CA3004503A1 - Method for the preparation of bis(fluorosulfonyl)-imide and of its salts - Google Patents
Method for the preparation of bis(fluorosulfonyl)-imide and of its salts Download PDFInfo
- Publication number
- CA3004503A1 CA3004503A1 CA3004503A CA3004503A CA3004503A1 CA 3004503 A1 CA3004503 A1 CA 3004503A1 CA 3004503 A CA3004503 A CA 3004503A CA 3004503 A CA3004503 A CA 3004503A CA 3004503 A1 CA3004503 A1 CA 3004503A1
- Authority
- CA
- Canada
- Prior art keywords
- compound
- formula
- done
- mixture
- step1
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
- C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
- C01B21/0935—Imidodisulfonic acid; Nitrilotrisulfonic acid; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
- C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (63)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201562254860P | 2015-11-13 | 2015-11-13 | |
| EP15194513.6 | 2015-11-13 | ||
| US62/254,860 | 2015-11-13 | ||
| EP15194513 | 2015-11-13 | ||
| EP15195231.4 | 2015-11-18 | ||
| EP15195231 | 2015-11-18 | ||
| US201662290523P | 2016-02-03 | 2016-02-03 | |
| EP16153983.8 | 2016-02-03 | ||
| EP16153983 | 2016-02-03 | ||
| US62/290,523 | 2016-02-03 | ||
| US201662308313P | 2016-03-15 | 2016-03-15 | |
| US62/308,313 | 2016-03-15 | ||
| EP16160248 | 2016-03-15 | ||
| EP16160245.3 | 2016-03-15 | ||
| EP16160245 | 2016-03-15 | ||
| EP16160248.7 | 2016-03-15 | ||
| EP16163043.9 | 2016-03-30 | ||
| EP16163043 | 2016-03-30 | ||
| EP16163045.4 | 2016-03-30 | ||
| EP16163045 | 2016-03-30 | ||
| EP16163835 | 2016-04-05 | ||
| EP16163835.8 | 2016-04-05 | ||
| EP16164023 | 2016-04-06 | ||
| EP16164023.0 | 2016-04-06 | ||
| EP16164146.9 | 2016-04-07 | ||
| EP16164148.5 | 2016-04-07 | ||
| EP16164146 | 2016-04-07 | ||
| EP16164148 | 2016-04-07 | ||
| EP16164373.9 | 2016-04-08 | ||
| EP16164371.3 | 2016-04-08 | ||
| EP16164373 | 2016-04-08 | ||
| EP16164371 | 2016-04-08 | ||
| EP16164595 | 2016-04-11 | ||
| EP16164593 | 2016-04-11 | ||
| EP16164593.2 | 2016-04-11 | ||
| EP16164595.7 | 2016-04-11 | ||
| EP16167626.7 | 2016-04-29 | ||
| EP16167626 | 2016-04-29 | ||
| EP16167634 | 2016-04-29 | ||
| EP16167634.1 | 2016-04-29 | ||
| EP16180255.8 | 2016-07-20 | ||
| EP16180254.1 | 2016-07-20 | ||
| EP16180255 | 2016-07-20 | ||
| EP16180254 | 2016-07-20 | ||
| EP16180274.9 | 2016-07-20 | ||
| EP16180274 | 2016-07-20 | ||
| EP16188591.8 | 2016-09-13 | ||
| EP16188590.0 | 2016-09-13 | ||
| EP16188590 | 2016-09-13 | ||
| EP16188591 | 2016-09-13 | ||
| EP16189474 | 2016-09-19 | ||
| EP16189382.1 | 2016-09-19 | ||
| EP16189478 | 2016-09-19 | ||
| EP16189383.9 | 2016-09-19 | ||
| EP16189478.7 | 2016-09-19 | ||
| EP16189474.6 | 2016-09-19 | ||
| EP16189382 | 2016-09-19 | ||
| EP16189383 | 2016-09-19 | ||
| EP16193206 | 2016-10-11 | ||
| EP16193206.6 | 2016-10-11 | ||
| EP16195489 | 2016-10-25 | ||
| EP16195489.6 | 2016-10-25 | ||
| PCT/EP2016/075836 WO2017080831A1 (en) | 2015-11-13 | 2016-10-26 | Method for the preparation of bis(fluorosulfonyl)-imide and of its salts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA3004503A1 true CA3004503A1 (en) | 2017-05-18 |
Family
ID=58694705
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3004503A Abandoned CA3004503A1 (en) | 2015-11-13 | 2016-10-26 | Method for the preparation of bis(fluorosulfonyl)-imide and of its salts |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20180362343A1 (enExample) |
| EP (1) | EP3334684A1 (enExample) |
| JP (1) | JP2018535181A (enExample) |
| KR (1) | KR20180083896A (enExample) |
| CN (1) | CN108349737A (enExample) |
| CA (1) | CA3004503A1 (enExample) |
| WO (1) | WO2017080831A1 (enExample) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109264682B (zh) * | 2017-07-18 | 2019-11-29 | 九江天赐高新材料有限公司 | 一种高纯度二氟磺酰亚胺的制备方法 |
| CN109835876B (zh) * | 2017-11-28 | 2022-11-29 | 株式会社日本触媒 | 双(氟磺酰)亚胺锂组合物 |
| FR3081723B1 (fr) * | 2018-06-01 | 2022-04-15 | Arkema France | Procede de purification d'un sel de lithium de bis(fluorosulfonyl)imide |
| FR3081725A1 (fr) * | 2018-06-01 | 2019-12-06 | Arkema France | Procede de purification d'un sel de lithium du bis(fluorosulfonyl)imide |
| CN109264683B (zh) * | 2018-10-16 | 2021-07-27 | 广州理文科技有限公司 | 一种双（氟磺酰）亚胺的提取与纯化方法 |
| US10967295B2 (en) | 2018-11-16 | 2021-04-06 | Ses Holdings Pte. Ltd. | Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries |
| US10926190B2 (en) * | 2018-11-16 | 2021-02-23 | Ses Holdings Pte. Ltd. | Purified lithium bis(fluorosulfonyl)imide (LiFSI) products, methods of purifying crude LiFSI, and uses of purified LiFSI products |
| US10734664B1 (en) * | 2019-03-01 | 2020-08-04 | Ses Holdings Pte. Ltd. | Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products |
| CN109721037B (zh) * | 2019-03-11 | 2019-12-24 | 上海如鲲新材料有限公司 | 一种双氟磺酰亚胺盐的新工艺 |
| KR102285464B1 (ko) * | 2019-03-28 | 2021-08-03 | 주식회사 천보 | 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법 |
| CN109928372A (zh) * | 2019-04-12 | 2019-06-25 | 广州理文科技有限公司 | 一种双氟磺酰亚胺的制备方法 |
| US11267707B2 (en) | 2019-04-16 | 2022-03-08 | Honeywell International Inc | Purification of bis(fluorosulfonyl) imide |
| FR3095440B1 (fr) * | 2019-04-25 | 2022-03-25 | Arkema France | Procédé de préparation du bis(fluorosulfonyle) imide |
| US12319571B2 (en) | 2019-05-23 | 2025-06-03 | Nippon Shokubai Co., Ltd. | Bis(fluorosulfonyl)imide compound and method for producing same |
| WO2021031430A1 (en) | 2019-08-22 | 2021-02-25 | Fujian Yongjing Technology Co., Ltd | New process for the synthesis of fluorinated conductive salts for lithium ion batteries |
| US20240308849A1 (en) * | 2021-06-30 | 2024-09-19 | Chunbo Co., Ltd | Bis(fluorosulfonyl)imide alkali metal salt |
| FR3130787B1 (fr) * | 2021-12-16 | 2023-11-03 | Arkema France | Procédé de préparation du bis(fluorosulfonyl)imidure de lithium |
| KR20260016502A (ko) * | 2023-06-02 | 2026-02-03 | 스페셜티 오퍼레이션스 프랑스 | 미정제 플루오로설포닐이미드 화합물로부터 하나 이상의 표적 불순물을 제거하는 방법 |
| CN119191240B (zh) * | 2024-10-11 | 2025-11-18 | 福州大学 | 一种利用反应-萃取技术连续合成LiFSI的方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4385047A (en) | 1981-01-05 | 1983-05-24 | Smithkline Beckman Corporation | Antiallergic imidodisulfamides |
| CA2527575A1 (en) * | 2005-12-12 | 2007-06-12 | Christophe Michot | Salts and their utilization |
| US7919629B2 (en) | 2005-12-12 | 2011-04-05 | Phostech Lithium Inc. | Sulphonyl-1,2,4-triazole salts |
| CA2527802A1 (en) * | 2005-12-12 | 2007-06-12 | Christophe Michot | Synthesis of anhydrous imides lithium salts containing fluorosulfonyl or fluorophosphoryl substituent |
| CN101980955B (zh) * | 2008-03-31 | 2013-07-03 | 株式会社日本触媒 | 磺酰亚胺盐及其制备方法 |
| KR101291903B1 (ko) * | 2008-07-23 | 2013-07-31 | 다이이치 고교 세이야쿠 가부시키가이샤 | 비스(플루오로설포닐)이미드 음이온 화합물의 제조 방법과 이온대화합물 |
| EP2505551B2 (en) | 2009-11-27 | 2022-03-09 | Nippon Shokubai Co., Ltd. | Fluorosulfonyl imide salt and method for producing fluorosulfonyl imide salt |
| JP5401336B2 (ja) * | 2010-01-15 | 2014-01-29 | 株式会社日本触媒 | フルオロスルホニルイミド塩の製造方法 |
| EP3736250B1 (en) | 2010-05-28 | 2023-07-26 | Nippon Shokubai Co., Ltd. | Alkali metal salt of fluorosulfonyl imide |
| EP2674395B1 (en) | 2011-02-10 | 2017-12-27 | Nippon Soda Co., Ltd. | Process for production of fluorosulfonylimide ammonium salt |
| KR101632857B1 (ko) | 2011-03-03 | 2016-06-22 | 닛뽕소다 가부시키가이샤 | 불소 함유 술포닐이미드염의 제조 방법 |
| KR101702656B1 (ko) | 2011-03-03 | 2017-02-03 | 닛뽕소다 가부시키가이샤 | 플루오로술포닐이미드암모늄염의 제조 방법 |
| FR2975694B1 (fr) * | 2011-05-24 | 2013-08-02 | Arkema France | Procede de preparation de bis(fluorosulfonyl)imidure de lithium |
| FR2998297B1 (fr) | 2012-11-22 | 2014-11-14 | Arkema France | Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle |
| CN106167455B (zh) | 2013-07-11 | 2018-09-14 | 隆萨有限公司 | 用于制备酰亚胺基二硫酰化合物的方法 |
| US8722005B1 (en) | 2013-07-26 | 2014-05-13 | Boulder Ionics Corporation | Synthesis of hydrogen bis(fluorosulfonyl)imide |
| CN104925765B (zh) * | 2015-05-21 | 2017-08-08 | 上海康鹏科技有限公司 | 一种双氟磺酰亚胺锂盐的制备方法 |
-
2016
- 2016-10-26 KR KR1020187016542A patent/KR20180083896A/ko not_active Withdrawn
- 2016-10-26 EP EP16788084.8A patent/EP3334684A1/en not_active Withdrawn
- 2016-10-26 WO PCT/EP2016/075836 patent/WO2017080831A1/en not_active Ceased
- 2016-10-26 CN CN201680064971.XA patent/CN108349737A/zh active Pending
- 2016-10-26 US US15/775,687 patent/US20180362343A1/en not_active Abandoned
- 2016-10-26 JP JP2018524477A patent/JP2018535181A/ja not_active Withdrawn
- 2016-10-26 CA CA3004503A patent/CA3004503A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| CN108349737A (zh) | 2018-07-31 |
| WO2017080831A1 (en) | 2017-05-18 |
| JP2018535181A (ja) | 2018-11-29 |
| EP3334684A1 (en) | 2018-06-20 |
| KR20180083896A (ko) | 2018-07-23 |
| US20180362343A1 (en) | 2018-12-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20220426 |