CH159030A - Process for the production of an ammonium salt. - Google Patents

Process for the production of an ammonium salt.

Info

Publication number
CH159030A
CH159030A CH159030DA CH159030A CH 159030 A CH159030 A CH 159030A CH 159030D A CH159030D A CH 159030DA CH 159030 A CH159030 A CH 159030A
Authority
CH
Switzerland
Prior art keywords
ammonium salt
production
new
picoline
stearic acid
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH159030A publication Critical patent/CH159030A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/06Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
    • C07D213/16Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing only one pyridine ring
    • C07D213/18Salts thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines     Ammoniumsalzes.       Es wurde gefunden, dass man ein neues       Ammoniumsalz    erhält, wenn man das Addi  tionsprodukt von     a-Picolin    an     Äthylenchlor-          hydrin    mit     Stearinsäurechlorid    behandelt.  



  Das neue Produkt, das die Konstitution  
EMI0001.0007     
    besitzt, stellt     eine    seifenähnliche Masse dar,  die sich in Wasser leicht unter Bildung  schäumender Lösungen löst. Es ist ein wert  voller     Hilfsstoff    für die     Textilindustrie.     



  <I>Beispiel:</I>  30 Teile     Oxyäthyl-a-picoliniumchlorid,    er  halten durch Addition von     Äthylenchlorhydrin     an     a-Picolin,    werden mit     56    Teilen Stearin-    Säurechlorid im Ölbad unter gutem Rühren  auf 110-120   erhitzt. Nach kurzer Zeit tritt  lebhafte Reaktion unter     Salzsäuregasentwiek-          lung    ein, wobei die Reaktionsmasse eine sal  benartige Konsistenz annimmt. Zur Beendi  gung der Reaktion wird noch während 3  Stunden bei 120   gerührt.



  Process for the production of an ammonium salt. It has been found that a new ammonium salt is obtained if the addition product of α-picoline to ethylene chlorohydrin is treated with stearic acid chloride.



  The new product that the constitution
EMI0001.0007
    is a soap-like mass that easily dissolves in water to form foaming solutions. It is a valuable auxiliary material for the textile industry.



  <I> Example: </I> 30 parts of oxyethyl-a-picolinium chloride, obtained by adding ethylene chlorohydrin to a-picoline, are heated to 110-120 with 56 parts of stearic acid chloride in an oil bath with thorough stirring. After a short time, a vigorous reaction occurs with the development of hydrochloric acid gases, the reaction mass taking on an ointment-like consistency. To terminate the reaction, the mixture is stirred at 120 for 3 hours.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Ammoniumsalzes, dadurch gekennzeichnet, dass man das Additionsprodukt von a-Picolin an Äthylenchlorhydrin mit Stearinsäurechlo- rid behandelt. Das neue Produkt, das die Konstitution EMI0001.0022 besitzt, stellt eine seifenähnliche blasse dar, die sich in Wasser leicht unter Bildung schäumender Lösungen löst. Es ist ein wert voller Hilfsstoff für die Textilindustrie. PATENT CLAIM: Process for the preparation of a new ammonium salt, characterized in that the addition product of a-picoline to ethylene chlorohydrin is treated with stearic acid chloride. The new product that the constitution EMI0001.0022 is a soap-like pale that easily dissolves in water to form foaming solutions. It is a valuable auxiliary material for the textile industry.
CH159030D 1931-07-08 1931-07-08 Process for the production of an ammonium salt. CH159030A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH156411T 1931-07-08
CH159030T 1931-07-08

Publications (1)

Publication Number Publication Date
CH159030A true CH159030A (en) 1932-12-15

Family

ID=25716763

Family Applications (1)

Application Number Title Priority Date Filing Date
CH159030D CH159030A (en) 1931-07-08 1931-07-08 Process for the production of an ammonium salt.

Country Status (1)

Country Link
CH (1) CH159030A (en)

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