CN103736994B - 一种化学镀镍溶液的处理方法 - Google Patents
一种化学镀镍溶液的处理方法 Download PDFInfo
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- CN103736994B CN103736994B CN201410016076.3A CN201410016076A CN103736994B CN 103736994 B CN103736994 B CN 103736994B CN 201410016076 A CN201410016076 A CN 201410016076A CN 103736994 B CN103736994 B CN 103736994B
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- nickel
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- 239000000126 substance Substances 0.000 title claims abstract description 78
- 238000007747 plating Methods 0.000 title claims abstract description 39
- 238000003672 processing method Methods 0.000 title claims abstract description 17
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 86
- 239000000843 powder Substances 0.000 claims abstract description 86
- 238000000034 method Methods 0.000 claims abstract description 58
- 239000007788 liquid Substances 0.000 claims abstract description 57
- 230000032683 aging Effects 0.000 claims abstract description 54
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 38
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 230000003647 oxidation Effects 0.000 claims abstract description 13
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 13
- 239000002244 precipitate Substances 0.000 claims abstract description 10
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 229910001379 sodium hypophosphite Inorganic materials 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 4
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000000243 solution Substances 0.000 claims description 82
- 239000000919 ceramic Substances 0.000 claims description 19
- 239000002994 raw material Substances 0.000 claims description 19
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 18
- 239000012670 alkaline solution Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 14
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 13
- 230000008021 deposition Effects 0.000 claims description 13
- 239000010865 sewage Substances 0.000 claims description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 8
- 229910001453 nickel ion Inorganic materials 0.000 claims description 8
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 8
- 229910001021 Ferroalloy Inorganic materials 0.000 claims description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 7
- 239000003337 fertilizer Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 239000013589 supplement Substances 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 4
- 230000008020 evaporation Effects 0.000 claims description 4
- 239000012528 membrane Substances 0.000 claims description 4
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 4
- 239000002686 phosphate fertilizer Substances 0.000 claims description 4
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 4
- 238000004663 powder metallurgy Methods 0.000 claims description 4
- 238000011084 recovery Methods 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 239000004408 titanium dioxide Substances 0.000 claims description 4
- 239000002351 wastewater Substances 0.000 claims description 4
- 239000011358 absorbing material Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 150000002500 ions Chemical class 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims 1
- 239000000292 calcium oxide Substances 0.000 claims 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims 1
- 229910052593 corundum Inorganic materials 0.000 claims 1
- 229910001845 yogo sapphire Inorganic materials 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 6
- 230000003197 catalytic effect Effects 0.000 description 7
- 206010070834 Sensitisation Diseases 0.000 description 6
- 230000004913 activation Effects 0.000 description 6
- 230000008313 sensitization Effects 0.000 description 6
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 238000006385 ozonation reaction Methods 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 3
- 229910001096 P alloy Inorganic materials 0.000 description 3
- 235000011941 Tilia x europaea Nutrition 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- -1 conduction Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000004571 lime Substances 0.000 description 3
- OFNHPGDEEMZPFG-UHFFFAOYSA-N phosphanylidynenickel Chemical compound [P].[Ni] OFNHPGDEEMZPFG-UHFFFAOYSA-N 0.000 description 3
- 229910000640 Fe alloy Inorganic materials 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000909 electrodialysis Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000008204 material by function Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 230000002085 persistent effect Effects 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- NCPXQVVMIXIKTN-UHFFFAOYSA-N trisodium;phosphite Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])[O-] NCPXQVVMIXIKTN-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- UGKDIUIOSMUOAW-UHFFFAOYSA-N iron nickel Chemical compound [Fe].[Ni] UGKDIUIOSMUOAW-UHFFFAOYSA-N 0.000 description 1
- 230000013016 learning Effects 0.000 description 1
- 239000010808 liquid waste Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 1
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- ACVYVLVWPXVTIT-UHFFFAOYSA-M phosphinate Chemical compound [O-][PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-M 0.000 description 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical group OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/17—Metallic particles coated with metal
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/18—Non-metallic particles coated with metal
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- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/021—After-treatment of oxides or hydroxides
-
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
- C02F1/004—Processes for the treatment of water whereby the filtration technique is of importance using large scale industrial sized filters
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- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/02—Treatment of water, waste water, or sewage by heating
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- C23C18/1851—Pretreatment of the material to be coated of surfaces of non-metallic or semiconducting in organic material
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KR1020167022034A KR101737292B1 (ko) | 2014-01-15 | 2015-01-08 | 화학 니켈 도금액의 처리 방법 |
PCT/CN2015/070347 WO2015106649A1 (zh) | 2014-01-15 | 2015-01-08 | 一种化学镀镍溶液的处理方法 |
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CN103736994B (zh) * | 2014-01-15 | 2015-11-18 | 南京德磊科技有限公司 | 一种化学镀镍溶液的处理方法 |
CN106045123B (zh) * | 2016-07-15 | 2019-03-08 | 苏州市东方环境工程有限公司 | 一种化学镍废液的资源化零排放回收工艺方法 |
CN107604346A (zh) * | 2017-09-06 | 2018-01-19 | 中航沈飞民用飞机有限责任公司 | 一种化学转化溶液的老化方法及新配制的化学转化溶液对金属板材的处理方法 |
CN109097807A (zh) * | 2018-07-27 | 2018-12-28 | 佛山市三水雄鹰铝表面技术创新中心有限公司 | 单镍盐着色回收封孔剂与中水利用的方法 |
CN111333152A (zh) * | 2019-04-11 | 2020-06-26 | 西南科技大学 | 一种电解氧化处理高浓度含镍含磷有机废液的方法 |
CN112158978B (zh) * | 2020-09-14 | 2021-08-10 | 浙江海拓环境技术有限公司 | 一种化学镀镍废液中次磷酸盐的处理方法 |
CN112251741A (zh) * | 2020-11-13 | 2021-01-22 | 北京曙光航空电气有限责任公司 | 一种镀镍膜修复液调制及修复方法 |
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CN101089225A (zh) * | 2006-06-16 | 2007-12-19 | 汉达精密电子(昆山)有限公司 | 化学镀镍老化液回收处理工艺 |
WO2008130080A1 (en) * | 2007-04-23 | 2008-10-30 | Hanwha Chemical Corporation | Manufacturing method of conductive electroless plating powder |
CN101805831A (zh) * | 2010-03-24 | 2010-08-18 | 埃梯星(厦门)电子科技有限公司 | 一种在碱性化学镀镍废液中直接提取镍的方法 |
CN101927343A (zh) * | 2010-08-09 | 2010-12-29 | 山东天诺光电材料有限公司 | 一种镀镍铝粉及其制备方法和用途 |
CN102452743A (zh) * | 2010-10-25 | 2012-05-16 | 上海丰信环保科技有限公司 | 含络合物镀镍废水的处理方法 |
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JPS59182961A (ja) * | 1983-03-31 | 1984-10-17 | Agency Of Ind Science & Technol | 金属皮膜を有する無機粉体の製造方法 |
JPS61276979A (ja) * | 1985-05-30 | 1986-12-06 | Nippon Chem Ind Co Ltd:The | ニッケルめっき材料の製造法 |
JP3180977B2 (ja) * | 1992-08-27 | 2001-07-03 | 日本化学工業株式会社 | 無電解めっき老化液の処理方法 |
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JP4405281B2 (ja) * | 2004-02-18 | 2010-01-27 | 株式会社アステック入江 | 無電解ニッケルめっき廃液の再資源化処理方法 |
JP4637649B2 (ja) | 2005-05-30 | 2011-02-23 | 株式会社神戸製鋼所 | 浄化用鉄系粉末 |
CN102616961A (zh) * | 2012-03-29 | 2012-08-01 | 李朝林 | 一种降解化学镀镍废液中有机污染物并回收磷酸盐的方法 |
CN103484927A (zh) * | 2013-10-08 | 2014-01-01 | 昆山纯柏精密五金有限公司 | 一种电镀镍废液的处理方法 |
CN103736994B (zh) * | 2014-01-15 | 2015-11-18 | 南京德磊科技有限公司 | 一种化学镀镍溶液的处理方法 |
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CN101089225A (zh) * | 2006-06-16 | 2007-12-19 | 汉达精密电子(昆山)有限公司 | 化学镀镍老化液回收处理工艺 |
WO2008130080A1 (en) * | 2007-04-23 | 2008-10-30 | Hanwha Chemical Corporation | Manufacturing method of conductive electroless plating powder |
CN101805831A (zh) * | 2010-03-24 | 2010-08-18 | 埃梯星(厦门)电子科技有限公司 | 一种在碱性化学镀镍废液中直接提取镍的方法 |
CN101927343A (zh) * | 2010-08-09 | 2010-12-29 | 山东天诺光电材料有限公司 | 一种镀镍铝粉及其制备方法和用途 |
CN102452743A (zh) * | 2010-10-25 | 2012-05-16 | 上海丰信环保科技有限公司 | 含络合物镀镍废水的处理方法 |
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