CN100336777C - 一种氧化镥基透明陶瓷的制备方法 - Google Patents
一种氧化镥基透明陶瓷的制备方法 Download PDFInfo
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- CN100336777C CN100336777C CNB2005100272083A CN200510027208A CN100336777C CN 100336777 C CN100336777 C CN 100336777C CN B2005100272083 A CNB2005100272083 A CN B2005100272083A CN 200510027208 A CN200510027208 A CN 200510027208A CN 100336777 C CN100336777 C CN 100336777C
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- based transparent
- lutetium oxide
- preparing
- lutetium
- transparent ceramics
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- 239000000919 ceramic Substances 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims description 24
- 229910003443 lutetium oxide Inorganic materials 0.000 claims abstract description 21
- MPARYNQUYZOBJM-UHFFFAOYSA-N oxo(oxolutetiooxy)lutetium Chemical compound O=[Lu]O[Lu]=O MPARYNQUYZOBJM-UHFFFAOYSA-N 0.000 claims abstract description 16
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 claims abstract description 12
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims abstract description 12
- 239000001099 ammonium carbonate Substances 0.000 claims abstract description 12
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 12
- 239000002243 precursor Substances 0.000 claims abstract description 11
- 239000012298 atmosphere Substances 0.000 claims abstract description 10
- 150000002500 ions Chemical class 0.000 claims abstract description 10
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000001272 pressureless sintering Methods 0.000 claims abstract description 8
- 239000002131 composite material Substances 0.000 claims abstract description 7
- -1 ion nitrate Chemical class 0.000 claims abstract description 7
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001257 hydrogen Substances 0.000 claims abstract description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 6
- 238000001556 precipitation Methods 0.000 claims abstract description 6
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 5
- 229910052765 Lutetium Inorganic materials 0.000 claims abstract description 3
- 238000001354 calcination Methods 0.000 claims abstract description 3
- 229910002651 NO3 Inorganic materials 0.000 claims abstract 3
- 238000000465 moulding Methods 0.000 claims abstract 2
- 238000005245 sintering Methods 0.000 claims description 11
- 238000003825 pressing Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 229910052693 Europium Inorganic materials 0.000 claims description 5
- 239000002019 doping agent Substances 0.000 claims description 5
- 238000000462 isostatic pressing Methods 0.000 claims description 4
- 229910052779 Neodymium Inorganic materials 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 229910052771 Terbium Inorganic materials 0.000 claims description 3
- 229910052775 Thulium Inorganic materials 0.000 claims description 3
- 229910052769 Ytterbium Inorganic materials 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 2
- 238000002156 mixing Methods 0.000 claims 1
- 238000004321 preservation Methods 0.000 claims 1
- 230000003287 optical effect Effects 0.000 abstract description 13
- 229910010293 ceramic material Inorganic materials 0.000 abstract description 5
- 238000002834 transmittance Methods 0.000 abstract description 4
- 230000032683 aging Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract description 2
- OHSVLFRHMCKCQY-UHFFFAOYSA-N lutetium atom Chemical compound [Lu] OHSVLFRHMCKCQY-UHFFFAOYSA-N 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 21
- 239000000463 material Substances 0.000 description 16
- 239000013078 crystal Substances 0.000 description 9
- 239000002245 particle Substances 0.000 description 9
- 239000000243 solution Substances 0.000 description 7
- 239000011259 mixed solution Substances 0.000 description 6
- 238000000975 co-precipitation Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000006185 dispersion Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 3
- 239000004202 carbamide Substances 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000011858 nanopowder Substances 0.000 description 3
- 238000004448 titration Methods 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- 229910052684 Cerium Inorganic materials 0.000 description 2
- 239000012190 activator Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000008204 material by function Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 230000005693 optoelectronics Effects 0.000 description 2
- 239000011224 oxide ceramic Substances 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000007088 Archimedes method Methods 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229910052691 Erbium Inorganic materials 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910052688 Gadolinium Inorganic materials 0.000 description 1
- 229910052777 Praseodymium Inorganic materials 0.000 description 1
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 1
- 229910001634 calcium fluoride Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 238000009841 combustion method Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000002159 nanocrystal Substances 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 229910052574 oxide ceramic Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Luminescent Compositions (AREA)
Abstract
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CNB2005100272083A CN100336777C (zh) | 2005-06-28 | 2005-06-28 | 一种氧化镥基透明陶瓷的制备方法 |
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CNB2005100272083A CN100336777C (zh) | 2005-06-28 | 2005-06-28 | 一种氧化镥基透明陶瓷的制备方法 |
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CN1760157A CN1760157A (zh) | 2006-04-19 |
CN100336777C true CN100336777C (zh) | 2007-09-12 |
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Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102006027957A1 (de) | 2006-06-14 | 2007-12-20 | Schott Ag | Optische Elemente sowie Abbildungsoptiken |
DE102006027958A1 (de) | 2006-06-14 | 2007-12-20 | Schott Ag | Optokeramiken, daraus hergestellte optische Elemente sowie Abbildungsoptiken |
CN102557598B (zh) * | 2011-03-21 | 2014-10-01 | 上海大学 | Ce:Lu2SiO5多晶闪烁光学陶瓷的无压烧结制备方法 |
CN103058254B (zh) * | 2012-09-22 | 2014-12-03 | 包头市京瑞新材料有限公司 | 制备大颗粒氧化镥的方法 |
CN103058256B (zh) * | 2012-09-22 | 2014-12-17 | 包头市京瑞新材料有限公司 | 制备大颗粒氧化镝的方法 |
CN105236980B (zh) * | 2015-11-19 | 2017-11-10 | 中国工程物理研究院化工材料研究所 | 一种ZrO2、LiF共掺杂真空烧结氧化镥透明陶瓷的方法 |
CN106145959B (zh) * | 2016-07-10 | 2018-08-17 | 九江学院 | 一种氧化镥透明陶瓷的制备方法 |
CN106588014B (zh) * | 2016-12-19 | 2019-08-23 | 中国科学院长春光学精密机械与物理研究所 | 一种发光增强的Tm3+掺杂氧化镥基透明陶瓷及制备方法 |
CN108751991B (zh) * | 2018-08-17 | 2020-03-13 | 徐州华焰特种陶瓷有限公司 | 一种激光烧结制备Tb:Lu2O3陶瓷的方法 |
CN110256074A (zh) * | 2019-07-16 | 2019-09-20 | 上海应用技术大学 | 一种钇稳定氧化铽粉体、磁光透明陶瓷及其制备方法 |
CN111138192A (zh) * | 2020-01-03 | 2020-05-12 | 上海应用技术大学 | 一种氧化镥铽磁光透明陶瓷的真空热压制备方法 |
CN112853489A (zh) * | 2021-01-06 | 2021-05-28 | 安徽工业大学 | 一种稀土离子掺杂倍半氧化物可见激光晶体材料 |
CN114988876B (zh) * | 2022-06-24 | 2023-05-12 | 中国工程物理研究院化工材料研究所 | 一种Eu、Sc共掺杂的透明氧化镥陶瓷及其制备方法 |
Citations (1)
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JP2004292186A (ja) * | 2003-03-25 | 2004-10-21 | Murata Mfg Co Ltd | 誘電体セラミックおよび積層セラミックコンデンサ |
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JP2004292186A (ja) * | 2003-03-25 | 2004-10-21 | Murata Mfg Co Ltd | 誘電体セラミックおよび積層セラミックコンデンサ |
Non-Patent Citations (1)
Title |
---|
陶瓷闪烁材料最新研究进展 陈启伟,施鹰 施剑林,材料科学与工程学报,第23卷第1期 2005 * |
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Owner name: NINGBO YUNSHENG PHOTO-COMMUNICATION TECHNOLOGY CO. Free format text: FORMER OWNER: SHANGHAI INSTITUTE OF CERAMICS, CHINESE ACADEMY OF SCIENCES Effective date: 20100604 |
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Effective date of registration: 20100604 Address after: 315000, No. 1, sailing Road, Ningbo national hi tech Zone Patentee after: Ningbo Yunsheng Photo-Communication Technology Co. Ltd. Address before: 1295 Dingxi Road, Shanghai, No. 200050 Patentee before: Shanghai Silicates Institute, the Chinese Academy of Sciences |
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