887996B (zh) * 2011-07-19 2016-03-16 因温斯特技术公司 聚醚多元醇过滤中的聚合物回收方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0982341A2 (de) * 1998-08-21 2000-03-01 Basf Aktiengesellschaft Verfahren zur Herstellung von Polyetherpolyolen
WO2001088015A1 (en) * 2000-05-15 2001-11-22 Shell Internationale Research Maatschappij B.V. Process for the preparation of polyether polyols
WO2004000914A1 (de) * 2002-06-20 2003-12-31 Basf Aktiengesellschaft Verfahren zur aufarbeitung von polyetheralkoholen
WO2010145899A1 (en) * 2009-06-18 2010-12-23 Huntsman International Llc A process for neutralizing an unneutralised polyether polyol

Also Published As

Publication number Publication date
EP2855559A1 (en) 2015-04-08
WO2013178410A1 (en) 2013-12-05
CN104428344A (zh) 2015-03-18
US20150133696A1 (en) 2015-05-14
RU2625310C2 (ru) 2017-07-13
US9353039B2 (en) 2016-05-31
EP2855559B1 (en) 2016-03-02
IN2014DN09290A (enExample) 2015-07-10
EP2669312A1 (en) 2013-12-04
RU2014153024A (ru) 2016-07-20
ES2566330T3 (es) 2016-04-12

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