CH495385A - Verfahren zur Herstellung von wasserlöslichen Kondensationsprodukten - Google Patents
Verfahren zur Herstellung von wasserlöslichen KondensationsproduktenInfo
- Publication number
- CH495385A CH495385A CH142767A CH142767A CH495385A CH 495385 A CH495385 A CH 495385A CH 142767 A CH142767 A CH 142767A CH 142767 A CH142767 A CH 142767A CH 495385 A CH495385 A CH 495385A
- Authority
- CH
- Switzerland
- Prior art keywords
- caprolactam
- water
- reaction
- alkylene
- formula
- Prior art date
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N Caprolactam Natural products O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 229910001868 water Inorganic materials 0.000 title claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 12
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007859 condensation product Substances 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 5
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims abstract description 5
- 150000001875 compounds Chemical class 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 239000000243 solution Substances 0.000 claims description 9
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000011541 reaction mixture Substances 0.000 claims description 4
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 3
- 239000012736 aqueous medium Substances 0.000 claims description 3
- 230000008030 elimination Effects 0.000 claims description 3
- 238000003379 elimination reaction Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 230000001419 dependent effect Effects 0.000 claims 1
- 239000013067 intermediate product Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 7
- 229920000768 polyamine Polymers 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 4
- 125000003277 amino group Chemical group 0.000 abstract description 3
- 239000000945 filler Substances 0.000 abstract description 2
- 239000008394 flocculating agent Substances 0.000 abstract description 2
- 239000002985 plastic film Substances 0.000 abstract description 2
- 238000009988 textile finishing Methods 0.000 abstract description 2
- 239000004952 Polyamide Substances 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 9
- 238000009833 condensation Methods 0.000 description 6
- 230000005494 condensation Effects 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000004753 textile Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- -1 triaminopropane Chemical compound 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 2
- XFNJVJPLKCPIBV-UHFFFAOYSA-N trimethylenediamine Chemical compound NCCCN XFNJVJPLKCPIBV-UHFFFAOYSA-N 0.000 description 2
- UYBWIEGTWASWSR-UHFFFAOYSA-N 1,3-diaminopropan-2-ol Chemical compound NCC(O)CN UYBWIEGTWASWSR-UHFFFAOYSA-N 0.000 description 1
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 description 1
- LBLYYCQCTBFVLH-UHFFFAOYSA-N 2-Methylbenzenesulfonic acid Chemical compound CC1=CC=CC=C1S(O)(=O)=O LBLYYCQCTBFVLH-UHFFFAOYSA-N 0.000 description 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000004873 anchoring Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- LSHROXHEILXKHM-UHFFFAOYSA-N n'-[2-[2-[2-(2-aminoethylamino)ethylamino]ethylamino]ethyl]ethane-1,2-diamine Chemical compound NCCNCCNCCNCCNCCN LSHROXHEILXKHM-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 238000003918 potentiometric titration Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
- C08G73/0206—Polyalkylene(poly)amines
- C08G73/0213—Preparatory process
- C08G73/022—Preparatory process from polyamines and epihalohydrins
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Paper (AREA)
- Polyamides (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEB0085704 | 1966-02-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH495385A true CH495385A (de) | 1970-08-31 |
Family
ID=6983032
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH142767A CH495385A (de) | 1966-02-08 | 1967-01-31 | Verfahren zur Herstellung von wasserlöslichen Kondensationsprodukten |
Country Status (8)
| Country | Link |
|---|---|
| AT (1) | AT267870B (en, 2012) |
| BE (1) | BE693442A (en, 2012) |
| CH (1) | CH495385A (en, 2012) |
| DE (1) | DE1595302A1 (en, 2012) |
| FR (1) | FR1510556A (en, 2012) |
| GB (1) | GB1165394A (en, 2012) |
| NL (1) | NL6701449A (en, 2012) |
| SE (1) | SE305082B (en, 2012) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2756469A1 (de) * | 1977-12-17 | 1979-06-21 | Bayer Ag | Amidgruppenhaltige polyamine |
| DE3300866A1 (de) * | 1983-01-13 | 1984-07-19 | Basf Ag, 6700 Ludwigshafen | Oxalkylierte polyamidoamine, deren herstellung und deren verwendung als erdoelemulsionsspalter |
| DE3810424A1 (de) * | 1988-03-26 | 1989-10-12 | Bayer Ag | Stickstoffhaltige polymere verbindungen |
-
1966
- 1966-02-08 DE DE19661595302 patent/DE1595302A1/de active Pending
-
1967
- 1967-01-30 NL NL6701449A patent/NL6701449A/xx unknown
- 1967-01-31 BE BE693442D patent/BE693442A/xx unknown
- 1967-01-31 CH CH142767A patent/CH495385A/de not_active IP Right Cessation
- 1967-02-07 FR FR93989A patent/FR1510556A/fr not_active Expired
- 1967-02-07 GB GB579067A patent/GB1165394A/en not_active Expired
- 1967-02-08 AT AT120867A patent/AT267870B/de active
- 1967-02-08 SE SE1783/67A patent/SE305082B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE693442A (en, 2012) | 1967-07-31 |
| GB1165394A (en) | 1969-09-24 |
| FR1510556A (fr) | 1968-01-19 |
| AT267870B (de) | 1969-01-27 |
| NL6701449A (en, 2012) | 1967-08-09 |
| DE1595302A1 (de) | 1970-03-05 |
| SE305082B (en, 2012) | 1968-10-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PL | Patent ceased |