CH159030A - Process for the production of an ammonium salt. - Google Patents
Process for the production of an ammonium salt.Info
- Publication number
- CH159030A CH159030A CH159030DA CH159030A CH 159030 A CH159030 A CH 159030A CH 159030D A CH159030D A CH 159030DA CH 159030 A CH159030 A CH 159030A
- Authority
- CH
- Switzerland
- Prior art keywords
- ammonium salt
- production
- new
- picoline
- stearic acid
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/16—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing only one pyridine ring
- C07D213/18—Salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines Ammoniumsalzes. Es wurde gefunden, dass man ein neues Ammoniumsalz erhält, wenn man das Addi tionsprodukt von a-Picolin an Äthylenchlor- hydrin mit Stearinsäurechlorid behandelt.
Das neue Produkt, das die Konstitution
EMI0001.0007
besitzt, stellt eine seifenähnliche Masse dar, die sich in Wasser leicht unter Bildung schäumender Lösungen löst. Es ist ein wert voller Hilfsstoff für die Textilindustrie.
<I>Beispiel:</I> 30 Teile Oxyäthyl-a-picoliniumchlorid, er halten durch Addition von Äthylenchlorhydrin an a-Picolin, werden mit 56 Teilen Stearin- Säurechlorid im Ölbad unter gutem Rühren auf 110-120 erhitzt. Nach kurzer Zeit tritt lebhafte Reaktion unter Salzsäuregasentwiek- lung ein, wobei die Reaktionsmasse eine sal benartige Konsistenz annimmt. Zur Beendi gung der Reaktion wird noch während 3 Stunden bei 120 gerührt.
Process for the production of an ammonium salt. It has been found that a new ammonium salt is obtained if the addition product of α-picoline to ethylene chlorohydrin is treated with stearic acid chloride.
The new product that the constitution
EMI0001.0007
is a soap-like mass that easily dissolves in water to form foaming solutions. It is a valuable auxiliary material for the textile industry.
<I> Example: </I> 30 parts of oxyethyl-a-picolinium chloride, obtained by adding ethylene chlorohydrin to a-picoline, are heated to 110-120 with 56 parts of stearic acid chloride in an oil bath with thorough stirring. After a short time, a vigorous reaction occurs with the development of hydrochloric acid gases, the reaction mass taking on an ointment-like consistency. To terminate the reaction, the mixture is stirred at 120 for 3 hours.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH156411T | 1931-07-08 | ||
CH159030T | 1931-07-08 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH159030A true CH159030A (en) | 1932-12-15 |
Family
ID=25716763
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH159030D CH159030A (en) | 1931-07-08 | 1931-07-08 | Process for the production of an ammonium salt. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH159030A (en) |
-
1931
- 1931-07-08 CH CH159030D patent/CH159030A/en unknown
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