CN102378776B - 制备聚合物的方法以及用于实施所述方法的反应器 - Google Patents

制备聚合物的方法以及用于实施所述方法的反应器 Download PDF

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Publication number
CN102378776B
CN102378776B CN2010800150259A CN201080015025A CN102378776B CN 102378776 B CN102378776 B CN 102378776B CN 2010800150259 A CN2010800150259 A CN 2010800150259A CN 201080015025 A CN201080015025 A CN 201080015025A CN 102378776 B CN102378776 B CN 102378776B
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China
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liquid phase
droplets
continuous liquid
reactor
monomers
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Expired - Fee Related
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Chinese (zh)
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CN102378776A (zh
Inventor
M·阿布德
P·德斯保斯
N·葛玛勒
H·罗马
T·克雷布斯
D·勒施
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/01—Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00—Making granules
    • B29B9/10—Making granules by moulding the material, i.e. treating it in the molten state
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/14—Organic medium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams
    • C08G69/16—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Polymerisation Methods In General (AREA)
  • Polyamides (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
CN2010800150259A 2009-02-02 2010-02-01 制备聚合物的方法以及用于实施所述方法的反应器 Expired - Fee Related CN102378776B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
EP09151847.2 2009-02-02
EP09151847 2009-02-02
EP091518472 2009-02-02
PCT/EP2010/051146 WO2010086433A1 (de) 2009-02-02 2010-02-01 Verfahren zur herstellung von polymeren sowie reaktor zur durchführung des verfahrens

Publications (2)

Publication Number Publication Date
CN102378776A CN102378776A (zh) 2012-03-14
CN102378776B true CN102378776B (zh) 2013-10-30

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CN2010800150259A Expired - Fee Related CN102378776B (zh) 2009-02-02 2010-02-01 制备聚合物的方法以及用于实施所述方法的反应器

Country Status (7)

Country Link
US (2) US8883939B2 (enExample)
EP (1) EP2391668B1 (enExample)
JP (1) JP5677979B2 (enExample)
KR (1) KR101640272B1 (enExample)
CN (1) CN102378776B (enExample)
ES (1) ES2637548T3 (enExample)
WO (1) WO2010086433A1 (enExample)

Families Citing this family (17)

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JP5709890B2 (ja) 2009-12-08 2015-04-30 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ポリアミドの製造方法
WO2011089130A2 (de) 2010-01-19 2011-07-28 Basf Se Verfahren zur herstellung von hohlkörpern mit eingeschlossenen frei beweglichen partikeln
EP2789641B1 (de) * 2010-10-07 2020-03-11 Basf Se Verfahren zur Herstellung von Monomer-Zusammensetzungen und deren Verwendung zur Herstellung eines Polyamid-Formteils
US9139692B2 (en) 2010-12-03 2015-09-22 Basf Se Process for polymerizing lactam
EP2460838A1 (de) 2010-12-03 2012-06-06 Basf Se Verfahren zur Polymerisation von Lactam
CA2919320C (en) 2013-07-31 2019-02-26 Basf Se Reverse-phase polymerisation process
KR101863463B1 (ko) 2013-07-31 2018-05-31 바스프 에스이 역상 중합 방법
RU2630696C2 (ru) 2013-07-31 2017-09-12 Басф Се Способ полимеризации с обращенной фазой
CN106573213B (zh) * 2014-06-23 2019-11-08 巴斯夫欧洲公司 将单体溶液的液滴分散到反应器中的装置
CN106573217B (zh) * 2014-06-23 2019-08-06 巴斯夫欧洲公司 用于将单体溶液的微滴引入到反应器内的设备
EP3265221B1 (de) * 2015-03-02 2019-01-30 Basf Se Vorrichtung zur herstellung von pulverförmigem poly(meth)acrylat
JP6882188B2 (ja) * 2015-04-08 2021-06-02 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ 反応器に液滴を導入するための装置
CN106046341A (zh) * 2016-07-19 2016-10-26 辽宁科技学院 一种用于增粘剂的聚氧富烯基醇醚及其制备装置
CN108970566B (zh) * 2018-08-17 2021-03-09 北京濮源新材料技术研究院(普通合伙) 用于生产聚碳酸酯的具有浸润性能的缩聚反应器
CN110606905A (zh) * 2019-09-16 2019-12-24 北京泽阳天成化工技术有限公司 聚丙烯生产工艺及生产装置
CN110813204B (zh) * 2019-11-28 2021-09-21 齐鲁理工学院 一种用于液相接触的生物化工反应容器
CN119081103B (zh) * 2024-09-18 2026-03-17 北京三联虹普新合纤技术服务股份有限公司 一种回收己内酰胺单体连续生产消光锦纶6的方法

Citations (3)

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Publication number Priority date Publication date Assignee Title
DE3009812A1 (de) * 1980-03-14 1981-09-24 Peter Dr. 5630 Remscheid Melchior Verfahren zur herstellung von perlen
US4623706A (en) * 1984-08-23 1986-11-18 The Dow Chemical Company Process for preparing uniformly sized polymer particles by suspension polymerization of vibratorily excited monomers in a gaseous or liquid stream
EP0243177A1 (en) * 1986-04-23 1987-10-28 Sumitomo Chemical Company, Limited Catalytic production of polyamide block copolymers

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NL280053A (enExample) * 1961-06-30 1900-01-01
US3922255A (en) * 1972-05-15 1975-11-25 Rohm & Haas Method of producing uniform polymer beads
CA1166413A (en) * 1980-10-30 1984-05-01 Edward E. Timm Process and apparatus for preparing uniform size polymer beads
US4487898A (en) * 1981-06-12 1984-12-11 Kanegafuchi Chemical Industry Co., Ltd. Process of continuous suspension polymerization
JP3176607B2 (ja) * 1990-02-07 2001-06-18 群馬大学長 均一な液滴の形成方法
US5269980A (en) 1991-08-05 1993-12-14 Northeastern University Production of polymer particles in powder form using an atomization technique
JP2001520526A (ja) * 1998-02-11 2001-10-30 トランスクラニア・ソシエダッド・アノニマ 粒状製品を得るための方法および該方法を行うための装置
JP2004525990A (ja) * 2000-09-21 2004-08-26 メルク　パテント　ゲゼルシャフト　ミット　ベシュレンクテル　ハフトング ポリスチレンのミクロスフェアとその製造方法
JP2008095115A (ja) * 2001-06-22 2008-04-24 Sekisui Chem Co Ltd 樹脂微粒子の製造方法、樹脂微粒子及び樹脂微粒子の製造装置
US6610798B1 (en) * 2002-10-08 2003-08-26 Nova Chemical Inc. Controlled suspension polymerization process without mechanical agitation
US7727555B2 (en) * 2005-03-02 2010-06-01 Boston Scientific Scimed, Inc. Particles
DE102005053559A1 (de) * 2005-11-08 2007-05-10 Basf Ag Verfahren zur Herstellung von Vinylformamid-Einheiten enthaltenden Polymerpulvern
US20090281272A1 (en) * 2005-12-07 2009-11-12 Mip Technologies Ab Monodisperse Molecularly Imprinted Polymer Beads
JP2008081639A (ja) * 2006-09-28 2008-04-10 Konica Minolta Business Technologies Inc 静電荷像現像用トナー、樹脂粒子、及び、樹脂微粒子重合装置

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3009812A1 (de) * 1980-03-14 1981-09-24 Peter Dr. 5630 Remscheid Melchior Verfahren zur herstellung von perlen
US4623706A (en) * 1984-08-23 1986-11-18 The Dow Chemical Company Process for preparing uniformly sized polymer particles by suspension polymerization of vibratorily excited monomers in a gaseous or liquid stream
EP0243177A1 (en) * 1986-04-23 1987-10-28 Sumitomo Chemical Company, Limited Catalytic production of polyamide block copolymers

Also Published As

Publication number Publication date
EP2391668A1 (de) 2011-12-07
US8883939B2 (en) 2014-11-11
EP2391668B1 (de) 2017-05-17
KR20110127173A (ko) 2011-11-24
US20110294968A1 (en) 2011-12-01
JP5677979B2 (ja) 2015-02-25
WO2010086433A1 (de) 2010-08-05
JP2012516901A (ja) 2012-07-26
ES2637548T3 (es) 2017-10-13
KR101640272B1 (ko) 2016-07-15
US20150038656A1 (en) 2015-02-05
CN102378776A (zh) 2012-03-14

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