CN102084038B - 硅或活性金属的直接铸造 - Google Patents
硅或活性金属的直接铸造 Download PDFInfo
- Publication number
- CN102084038B CN102084038B CN2009801187328A CN200980118732A CN102084038B CN 102084038 B CN102084038 B CN 102084038B CN 2009801187328 A CN2009801187328 A CN 2009801187328A CN 200980118732 A CN200980118732 A CN 200980118732A CN 102084038 B CN102084038 B CN 102084038B
- Authority
- CN
- China
- Prior art keywords
- silicon
- reaction chamber
- containing gas
- liquid
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/06—Silicon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
- C30B11/04—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method adding crystallising materials or reactants forming it in situ to the melt
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12884708P | 2008-05-23 | 2008-05-23 | |
| US61/128,847 | 2008-05-23 | ||
| US12/378,243 US20090289390A1 (en) | 2008-05-23 | 2009-02-11 | Direct silicon or reactive metal casting |
| US12/378,243 | 2009-02-11 | ||
| PCT/US2009/044704 WO2009143264A2 (en) | 2008-05-23 | 2009-05-20 | Direct silicon or reactive metal casting |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102084038A CN102084038A (zh) | 2011-06-01 |
| CN102084038B true CN102084038B (zh) | 2013-12-11 |
Family
ID=41340860
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009801187328A Expired - Fee Related CN102084038B (zh) | 2008-05-23 | 2009-05-20 | 硅或活性金属的直接铸造 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20090289390A1 (enExample) |
| EP (1) | EP2291552A4 (enExample) |
| JP (1) | JP2011521874A (enExample) |
| KR (1) | KR20110030482A (enExample) |
| CN (1) | CN102084038B (enExample) |
| CA (1) | CA2725104A1 (enExample) |
| TW (1) | TW201009139A (enExample) |
| WO (1) | WO2009143264A2 (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100189926A1 (en) * | 2006-04-14 | 2010-07-29 | Deluca Charles | Plasma deposition apparatus and method for making high purity silicon |
| US20100047148A1 (en) * | 2008-05-23 | 2010-02-25 | Rec Silicon, Inc. | Skull reactor |
| CN102498062A (zh) * | 2009-04-29 | 2012-06-13 | 卡利太阳能有限公司 | 升级冶金级硅材料提纯的过程控制 |
| WO2011079485A1 (zh) * | 2009-12-31 | 2011-07-07 | 江苏中能硅业科技发展有限公司 | 硅单质的生产方法及生产设备 |
| DE102010011853A1 (de) * | 2010-03-09 | 2011-09-15 | Schmid Silicon Technology Gmbh | Verfahren zur Herstellung von hochreinem Silizium |
| EP2558232B1 (de) * | 2010-04-13 | 2017-07-12 | Schmid Silicon Technology GmbH | Herstellung von monokristallinen halbleiterwerkstoffen |
| DE102010021004A1 (de) * | 2010-05-14 | 2011-11-17 | Schmid Silicon Technology Gmbh | Herstellung von monokristallinen Halbleiterwerkstoffen |
| DE102010015354A1 (de) * | 2010-04-13 | 2011-10-13 | Schmid Silicon Technology Gmbh | Herstellung eines kristallinen Halbleiterwerkstoffs |
| DE102010045040A1 (de) * | 2010-09-10 | 2012-03-15 | Centrotherm Sitec Gmbh | Verfahren und Vorrichtung zum Herstellen von Silizium |
| US20120082610A1 (en) * | 2010-10-02 | 2012-04-05 | Channon Matthew J | Fluorspar/Iodide process for reduction,purificatioin, and crystallization of silicon |
| KR101339481B1 (ko) * | 2011-08-05 | 2013-12-10 | 주식회사 글로실 | 단결정 실리콘 웨이퍼 원료 제조를 위한 다결정 실리콘 로드 제조방법 |
| CN104583122B (zh) * | 2012-08-29 | 2017-09-05 | 赫姆洛克半导体运营有限责任公司 | 锥形流化床反应器及其使用方法 |
| CN103626184B (zh) * | 2013-07-31 | 2016-02-24 | 浙江精功新材料技术有限公司 | 一种高纯液体多晶硅的制备方法 |
| CN106365169A (zh) * | 2016-08-24 | 2017-02-01 | 上海交通大学 | 一种由硅烷直接铸造多晶硅锭的设备及方法 |
| CN106319618A (zh) * | 2016-09-22 | 2017-01-11 | 上海交通大学 | 一种由硅烷制造直拉单晶硅棒的设备及方法 |
| DE102019209898A1 (de) * | 2019-07-04 | 2021-01-07 | Schmid Silicon Technology Gmbh | Vorrichtung und Verfahren zur Bildung von flüssigem Silizium |
| DE102019211921A1 (de) * | 2019-08-08 | 2021-02-11 | Schmid Silicon Technology Gmbh | Verfahren und Vorrichtung zur Erzeugung siliziumhaltiger Materialien |
| CN112893789B (zh) * | 2021-01-15 | 2022-08-30 | 台州学院 | 一种用于生产半导体材料箔的装置及方法 |
| CN113415805B (zh) * | 2021-06-16 | 2022-03-29 | 何良雨 | 一种激光维持等离子体制备多晶硅的方法及系统 |
| EP4479582A1 (en) * | 2022-02-15 | 2024-12-25 | Lau Superconductors Inc. | Manufacture and repair of high temperature reinforced superconductors |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4188368A (en) * | 1978-03-29 | 1980-02-12 | Nasa | Method of producing silicon |
| US4343772A (en) * | 1980-02-29 | 1982-08-10 | Nasa | Thermal reactor |
| US5961944A (en) * | 1996-10-14 | 1999-10-05 | Kawasaki Steel Corporation | Process and apparatus for manufacturing polycrystalline silicon, and process for manufacturing silicon wafer for solar cell |
| US20030150374A1 (en) * | 2000-12-28 | 2003-08-14 | Kenichi Sasatani | Silicon continuous casting method |
Family Cites Families (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4049384A (en) * | 1975-04-14 | 1977-09-20 | Arthur D. Little, Inc. | Cold crucible system |
| US4102765A (en) * | 1977-01-06 | 1978-07-25 | Westinghouse Electric Corp. | Arc heater production of silicon involving alkali or alkaline-earth metals |
| US4212343A (en) * | 1979-03-16 | 1980-07-15 | Allied Chemical Corporation | Continuous casting method and apparatus for structurally defined metallic strips |
| DE3016807A1 (de) * | 1980-05-02 | 1981-11-05 | Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt | Verfahren zur herstellung von silizium |
| US4274473A (en) * | 1980-01-14 | 1981-06-23 | Allied Chemical Corporation | Contour control for planar flow casting of metal ribbon |
| CA1147698A (en) * | 1980-10-15 | 1983-06-07 | Maher I. Boulos | Purification of metallurgical grade silicon |
| JPS59501109A (ja) * | 1982-06-22 | 1984-06-28 | エシルコ−ポレ−シヨン | ソ−ラ−グレ−ドの珪素を製造するための装置と方法 |
| DE3419137A1 (de) * | 1984-05-23 | 1985-11-28 | Bayer Ag, 5090 Leverkusen | Verfahren und vorrichtung zur herstellung von halbleiterfolien |
| DE3629231A1 (de) * | 1986-08-28 | 1988-03-03 | Heliotronic Gmbh | Verfahren zum aufschmelzen von in einen schmelztiegel chargiertem siliciumpulver und schmelztiegel zur durchfuehrung des verfahrens |
| US4936375A (en) * | 1988-10-13 | 1990-06-26 | Axel Johnson Metals, Inc. | Continuous casting of ingots |
| DE4228402C2 (de) * | 1992-08-26 | 2000-08-03 | Ald Vacuum Techn Ag | Zur Atmosphäre hin abgeschlossene Induktionsschmelzvorrichtung |
| DE4320766C2 (de) * | 1993-06-23 | 2002-06-27 | Ald Vacuum Techn Ag | Vorrichtung zum Einschmelzen einer festen Schicht aus elektrisch leitfähigem Material |
| DE19607805C1 (de) * | 1996-03-01 | 1997-07-17 | Ald Vacuum Techn Gmbh | Verfahren und Vorrichtung zum Schmelzen und Gießen von Metallen in Formen |
| US5842511A (en) * | 1996-08-19 | 1998-12-01 | Alliedsignal Inc. | Casting wheel having equiaxed fine grain quench surface |
| FR2772741B1 (fr) * | 1997-12-19 | 2000-03-10 | Centre Nat Rech Scient | Procede et installation d'affinage du silicium |
| US6468886B2 (en) * | 1999-06-15 | 2002-10-22 | Midwest Research Institute | Purification and deposition of silicon by an iodide disproportionation reaction |
| JP3646570B2 (ja) * | 1999-07-01 | 2005-05-11 | 三菱住友シリコン株式会社 | シリコン連続鋳造方法 |
| US6960537B2 (en) * | 2001-10-02 | 2005-11-01 | Asm America, Inc. | Incorporation of nitrogen into high k dielectric film |
| US6926876B2 (en) * | 2002-01-17 | 2005-08-09 | Paul V. Kelsey | Plasma production of polycrystalline silicon |
| US7082986B2 (en) * | 2002-02-08 | 2006-08-01 | Cornell Research Foundation, Inc. | System and method for continuous casting of a molten material |
| US7175685B1 (en) * | 2002-04-15 | 2007-02-13 | Gt Solar Incorporated | Dry conversion of high purity ultrafine silicon powder to densified pellet form for silicon melting applications |
| RU2213792C1 (ru) * | 2002-04-19 | 2003-10-10 | Бурлов Юрий Александрович | Плазменный реактор-сепаратор |
| US6780219B2 (en) * | 2002-07-03 | 2004-08-24 | Osram Sylvania Inc. | Method of spheridizing silicon metal powders |
| NO20033207D0 (no) * | 2002-07-31 | 2003-07-15 | Per Kristian Egeberg | Fremgangsmåte og reaktor for fremstilling av höyrent silisium, samt anvendelse av fremgangsmåten og reaktoren ved fremstilling av höyrentsilisium fra uraffinert silisium |
| JP2005033173A (ja) * | 2003-06-16 | 2005-02-03 | Renesas Technology Corp | 半導体集積回路装置の製造方法 |
| JP4235066B2 (ja) * | 2003-09-03 | 2009-03-04 | 日本エー・エス・エム株式会社 | 薄膜形成方法 |
| US20070207268A1 (en) * | 2003-12-08 | 2007-09-06 | Webb R K | Ribbed CVC structures and methods of producing |
| US7141114B2 (en) * | 2004-06-30 | 2006-11-28 | Rec Silicon Inc | Process for producing a crystalline silicon ingot |
| JP2008535758A (ja) * | 2005-04-10 | 2008-09-04 | アールイーシー シリコン インコーポレイテッド | 多結晶シリコンの製造 |
| US7396415B2 (en) * | 2005-06-02 | 2008-07-08 | Asm America, Inc. | Apparatus and methods for isolating chemical vapor reactions at a substrate surface |
| JP5141020B2 (ja) * | 2007-01-16 | 2013-02-13 | 株式会社Sumco | 多結晶シリコンの鋳造方法 |
-
2009
- 2009-02-11 US US12/378,243 patent/US20090289390A1/en not_active Abandoned
- 2009-05-15 TW TW098116130A patent/TW201009139A/zh unknown
- 2009-05-20 KR KR1020107028966A patent/KR20110030482A/ko not_active Withdrawn
- 2009-05-20 JP JP2011510685A patent/JP2011521874A/ja active Pending
- 2009-05-20 WO PCT/US2009/044704 patent/WO2009143264A2/en not_active Ceased
- 2009-05-20 CN CN2009801187328A patent/CN102084038B/zh not_active Expired - Fee Related
- 2009-05-20 CA CA2725104A patent/CA2725104A1/en not_active Abandoned
- 2009-05-20 EP EP09751492A patent/EP2291552A4/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4188368A (en) * | 1978-03-29 | 1980-02-12 | Nasa | Method of producing silicon |
| US4343772A (en) * | 1980-02-29 | 1982-08-10 | Nasa | Thermal reactor |
| US5961944A (en) * | 1996-10-14 | 1999-10-05 | Kawasaki Steel Corporation | Process and apparatus for manufacturing polycrystalline silicon, and process for manufacturing silicon wafer for solar cell |
| US20030150374A1 (en) * | 2000-12-28 | 2003-08-14 | Kenichi Sasatani | Silicon continuous casting method |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2011521874A (ja) | 2011-07-28 |
| WO2009143264A3 (en) | 2010-03-11 |
| EP2291552A2 (en) | 2011-03-09 |
| TW201009139A (en) | 2010-03-01 |
| CA2725104A1 (en) | 2009-11-26 |
| US20090289390A1 (en) | 2009-11-26 |
| WO2009143264A2 (en) | 2009-11-26 |
| EP2291552A4 (en) | 2012-01-04 |
| KR20110030482A (ko) | 2011-03-23 |
| CN102084038A (zh) | 2011-06-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102084038B (zh) | 硅或活性金属的直接铸造 | |
| KR100411180B1 (ko) | 다결정실리콘의 제조방법과 그 장치 | |
| EP2294005B1 (en) | Method and skull reactor for producing silicon or a reactive metal | |
| CA2795395C (en) | Production of monocrystalline semiconductor materials | |
| JP4157281B2 (ja) | シリコン生成用反応装置 | |
| US20160348271A1 (en) | Integrated System of Silicon Casting and Float Zone Crystallization | |
| JP4639004B2 (ja) | シリコン製造装置および製造方法 | |
| US10196273B2 (en) | Device for manufacturing polysilicon using horizontal reactor and method for manufacturing same | |
| TWI551735B (zh) | 結晶半導體材料之製造 | |
| KR102045615B1 (ko) | 폴리실리콘 제조를 위한 초고온 석출 공정 | |
| KR20110010249A (ko) | 태양전지용 고순도 실리콘 제조 방법 및 그를 위한 장치 | |
| JP2009033013A (ja) | 結晶シリコン粒子の製造方法 | |
| KR20120007143A (ko) | 마이크로파로 화학증기증착 반응로 내부 입자 또는 소재를 가열, 용융하는 방법 | |
| JPS63225516A (ja) | 高純度粒状珪素の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131211 Termination date: 20140520 |