CH159031A - Process for the production of an ammonium salt. - Google Patents

Process for the production of an ammonium salt.

Info

Publication number
CH159031A
CH159031A CH159031DA CH159031A CH 159031 A CH159031 A CH 159031A CH 159031D A CH159031D A CH 159031DA CH 159031 A CH159031 A CH 159031A
Authority
CH
Switzerland
Prior art keywords
ammonium salt
production
new
pyridine
oleic acid
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH159031A publication Critical patent/CH159031A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
    • C07D213/16—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing only one pyridine ring
    • C07D213/18—Salts thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur     Herstellung    eines     Ammoninmsalzes.       Es wurde gefunden, dass man.ein neues       Ammoniumsalz    erhält, wenn man das Addi  tionsprodukt von     Pyridin    an     Äthylenchlor-          hydrin    mit     Ölsäurechlorid    behandelt.  



  Das neue Produkt, das die Konstitution  
EMI0001.0008     
    besitzt, stellt eine seifenähnliche Masse dar,  die sich in Wasser leicht unter Bildung  schäumender Lösungen löst. Es ist ein wert  voller     Hilfsstoff    für die Textilindustrie.  



  <I>Beispiel:</I>  30 Teile     Oxyäthylpyridiniumchlorid,    er  halten durch Addition von     Äthylenchlorhydrin     an     Pyridin,    werden mit     66    Teilen Ölsäure-         ehlorid    im     Olbad    unter gutem Rühren auf  110-120  erhitzt. Nach kurzer Zeit tritt  lebhafte Reaktion unter     Salzsäuregasentwick-          lung    ein, wobei die Reaktionsmasse eine sal  benartige Konsistenz annimmt. Zur Beendi  gung der Reaktion wird noch während 3  Stunden bei 1200 gerührt.



  Process for the preparation of an ammonine salt. It has been found that a new ammonium salt is obtained if the addition product of pyridine to ethylene chlorohydrin is treated with oleic acid chloride.



  The new product that the constitution
EMI0001.0008
    is a soap-like mass that easily dissolves in water to form foaming solutions. It is a valuable auxiliary material for the textile industry.



  <I> Example: </I> 30 parts of oxyäthylpyridinium chloride, obtained by adding ethylene chlorohydrin to pyridine, are heated to 110-120 with 66 parts of oleic acid chloride in an oil bath with thorough stirring. After a short time a vigorous reaction occurs with the development of hydrochloric acid gas, whereby the reaction mass takes on an ointment-like consistency. To terminate the reaction, the mixture is stirred at 1200 for a further 3 hours.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Ammoniumsalzes, dadurch gekennzeichnet, dass man das Additionsprodukt von Pyridin an Äthylenchlorhydrin mit Olsäurechlorid behandelt. Das neue Produkt, das die Konstitution EMI0001.0022 besitzt, stellt eine seifenähnliche Masse dar, die sich in Wasser leicht unter Bildung schäumender Lösungen löst. Es ist ein wert voller Hilfsstoff für die Textilindustrie. Claim: Process for the production of a new ammonium salt, characterized in that the addition product of pyridine to ethylene chlorohydrin is treated with oleic acid chloride. The new product that the constitution EMI0001.0022 is a soap-like mass that easily dissolves in water to form foaming solutions. It is a valuable auxiliary material for the textile industry.
CH159031D 1931-07-08 1931-07-08 Process for the production of an ammonium salt. CH159031A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH159031T 1931-07-08
CH156411T 1931-07-08

Publications (1)

Publication Number Publication Date
CH159031A true CH159031A (en) 1932-12-15

Family

ID=25716764

Family Applications (1)

Application Number Title Priority Date Filing Date
CH159031D CH159031A (en) 1931-07-08 1931-07-08 Process for the production of an ammonium salt.

Country Status (1)

Country Link
CH (1) CH159031A (en)

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