ES2637548T3 - Procedimiento para la preparación de polímeros así como reactor para la realización del procedimiento - Google Patents

Procedimiento para la preparación de polímeros así como reactor para la realización del procedimiento Download PDF

Info

Publication number
ES2637548T3
ES2637548T3 ES10701553.9T ES10701553T ES2637548T3 ES 2637548 T3 ES2637548 T3 ES 2637548T3 ES 10701553 T ES10701553 T ES 10701553T ES 2637548 T3 ES2637548 T3 ES 2637548T3
Authority
ES
Spain
Prior art keywords
monomers
drops
liquid phase
oligomers
continuous liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES10701553.9T
Other languages
English (en)
Spanish (es)
Inventor
Mohammed Abboud
Philippe Desbois
Norbert GMÄHLE
Herbert RÖMER
Thilo Krebs
Dennis LÖSCH
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2637548T3 publication Critical patent/ES2637548T3/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/01Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/10Making granules by moulding the material, i.e. treating it in the molten state
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/12Polymerisation in non-solvents
    • C08F2/14Organic medium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04Preparatory processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14Lactams
    • C08G69/16Preparatory processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00027Process aspects
    • B01J2219/00033Continuous processes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Polymerisation Methods In General (AREA)
  • Polyamides (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
ES10701553.9T 2009-02-02 2010-02-01 Procedimiento para la preparación de polímeros así como reactor para la realización del procedimiento Active ES2637548T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09151847 2009-02-02
EP09151847 2009-02-02
PCT/EP2010/051146 WO2010086433A1 (de) 2009-02-02 2010-02-01 Verfahren zur herstellung von polymeren sowie reaktor zur durchführung des verfahrens

Publications (1)

Publication Number Publication Date
ES2637548T3 true ES2637548T3 (es) 2017-10-13

Family

ID=41716688

Family Applications (1)

Application Number Title Priority Date Filing Date
ES10701553.9T Active ES2637548T3 (es) 2009-02-02 2010-02-01 Procedimiento para la preparación de polímeros así como reactor para la realización del procedimiento

Country Status (7)

Country Link
US (2) US8883939B2 (enExample)
EP (1) EP2391668B1 (enExample)
JP (1) JP5677979B2 (enExample)
KR (1) KR101640272B1 (enExample)
CN (1) CN102378776B (enExample)
ES (1) ES2637548T3 (enExample)
WO (1) WO2010086433A1 (enExample)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5709890B2 (ja) 2009-12-08 2015-04-30 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ポリアミドの製造方法
WO2011089130A2 (de) 2010-01-19 2011-07-28 Basf Se Verfahren zur herstellung von hohlkörpern mit eingeschlossenen frei beweglichen partikeln
EP2789641B1 (de) * 2010-10-07 2020-03-11 Basf Se Verfahren zur Herstellung von Monomer-Zusammensetzungen und deren Verwendung zur Herstellung eines Polyamid-Formteils
US9139692B2 (en) 2010-12-03 2015-09-22 Basf Se Process for polymerizing lactam
EP2460838A1 (de) 2010-12-03 2012-06-06 Basf Se Verfahren zur Polymerisation von Lactam
CA2919320C (en) 2013-07-31 2019-02-26 Basf Se Reverse-phase polymerisation process
KR101863463B1 (ko) 2013-07-31 2018-05-31 바스프 에스이 역상 중합 방법
RU2630696C2 (ru) 2013-07-31 2017-09-12 Басф Се Способ полимеризации с обращенной фазой
CN106573213B (zh) * 2014-06-23 2019-11-08 巴斯夫欧洲公司 将单体溶液的液滴分散到反应器中的装置
CN106573217B (zh) * 2014-06-23 2019-08-06 巴斯夫欧洲公司 用于将单体溶液的微滴引入到反应器内的设备
EP3265221B1 (de) * 2015-03-02 2019-01-30 Basf Se Vorrichtung zur herstellung von pulverförmigem poly(meth)acrylat
JP6882188B2 (ja) * 2015-04-08 2021-06-02 ビーエイエスエフ・ソシエタス・エウロパエアBasf Se 反応器に液滴を導入するための装置
CN106046341A (zh) * 2016-07-19 2016-10-26 辽宁科技学院 一种用于增粘剂的聚氧富烯基醇醚及其制备装置
CN108970566B (zh) * 2018-08-17 2021-03-09 北京濮源新材料技术研究院(普通合伙) 用于生产聚碳酸酯的具有浸润性能的缩聚反应器
CN110606905A (zh) * 2019-09-16 2019-12-24 北京泽阳天成化工技术有限公司 聚丙烯生产工艺及生产装置
CN110813204B (zh) * 2019-11-28 2021-09-21 齐鲁理工学院 一种用于液相接触的生物化工反应容器
CN119081103B (zh) * 2024-09-18 2026-03-17 北京三联虹普新合纤技术服务股份有限公司 一种回收己内酰胺单体连续生产消光锦纶6的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL280053A (enExample) * 1961-06-30 1900-01-01
US3922255A (en) * 1972-05-15 1975-11-25 Rohm & Haas Method of producing uniform polymer beads
DE3009812C2 (de) * 1980-03-14 1986-06-26 Peter Dr. 5630 Remscheid Melchior Verfahren zur Herstellung von Perlen aus Polymethacrylat
CA1166413A (en) * 1980-10-30 1984-05-01 Edward E. Timm Process and apparatus for preparing uniform size polymer beads
US4487898A (en) * 1981-06-12 1984-12-11 Kanegafuchi Chemical Industry Co., Ltd. Process of continuous suspension polymerization
US4623706A (en) * 1984-08-23 1986-11-18 The Dow Chemical Company Process for preparing uniformly sized polymer particles by suspension polymerization of vibratorily excited monomers in a gaseous or liquid stream
DE3786415T2 (de) * 1986-04-23 1993-10-21 Sumitomo Chemical Co Katalytische Herstellung von Polyamidblockcopolymeren.
JP3176607B2 (ja) * 1990-02-07 2001-06-18 群馬大学長 均一な液滴の形成方法
US5269980A (en) 1991-08-05 1993-12-14 Northeastern University Production of polymer particles in powder form using an atomization technique
JP2001520526A (ja) * 1998-02-11 2001-10-30 トランスクラニア・ソシエダッド・アノニマ 粒状製品を得るための方法および該方法を行うための装置
JP2004525990A (ja) * 2000-09-21 2004-08-26 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング ポリスチレンのミクロスフェアとその製造方法
JP2008095115A (ja) * 2001-06-22 2008-04-24 Sekisui Chem Co Ltd 樹脂微粒子の製造方法、樹脂微粒子及び樹脂微粒子の製造装置
US6610798B1 (en) * 2002-10-08 2003-08-26 Nova Chemical Inc. Controlled suspension polymerization process without mechanical agitation
US7727555B2 (en) * 2005-03-02 2010-06-01 Boston Scientific Scimed, Inc. Particles
DE102005053559A1 (de) * 2005-11-08 2007-05-10 Basf Ag Verfahren zur Herstellung von Vinylformamid-Einheiten enthaltenden Polymerpulvern
US20090281272A1 (en) * 2005-12-07 2009-11-12 Mip Technologies Ab Monodisperse Molecularly Imprinted Polymer Beads
JP2008081639A (ja) * 2006-09-28 2008-04-10 Konica Minolta Business Technologies Inc 静電荷像現像用トナー、樹脂粒子、及び、樹脂微粒子重合装置

Also Published As

Publication number Publication date
EP2391668A1 (de) 2011-12-07
US8883939B2 (en) 2014-11-11
EP2391668B1 (de) 2017-05-17
KR20110127173A (ko) 2011-11-24
US20110294968A1 (en) 2011-12-01
JP5677979B2 (ja) 2015-02-25
WO2010086433A1 (de) 2010-08-05
JP2012516901A (ja) 2012-07-26
CN102378776B (zh) 2013-10-30
KR101640272B1 (ko) 2016-07-15
US20150038656A1 (en) 2015-02-05
CN102378776A (zh) 2012-03-14

Similar Documents

Publication Publication Date Title
CN102378776B (zh) 制备聚合物的方法以及用于实施所述方法的反应器
JP5659156B2 (ja) 多成分粒子生成システム
US8826848B2 (en) Multi component particle generating system
US20240050914A1 (en) Method for Generating Solid Capsules
KR101658375B1 (ko) 현탁 중합에 의해 균일한 입자 크기의 중합체 비드를 제조하는 방법 및 장치
WO2021023041A1 (zh) 非球形水凝胶微粒栓塞剂的制备方法
KR101725508B1 (ko) 헥사나이트로스틸벤 입자의 제조 방법과 그 장치
JP2019508233A (ja) エマルションを調製する方法
JP7050877B2 (ja) 粉末状ポリ(メタ)アクリレートを製造するための装置
Chafidz et al. Formation of fine particles using supercritical fluid (SCF) process: Short review
Lee et al. Fabrication of kinetically stable micropolymofoam particles and the spontaneous induction of morphological transformation
JP2004250630A (ja) 疎水性液滴の製造方法、ポリマービーズの製造方法及び製造装置、並びにイオン交換樹脂の製造方法
US20170246607A1 (en) Apparatus for Production of Pulverulent Poly(Meth)Acrylate
EP2213366A1 (en) Multi component particle generating system
Meng et al. A Practical Guide to Microparticle Fabrication: A Comprehensive Illustrated and Updated Review
JPS61252202A (ja) 均一な球状重合体の製造方法
KR102686942B9 (ko) 용매 제거 장치 및 이를 이용한 미소구체 제조 방법
Cha et al. Simultaneous size control of microcapsule and its nanopores using polymer concentration
Liu et al. Using a CD-like microfluidic platform for uniform calcium alginate drug carrier generation
CN109772240A (zh) 一种用于将液体物料产生微滴的转盘装置及用于制造微球的设备
SU686746A1 (ru) Аппарат дл гранулировани расплавов