CN1003588B - 酰化二酮化合物的制备方法 - Google Patents

酰化二酮化合物的制备方法 Download PDF

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Publication number
CN1003588B
CN1003588B CN85109777.4A CN85109777A CN1003588B CN 1003588 B CN1003588 B CN 1003588B CN 85109777 A CN85109777 A CN 85109777A CN 1003588 B CN1003588 B CN 1003588B
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CN
China
Prior art keywords
alkyl
cyanide
enol ester
production method
mole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CN85109777.4A
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English (en)
Chinese (zh)
Other versions
CN85109777A (zh
Inventor
詹姆斯·布里安·黑瑟
帕米拉·戴尼斯·米拉诺
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stauffer Chemical Co
Original Assignee
Stauffer Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stauffer Chemical Co filed Critical Stauffer Chemical Co
Publication of CN85109777A publication Critical patent/CN85109777A/zh
Publication of CN1003588B publication Critical patent/CN1003588B/zh
Expired legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/12Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/30Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/455Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation with carboxylic acids or their derivatives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/54Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385Saturated compounds containing a keto group being part of a ring
    • C07C49/403Saturated compounds containing a keto group being part of a ring of a six-membered ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Heterocyclic Compounds Containing Sulfur Atoms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN85109777.4A 1984-12-20 1985-12-19 酰化二酮化合物的制备方法 Expired CN1003588B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US68388284A 1984-12-20 1984-12-20
US683,882 1984-12-20
US79884285A 1985-11-20 1985-11-20
US798,842 1985-11-20

Publications (2)

Publication Number Publication Date
CN85109777A CN85109777A (zh) 1987-02-04
CN1003588B true CN1003588B (zh) 1989-03-15

Family

ID=27103213

Family Applications (1)

Application Number Title Priority Date Filing Date
CN85109777.4A Expired CN1003588B (zh) 1984-12-20 1985-12-19 酰化二酮化合物的制备方法

Country Status (24)

Country Link
EP (1) EP0186117B1 (US06373033-20020416-M00035.png)
JP (1) JPH0710787B2 (US06373033-20020416-M00035.png)
KR (1) KR920000907B1 (US06373033-20020416-M00035.png)
CN (1) CN1003588B (US06373033-20020416-M00035.png)
AU (1) AU592069B2 (US06373033-20020416-M00035.png)
BG (1) BG45042A3 (US06373033-20020416-M00035.png)
BR (1) BR8506421A (US06373033-20020416-M00035.png)
CA (1) CA1317976C (US06373033-20020416-M00035.png)
DE (1) DE3580657D1 (US06373033-20020416-M00035.png)
DK (1) DK174911B1 (US06373033-20020416-M00035.png)
FI (1) FI86542C (US06373033-20020416-M00035.png)
GE (1) GEP19960642B (US06373033-20020416-M00035.png)
GR (1) GR853110B (US06373033-20020416-M00035.png)
HU (1) HU204753B (US06373033-20020416-M00035.png)
IL (1) IL77350A (US06373033-20020416-M00035.png)
MX (1) MX170385B (US06373033-20020416-M00035.png)
NO (1) NO163402C (US06373033-20020416-M00035.png)
PL (1) PL148102B1 (US06373033-20020416-M00035.png)
PT (1) PT81730B (US06373033-20020416-M00035.png)
RO (1) RO93561A (US06373033-20020416-M00035.png)
SU (1) SU1697591A3 (US06373033-20020416-M00035.png)
TR (1) TR23030A (US06373033-20020416-M00035.png)
YU (1) YU45754B (US06373033-20020416-M00035.png)
ZW (1) ZW23785A1 (US06373033-20020416-M00035.png)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL77348A (en) * 1984-12-20 1991-05-12 Stauffer Chemical Co 2-(2'-substituted benzoyl)-1,3-cyclohexanediones,their preparation and their use as herbicides
IL77349A (en) * 1984-12-20 1990-07-12 Stauffer Chemical Co 2-(2'-nitrobenzoyl)-1,3-cyclohexanediones,their preparation and their use as herbicides
TR22585A (tr) * 1984-12-20 1987-12-07 Stauffer Chemical Co Bazi 2-(2'-alkilbenzoil)-1,3-sikloheksandion'lar
AU583089B2 (en) * 1985-02-15 1989-04-20 Ici Australia Limited Process for the preparation of 2-acylcyclohexane-1,3-dione derivatives
US4724263A (en) * 1986-06-09 1988-02-09 Stauffer Chemical Company Certain 2-phenylacetyl-1,3,5-cyclohexanetriones
US4783213A (en) * 1986-10-16 1988-11-08 Stauffer Chemical Company Certain 2-(2-substituted benzoyl)-4-(substituted oxy or substituted thio)-1,3-cyclohexanediones
KR890003680A (ko) * 1986-10-16 1989-04-17 죤 알.페넬 2-(2-치환 벤조일)-4-(치환)-1,3-시클로헥산디온 및 그 제조방법과 이를 이용한 조성물 및 식물체의 억제방법
US4808214A (en) * 1986-10-16 1989-02-28 Stauffer Chemical Company Certain 2-(2-substituted benzoyl)-4-(substituted oxy or substituted thio)-1,3-cyclohexanediones
DE3743695A1 (de) * 1987-12-18 1989-06-29 Schering Ag 4-benzoyl-3-hydroxy-5-oxo-3-cyclohexencarbonsaeurederivate, verfahren zur herstellung dieser verbindungen und ihre verwendung als mittel mit pflanzenwachstumsregulierender wirkung
HUT50312A (en) * 1988-02-01 1990-01-29 Sandoz Ag Herbicide composition containing new dion-compounds and process for producing these compounds
CN1038093A (zh) * 1988-04-18 1989-12-20 山道士有限公司 对有机化合物和关于有机化合物的改进
US4869748A (en) * 1988-12-02 1989-09-26 Ici Americas Inc. Certain 3-(substituted benzoyl)-3:2:1-bicyclooctan-2,4-diones
US5336662A (en) * 1989-04-25 1994-08-09 Sandoz Ltd. Heterocyclic diones as plant growth regulators
AU642052B2 (en) * 1990-10-25 1993-10-07 Sandoz Ltd. Heterocyclic dione derivatives as pesticides and plant growth regulators
GB9501434D0 (en) * 1995-01-25 1995-03-15 Zeneca Ltd Chemical process
GB9501433D0 (en) * 1995-01-25 1995-03-15 Zeneca Ltd Chemical process
DE10113137C2 (de) * 2001-03-17 2003-05-15 Bayer Cropscience Gmbh Verfahren zur Herstellung von substituierten 2-Benzoyl-1,3-cyclohexandionen
AU2003203482B2 (en) * 2002-04-09 2005-06-02 Syngenta Participations Ag Process for the preparation of cyclic diketones
TWI348999B (en) * 2003-10-02 2011-09-21 Syngenta Participations Ag Process
DE102004016496A1 (de) 2004-04-03 2005-10-20 Bayer Cropscience Gmbh Herbizid wirksame 3-Amino-2-thiomethyl-benzoylpyrazole
DE102007026875A1 (de) 2007-06-11 2008-12-24 Bayer Cropscience Ag 3-Cyclopropyl-4-(3-thiobenzoyl)pyrazole und ihre Verwendung als Herbizide
PT104664A (pt) * 2009-07-07 2011-01-07 Sapec Agro S A Polimorfo cristalino estável de 2-(2-cloro-4-mesil-benzoil)- ciclo-hexano-1,3-diona e processo para preparar o mesmo
EP2536277B1 (de) 2010-02-19 2016-01-20 Bayer Intellectual Property GmbH 3-aminocarbonyl substituierte benzoylcyclohexandione und ihre verwendung als herbizide
WO2012010573A1 (de) 2010-07-21 2012-01-26 Bayer Cropscience Ag 4-(4-halogenalkyl-3-thiobenzoyl)pyrazole und ihre verwendung als herbizide
JP5906314B2 (ja) 2011-07-15 2016-04-20 バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングBayer Intellectual Property GmbH 2,3−ジフェニル−バレロニトリル誘導体、それらを製造する方法並びに除草剤及び植物成長調節剤としてのそれらの使用
CN113845451B (zh) * 2020-06-28 2023-07-14 沈阳中化农药化工研发有限公司 一种制备三酮类除草剂的方法
CN113233998B (zh) * 2021-05-24 2021-12-28 浙江新安化工集团股份有限公司 一种硝磺草酮的制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4350705A (en) * 1979-03-31 1982-09-21 Eisai Co., Ltd. Cyclohexane derivatives, process for preparation thereof and medicines containing these cyclohexane derivatives
EP0090262B1 (en) * 1982-03-25 1992-08-05 Stauffer Chemical Company Certain 2-(2-substituted benzoyl)-1,3-cyclohexanediones
JPS59196840A (ja) * 1983-04-22 1984-11-08 Kumiai Chem Ind Co Ltd シクロヘキサン誘導体および植物生長調節剤
US4482727A (en) * 1983-07-01 1984-11-13 Stauffer Chemical Company Certain 1,3-cyclohexanedione adducts of substituted phenoxyphenoxypropionic acids and their use as an herbicide
EP0162336B1 (en) * 1984-05-21 1989-03-22 Stauffer Chemical Company Certain 2-(2-(substituted phenyl)acetyl)-1,3-cyclohexanediones
IL77349A (en) * 1984-12-20 1990-07-12 Stauffer Chemical Co 2-(2'-nitrobenzoyl)-1,3-cyclohexanediones,their preparation and their use as herbicides
TR22585A (tr) * 1984-12-20 1987-12-07 Stauffer Chemical Co Bazi 2-(2'-alkilbenzoil)-1,3-sikloheksandion'lar

Also Published As

Publication number Publication date
AU592069B2 (en) 1990-01-04
FI855047A0 (fi) 1985-12-18
IL77350A (en) 1991-01-31
DK174911B1 (da) 2004-02-16
PT81730A (en) 1986-01-01
AU5133585A (en) 1986-06-26
CA1317976C (en) 1993-05-18
BR8506421A (pt) 1986-09-02
YU45754B (sh) 1992-07-20
JPS61171449A (ja) 1986-08-02
NO855163L (no) 1986-06-23
EP0186117B1 (en) 1990-11-22
GR853110B (US06373033-20020416-M00035.png) 1986-04-22
EP0186117A3 (en) 1987-06-16
NO163402B (no) 1990-02-12
NO163402C (no) 1990-05-23
FI86542B (fi) 1992-05-29
PL148102B1 (en) 1989-09-30
YU200985A (en) 1988-02-29
FI86542C (fi) 1992-09-10
KR860004825A (ko) 1986-07-14
EP0186117A2 (en) 1986-07-02
PT81730B (pt) 1988-07-01
FI855047A (fi) 1986-06-21
PL256982A1 (en) 1987-03-09
TR23030A (tr) 1989-02-10
JPH0710787B2 (ja) 1995-02-08
SU1697591A3 (ru) 1991-12-07
MX170385B (es) 1993-08-19
KR920000907B1 (ko) 1992-01-31
CN85109777A (zh) 1987-02-04
RO93561A (ro) 1987-12-31
GEP19960642B (en) 1996-11-15
HU204753B (en) 1992-02-28
DK594585D0 (da) 1985-12-19
BG45042A3 (bg) 1989-03-15
HUT41368A (en) 1987-04-28
ZW23785A1 (en) 1986-03-19
DE3580657D1 (de) 1991-01-03
DK594585A (da) 1986-06-21

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GR01 Patent grant
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Address after: Delaware

Applicant after: Seneca Corp.

Address before: American Connecticut

Applicant before: Stauffer Chemical Co.

COR Change of bibliographic data

Free format text: CORRECT: APPLICANT; FROM: STAUFFER CHEMICAL CO. TO: ZENIKA COMPANY

C17 Cessation of patent right
CX01 Expiry of patent term