CN101368014B - Inorganic putty powder with function of governing humidness - Google Patents
Inorganic putty powder with function of governing humidness Download PDFInfo
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- CN101368014B CN101368014B CN2008102223780A CN200810222378A CN101368014B CN 101368014 B CN101368014 B CN 101368014B CN 2008102223780 A CN2008102223780 A CN 2008102223780A CN 200810222378 A CN200810222378 A CN 200810222378A CN 101368014 B CN101368014 B CN 101368014B
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Abstract
The invention relates to interior wall putty powder with air humidity regulating function, which belongs to the field of building materials. The putty powder is composed of 10 to 50 weight portions of humidity regulating material, 15 to 50 weight portions of inorganic binding material, 15 to 50 weight portions of inorganic filler, and 1 to 5 weight portions of sub divisible rubber powder; the humidity regulating material comprises one type or more than one type of diatomite, sepiolite, attapulgite, vermiculite, zeolite powder, kaolin and bentonite. Because of the environment protection and humidity regulating functions, the multi-pore inorganic mineral material is taken as humidity regulating material and applied in the building interior wall putty powder. With water added in, the putty powder is mixed into lacquer putty and applied on the wall surface, which can effectively regulate the indoor air humidity, so that the indoor air humidity is controlled within the scope which is beneficial to the health of human body; meanwhile, the putty powder has no pollution, no VOC released and can be directly used for decoration.
Description
Technical field
The present invention relates to building and ornament materials, be specifically related to the inner wall putty powder of ambient relative humidity in a kind of effectively surge chamber.
Background technology
In the daily life, the too high meeting of humidity makes the people feel unsmooth breath uncomfortable in chest, and too high humidity helps the growth of bacterium; Humidity crosses that air then can seem dry when low, and article are dry and cracked easily or the like.In recent years, along with the raising day by day that people require the life comfort level, the humidity height is more and more paid attention to the influence of human settlements living environment.In order to pursue the humidity environment of relative comfort, people make and come controlling moisture in many ways, modal is exactly the use of humidifier and air-conditioning, yet these mechanical controlling moisturies need expend a large amount of energy, and indoor can not the ventilation caused pollution significantly when using no fresh air conditioner.At present, energy consumption is than higher aspect building in China, and waste is serious, and unit floor area of building energy consumption is 2～3 times of developed country, and the whole process from building, 50% of the whole energy consumptions of whole building energy consumption account China.Therefore, from the machinery control wet outside development have the moisture control effect material of construction not only significant aspect the environmental protection and energy saving, and be one of important method that solves indoor environment humidity comfort level problem.
The research of damping building materials comes from Japan, and this is determined by its special island weather.Its special structure and composition of porous mineral material becomes the humidity adjusting material research object of the favor of various countries' researcher in recent years.In Japan, utilize the various damping building materials that diatomite, zeolite and vermiculite or the like make use at venues such as memorial museum, exhibition center, Libraries (Ran Maoyu. Japan is to Research on moisture conditioning materials and application. material Leader .2002,16 (11): 42-44)).Chinese patent application 200610099093.3 discloses a kind of humidity adjusting material that is used for textiles and body of wall, mesoporous material (sepiolite, diatomite, attapulgite etc.) and super absorbent resin by biocatalyzer, 2-5nm are formed, the damping scope is relative humidity 35-75%, wherein super absorbent resin is brought into play humidity conditioning function, mesoporous material is the carrier of other components, this humidity adjusting material moisture uptake is big, but still have the defective that the moisture adsorption and releasing characteristic is bad, the moisture adsorption and releasing amount is limited, and directly also there is technical obstacle in use.
Along with the day by day raising of people to finishing material quality and functional requirement, supporting with it putty also causes people's attention gradually.Tradition putty has that intensity is low, water-intake rate is big, quality is loosened, contain the fatal shortcoming of formaldehyde or the like, can not satisfy the service requirements that improves day by day; On the other hand, existing humidity adjusting material directly adds in the putty powder can not bring into play the damping effect, and need allocate from the suitability of whole components, and therefore, high-quality environmental protection in the market, the putty product with humidity conditioning function still belong to blank.
Summary of the invention
The purpose of this invention is to provide a kind of environmental protection and have the excellent putty product of regulating the indoor relative humidity function.
The present invention has the inner wall putty powder of atmospheric moisture regulatory function, in the described putty powder of per 100 weight parts, following component is arranged:
Humidity-controlling functional material 10-50 weight part;
Inorganic coagulation material 15-50 weight part;
Mineral filler 15-50 weight part; And
Re-dispersible glue powder 1-5 weight part.
Wherein, described humidity-controlling functional material is one or more in diatomite, sepiolite, attapulgite, vermiculite, zeolite powder, kaolin and the wilkinite.
The best acidified pre-treatment of described humidity-controlling functional material.Acidization is for to soak the porous mineral material in sulfuric acid or hydrochloric acid, use filtration then, dry back.
Wherein, described gelling material is ordinary Portland cement or white cement.
Wherein, re-dispersible glue powder is selected from a kind of in the emulsion powder, Taiwan Mortarplus polyvinyl alcohol rubber powder, starch ethers of the ROHM AND HAAS Rovace of the U.S., the triumphant chemical company VINNAPASR of German prestige, Japanese Clariant Clariant, and adds methylcellulose gum simultaneously and be used.Methylcellulose gum and re-dispersible glue powder are by weight using 1: 1～1: 9 scope.
Wherein, described mineral filler be in dicalcium powder, talcum powder, zinc sulfide white, wollastonite powder, grey calcium powder, the dry powder one or more.
Inner wall putty with atmospheric moisture regulatory function also belongs to the technology of the present invention content, and this inner wall putty with atmospheric moisture regulatory function is that above-mentioned inner wall putty powder and water are formed by weight allotment in 1: 0.4.
Adopt above design, the present invention utilizes the environmental protection and the moisture control function of porous, inorganic mineral material, and it as humidity-controlling functional material, is applied to the inner wall of building putty powder.The porous, inorganic mineral material adds other component, mixes the back blade coating in metope, can effectively regulate indoor air humidity, makes it to be controlled in the scope that is of value to HUMAN HEALTH, and simultaneously pollution-free, zero VOC discharges, and also can directly play decoration function.
The every performance of product of the present invention all meets the JG/T157-2004 industry standard, in addition, also satisfies the National Environmental specification of quality, and effectively ambient relative humidity in the surge chamber has good environmental protection characteristic.This product also can directly use as decorative material for internal wall simultaneously.
Description of drawings
Fig. 1 is 25 ℃, 85%RH moisture absorption correlation curve.
Fig. 2 is 25 ℃, 35%RH moisture releasing correlation curve.
Embodiment
The present invention is intended to overcome mechanical damping such as air-conditioning technical and produces problems such as power consumption and pollution, solves the shortcoming of traditional putty, utilizes indoor decoration putty that indoor environment relative humidity is regulated.In the present invention, damping refers to moisture absorption and two aspects of moisture releasing.
Among the present invention, the inner wall putty powder of atmospheric moisture regulatory function mainly with porous, inorganic mineral materials such as diatomite, sepiolite, attapulgite, zeolites as humidity-controlling functional material, adaptive again other material, being mixed by a certain percentage forms.Wherein:
Inorganic coagulation material: a kind of in ordinary Portland cement, the white cement accounts for 15～50% of putty powder gross weight;
The preferred white cement of the present invention is as main gelling material.The main component of white cement own is SiO
2, Ca (OH)
2, CaCO
3Deng, the Ca that the moulding rear surface is exposed
2+, Si
4+, O
2-The water molecules of plasma in can absorbed air innerly after the white cement hydration simultaneously can stay a large amount of pore structures, can the airborne water molecules of active adsorption.
Humidity-controlling functional material: at least a or multiple being used in combination in diatomite, sepiolite, attapulgite, vermiculite, zeolite powder, kaolin, the wilkinite, ratio accounts for 10～50% of putty powder gross weight without limits when being used in combination.
Inorganic mineral material for having porous road structure such as diatomite, sepiolite, attapulgite, vermiculite, zeolite powder, kaolin, the present invention utilizes its its specific structure that water vapour is had good absorption, releasability, and, do not use any organic materials as the humidity conditioning function component to the characteristics of HUMAN HEALTH without any influence.
Processing such as the high temperature of mineral material, acidifying: porous mineral material requirements purity is higher, firsthand starting material are general impure more on the market, add the damping effect that will influence product in the coating, can carry out acidification and remove impurity, simultaneously also improve raw-material pore passage structure (most of pore size distribution is between 2-10nm), make its maintenance higher degree and have good humidity conditioning function.Specific operation process is: after soaking the porous mineral material more than 6 hours in sulfuric acid (for example mass concentration is 6%) or hydrochloric acid (for example mass concentration is 10%), filtration, drying can directly be used after the oven dry.
Mineral filler: at least a in dicalcium powder, talcum powder, zinc sulfide white, wollastonite powder, grey calcium powder, terra alba, the dry powder, or multiple being used in combination (portfolio ratio without limits), account for 15～50% of putty powder gross weight; Add mineral filler and be mainly used in application property and the scrub resistance that improves putty, guarantee the feature of environmental protection of putty simultaneously.
Re-dispersible glue powder: choose the ROHM AND HAAS Rovace DP-88 of the U.S., the triumphant chemical company VINNAPAS of German prestige
A kind of among the emulsion powder DM200 of R1551Z, Japanese Clariant Clariant, Taiwan Mortarplus polyvinyl alcohol rubber powder 2488, the starch ethers SE7.Simultaneously can add Mierocrystalline cellulose is used.Re-dispersible glue powder accounts for 1%～5% of putty powder gross weight.
Re-dispersible glue powder can strengthen paint film adhesion, improves the cohesive force of coating, reduces shrinking percentage, improves the surface strength of coating, also makes the coating workability good, easy construction.
More than raw materials used all can be commercially available.
Followingly assembly of the present invention and function are described according to specific embodiment:
Example one: following component is mixed into putty powder:
15 kilograms of white cements
10 kilograms of ash calcium powders
10 kilograms of dicalcium powders
10 kilograms of talcum powder
20 kilograms of terra albas
4.5 kilograms of latex powder DM200
0.5 kilogram of methylcellulose gum
30 kilograms in diatomite (after the pre-treatment)
Be mixed into the putty powder double centner by said components, during use, can be by water: putty powder weight ratio 0.4:1 allocates.
Testing method: get the 200g putty powder and be divided into two fens, with water stir the back respectively blade coating on the sheet glass of 150mm * 1500mm, dry naturally and be placed in the baking oven, under 80 ℃ of conditions, dried 5 hours.Then two models are placed in the 10L encloses container of 25 ℃ of temperature, relative humidity 85% the maximum reduction of the relative humidity in the measuring vessel.After relative humidity reached balance in the encloses container, changing the interior envrionment conditions of container was 25 ℃, relative humidity 35%, the maximum increasing amount of the relative humidity in the measuring vessel.By relative humidity variations situation in the Temperature Humidity Sensor record container.
The damping test result: 25 ℃ of temperature, under the condition of relative humidity 85%, the maximum reduction of relative humidity (moisture uptake) reaches 13%RH, illustrates that this test putty powder has moisture absorbing; After moisture absorption is saturated, be that test putty can moisture releasing under 35% the condition in 25 ℃ of temperature, relative humidity, the maximum increasing amount of relative humidity (humidification amount) reaches 10%RH as a result.
The test of contrast putty powder:
According to above-mentioned experimental technique, the rh value of record different time encloses container, curve plotting.Wherein: the damping putty of specimen 1# representative instance one; 2# represents same recipe, and the humidity adjusting material with 200610099093.3 is the putty that humidity-controlling functional material is made; 3# represents same recipe, and humidity-controlling functional material is unprocessed, the higher and putty made of foreign matter content; 4# represents decoration putty common on the market.
Test result: referring to Fig. 1 (sucting wet experiment curve) and Fig. 2 (moisture releasing empirical curve).As can be seen from the figure, 25 ℃ of temperature, under the condition of relative humidity 85%, the maximum reduction of relative humidity is respectively: 1#:13.25%RH, 2#:6.11%RH, 3#:6.03%RH, 4#:5.22%RH; After moisture absorption is saturated, be that test putty can moisture releasing under 35% the condition in 25 ℃ of temperature, relative humidity, the maximum increasing amount of relative humidity is respectively as a result: 1#:10.43%RH, 2#:5.02%RH, 3#:5.85%RH, 4#:4.39%RH.By contrast as can be seen: compare with other several putty, damping putty moisture uptake of the present invention and moisture releasing amount all exceed much than other comparative sample, illustrate to have good damping effect.
Example two; Following component is mixed into putty powder:
33 kilograms of ordinary Portland cements
9 kilograms of dicalcium powders
6 kilograms of talcum powder
2,488 1.5 kilograms of latex powder
0.5 kilogram of methylcellulose gum
25 kilograms of attapulgites
25 kilograms of sepiolites (after the pre-treatment)
Be mixed into the putty powder double centner by said components.During use, can be by water: putty powder weight ratio 0.4:1 allocates.
Carry out Function detection with the method identical with embodiment one, the result is 25 ℃ of temperature, and under the condition of relative humidity 85%, the maximum reduction of relative humidity reaches 14%RH; After moisture absorption is saturated, be moisture releasing under 35% the condition in 25 ℃ of temperature, relative humidity, the maximum increasing amount of relative humidity reaches 12%RH as a result.
Example three: following component is mixed into putty powder:
50 kilograms of normal silicate white cements
14 kilograms of dry powders
10 kilograms in zinc sulfide white
0.5 kilogram of latex powder DP-88
0.5 kilogram of methylcellulose gum
15 kilograms of vermiculite powers (after the pre-treatment)
10 kilograms of wilkinites (after the pre-treatment)
Be mixed into the putty powder double centner by said components.During use, can be by water: putty powder weight ratio 0.4:1 allocates.
Carry out Function detection with the method identical with embodiment one, the result is 25 ℃ of temperature, and under the condition of relative humidity 85%, the maximum reduction of relative humidity reaches 10%RH; After moisture absorption is saturated, be moisture releasing under 35% the condition in 25 ℃ of temperature, relative humidity, the maximum increasing amount of relative humidity reaches 7%RH as a result.
Embodiment four～six, be mixed into putty powder, and use the method identical to carry out Function detection with embodiment one by table 1 component and consumption.These embodiment show that the putty powder that makes by proportioning of the present invention all has humidity conditioning function preferably.
Table 1
More than experiment shows, putty of the present invention, and 25 ℃ of temperature, under the condition of relative humidity 85%, the maximum reduction of relative humidity reaches above 8%RH; After moisture absorption is saturated, be moisture releasing under 35% the condition in 25 ℃ of temperature, relative humidity, the maximum increasing amount of relative humidity exceeds much than other comparative sample greater than 7%RH as a result, illustrates to have good damping effect.
Claims (7)
1. the inner wall putty powder with atmospheric moisture regulatory function is characterized in that, in the described putty powder of per 100 weight parts, following component is arranged:
Humidity-controlling functional material 10-50 weight part;
Inorganic coagulation material 15-50 weight part;
Mineral filler 15-50 weight part: and
Re-dispersible glue powder 1-5 weight part;
Wherein, described humidity-controlling functional material is one or more on diatomite, sepiolite, attapulgite, vermiculite, zeolite powder, the high mountain range and in the wilkinite; And described humidity-controlling functional material is through the acidifying pre-treatment:
Described re-dispersible glue powder is to be used with methylcellulose gum.
2. according to right 1 described inner wall putty powder, it is characterized in that described acidifying preprocessing process is for to soak humidity-controlling functional material in sulfuric acid or hydrochloric acid, filter then, drying with atmospheric moisture regulatory function.
3. according to right 1 or 2 described inner wall putty powders, it is characterized in that described gelling material is ordinary Portland cement or white cement with atmospheric moisture regulatory function.
4. according to right 1 or 2 described inner wall putty powders with atmospheric moisture regulatory function, it is characterized in that re-dispersible glue powder is selected from a kind of in the emulsion powder, Taiwan Mortarplus polyvinyl alcohol rubber powder, starch ethers of the ROHM AND HAAS Rovace of the U.S., the triumphant chemical company VINNAPAS R of German prestige, Japanese Clariant Clariant.
5. the inner wall putty powder with atmospheric moisture regulatory function according to claim 4 is characterized in that, described methylcellulose gum and re-dispersible glue powder are by weight using 1: 1～1: 9 scope.
6. the inner wall putty powder with atmospheric moisture regulatory function according to claim 1 and 2 is characterized in that, described mineral filler be in dicalcium powder, talcum powder, zinc sulfide white, wollastonite powder, grey calcium powder and the dry powder one or more.
7. the inner wall putty that has the atmospheric moisture regulatory function is that arbitrary described inner wall putty powder of claim 1 to 6 and water are formed by weight allotment in 1: 0.4.
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