CA2878356C - Free flowing sodium chloride salt composition prepared by evaporative crystallization - Google Patents
Free flowing sodium chloride salt composition prepared by evaporative crystallization Download PDFInfo
- Publication number
- CA2878356C CA2878356C CA2878356A CA2878356A CA2878356C CA 2878356 C CA2878356 C CA 2878356C CA 2878356 A CA2878356 A CA 2878356A CA 2878356 A CA2878356 A CA 2878356A CA 2878356 C CA2878356 C CA 2878356C
- Authority
- CA
- Canada
- Prior art keywords
- salt
- crystals
- ppm
- water
- shaped
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 11
- 238000002425 crystallisation Methods 0.000 title claims abstract description 9
- 230000008025 crystallization Effects 0.000 title claims abstract description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 title claims description 9
- 150000003839 salts Chemical class 0.000 claims abstract description 103
- 229920000058 polyacrylate Polymers 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000000654 additive Substances 0.000 claims abstract description 12
- 230000000996 additive effect Effects 0.000 claims abstract description 11
- 238000001704 evaporation Methods 0.000 claims abstract description 8
- 239000012452 mother liquor Substances 0.000 claims abstract description 8
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 7
- 229920001577 copolymer Polymers 0.000 claims description 7
- 238000005868 electrolysis reaction Methods 0.000 claims description 6
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000012528 membrane Substances 0.000 claims description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 2
- 239000011976 maleic acid Substances 0.000 claims description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 2
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical group OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 235000002639 sodium chloride Nutrition 0.000 description 90
- 239000013078 crystal Substances 0.000 description 78
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 29
- 239000012267 brine Substances 0.000 description 27
- 239000000523 sample Substances 0.000 description 26
- 238000012360 testing method Methods 0.000 description 16
- 239000000843 powder Substances 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 9
- 239000000243 solution Substances 0.000 description 7
- 229920002125 Sokalan® Polymers 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 6
- 229920006395 saturated elastomer Polymers 0.000 description 6
- 230000035515 penetration Effects 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 230000009969 flowable effect Effects 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000012266 salt solution Substances 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000012047 saturated solution Substances 0.000 description 2
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 2
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 2
- 229940045919 sodium polymetaphosphate Drugs 0.000 description 2
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 2
- XHZPRMZZQOIPDS-UHFFFAOYSA-N 2-Methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(C)(C)NC(=O)C=C XHZPRMZZQOIPDS-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000004520 agglutination Effects 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 238000004619 light microscopy Methods 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- FVZVCSNXTFCBQU-UHFFFAOYSA-N phosphanyl Chemical group [PH2] FVZVCSNXTFCBQU-UHFFFAOYSA-N 0.000 description 1
- MEUIIHOXOWVKNP-UHFFFAOYSA-N phosphanylformic acid Chemical compound OC(P)=O MEUIIHOXOWVKNP-UHFFFAOYSA-N 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920000447 polyanionic polymer Polymers 0.000 description 1
- 229920005996 polystyrene-poly(ethylene-butylene)-polystyrene Polymers 0.000 description 1
- 239000013074 reference sample Substances 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
- C01D3/06—Preparation by working up brines; seawater or spent lyes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/14—Purification
- C01D3/16—Purification by precipitation or adsorption
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/22—Preparation in the form of granules, pieces, or other shaped products
- C01D3/24—Influencing the crystallisation process
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/02—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form
- C25B11/03—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form perforated or foraminous
- C25B11/031—Porous electrodes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Electrochemistry (AREA)
- Metallurgy (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Seasonings (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12176201.7 | 2012-07-12 | ||
| EP12176201 | 2012-07-12 | ||
| US201261680811P | 2012-08-08 | 2012-08-08 | |
| US61/680,811 | 2012-08-08 | ||
| PCT/EP2013/064577 WO2014009411A1 (en) | 2012-07-12 | 2013-07-10 | Free flowing salt composition prepared by evaporative crystallization |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2878356A1 CA2878356A1 (en) | 2014-01-16 |
| CA2878356C true CA2878356C (en) | 2020-09-01 |
Family
ID=49915436
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2878356A Active CA2878356C (en) | 2012-07-12 | 2013-07-10 | Free flowing sodium chloride salt composition prepared by evaporative crystallization |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9394182B2 (show.php) |
| EP (1) | EP2872446B1 (show.php) |
| JP (1) | JP5973664B2 (show.php) |
| KR (1) | KR102040743B1 (show.php) |
| CN (1) | CN104411639B (show.php) |
| AU (1) | AU2013288808B2 (show.php) |
| BR (1) | BR112015000173B1 (show.php) |
| CA (1) | CA2878356C (show.php) |
| CL (1) | CL2015000013A1 (show.php) |
| EA (1) | EA028693B1 (show.php) |
| IL (1) | IL236178B (show.php) |
| IN (1) | IN2014DN10826A (show.php) |
| TN (1) | TN2014000527A1 (show.php) |
| WO (1) | WO2014009411A1 (show.php) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2018332654B2 (en) * | 2017-09-18 | 2022-07-21 | S & P Ingredient Development, Llc | Low sodium salt substitute with potassium chloride |
| CN111302362B (zh) * | 2020-04-03 | 2021-05-07 | 天津科技大学 | 一种大颗粒球形盐及其制备方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB822893A (en) * | 1955-07-21 | 1959-11-04 | Palmer Mann And Company Ltd | Crystallisation of salt |
| DE1265151B (de) * | 1959-08-10 | 1968-04-04 | Wintershall Ag | Verfahren zur verwachsungsfreien Kristallisation von Steinsalz |
| JPH01145320A (ja) * | 1987-11-30 | 1989-06-07 | Japan Tobacco Inc | ８〜１４面体結晶食塩製造方法 |
| JPH01145319A (ja) | 1987-11-30 | 1989-06-07 | Japan Tobacco Inc | ８〜１４面体結晶食塩の製造方法 |
| JPH0624973B2 (ja) * | 1990-11-07 | 1994-04-06 | 那須 久太 | 天然産出塩の塩分離方法 |
| JP3370348B2 (ja) | 1991-01-11 | 2003-01-27 | 丸尾カルシウム株式会社 | 分散剤 |
| JP3249677B2 (ja) * | 1993-02-05 | 2002-01-21 | 日本錬水株式会社 | アルカリ金属塩化物の電解方法 |
| DE19902395C2 (de) | 1999-01-22 | 2001-05-03 | Kali & Salz Ag | Verfahren zur Verengung des Kornspektrums von Kalium- und Natriumchloridkristallisaten zur Verbesserung der Rieseleigenschaften |
| DE10063291A1 (de) | 2000-12-19 | 2002-06-20 | Skw Polymers Gmbh | Verwendung von Fließmitteln auf Polycarboxylat-Basis für Anhydrit-basierte Fließestriche |
| DE60202609T2 (de) | 2001-07-09 | 2005-12-29 | Akzo Nobel N.V. | Verfahren zur herstellung von hochreinem feuchtem salz, so erhältliches feuchtes salz und verwendung davon bei einem elektrolyseverfahren |
| EA006738B1 (ru) * | 2001-08-21 | 2006-04-28 | Акцо Нобель Н.В. | Соингибиторы для получения очищенного насыщенного солевого раствора |
| ES2279216T3 (es) | 2002-08-08 | 2007-08-16 | Akzo Nobel N.V. | Procedimiento para fabricar sal de gran pureza y su uso en procesos de electrolisis. |
| EP1753895A2 (en) | 2004-06-08 | 2007-02-21 | Akzo Nobel N.V. | Process for preventing membrane degeneration using complexing agents |
| CN101044091B (zh) | 2004-10-22 | 2011-05-25 | 阿克佐诺贝尔股份有限公司 | 从盐水中结晶二价阴离子的可溶性盐的方法 |
| DK1858806T3 (da) * | 2005-02-18 | 2009-05-25 | Akzo Nobel Nv | Fremgangsmåde til fremstilling af salt |
| EP1848661B1 (en) | 2005-02-18 | 2018-08-01 | Akzo Nobel Chemicals International B.V. | Process to prepare chlorine or sodium chlorate |
| EP2423165A1 (en) * | 2007-08-23 | 2012-02-29 | Dow Global Technologies LLC | Process, adapted microbes, composition and apparatus for purification of industrial brine |
| JP5532199B2 (ja) | 2008-11-07 | 2014-06-25 | 株式会社豊田中央研究所 | 金属化合物のコロイド溶液およびその製造方法 |
| CN101559340B (zh) | 2009-05-18 | 2012-01-25 | 中国科学院长春应用化学研究所 | 一种制备无团聚纳米材料的方法 |
| CN101585549B (zh) | 2009-06-18 | 2011-05-11 | 中盐制盐工程技术研究院 | 工业盐的制备方法和电解制烧碱的方法 |
| EP2377900B1 (en) | 2010-04-16 | 2013-07-31 | Omya Development AG | Process to prepare surface-modified mineral material, resulting products and uses thereof |
| DK2390284T4 (en) | 2010-05-28 | 2017-06-19 | Omya Int Ag | Process for preparing suspensions of high solids mineral materials |
-
2013
- 2013-07-10 IN IN10826DEN2014 patent/IN2014DN10826A/en unknown
- 2013-07-10 CA CA2878356A patent/CA2878356C/en active Active
- 2013-07-10 JP JP2015520973A patent/JP5973664B2/ja active Active
- 2013-07-10 WO PCT/EP2013/064577 patent/WO2014009411A1/en not_active Ceased
- 2013-07-10 EP EP13736550.8A patent/EP2872446B1/en active Active
- 2013-07-10 CN CN201380034842.2A patent/CN104411639B/zh active Active
- 2013-07-10 EA EA201590155A patent/EA028693B1/ru not_active IP Right Cessation
- 2013-07-10 US US14/412,936 patent/US9394182B2/en active Active
- 2013-07-10 AU AU2013288808A patent/AU2013288808B2/en active Active
- 2013-07-10 BR BR112015000173-4A patent/BR112015000173B1/pt active IP Right Grant
- 2013-07-10 KR KR1020157003177A patent/KR102040743B1/ko active Active
-
2014
- 2014-12-11 IL IL236178A patent/IL236178B/en active IP Right Grant
- 2014-12-19 TN TN2014000527A patent/TN2014000527A1/fr unknown
-
2015
- 2015-01-05 CL CL2015000013A patent/CL2015000013A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2872446A1 (en) | 2015-05-20 |
| IL236178A0 (en) | 2015-01-29 |
| BR112015000173A2 (pt) | 2017-06-27 |
| TN2014000527A1 (en) | 2016-03-30 |
| JP5973664B2 (ja) | 2016-08-23 |
| EP2872446B1 (en) | 2020-01-22 |
| AU2013288808A1 (en) | 2015-01-22 |
| IN2014DN10826A (show.php) | 2015-09-04 |
| IL236178B (en) | 2019-07-31 |
| US20150191361A1 (en) | 2015-07-09 |
| EA201590155A1 (ru) | 2015-04-30 |
| US9394182B2 (en) | 2016-07-19 |
| AU2013288808B2 (en) | 2016-04-07 |
| EA028693B1 (ru) | 2017-12-29 |
| CN104411639A (zh) | 2015-03-11 |
| BR112015000173B1 (pt) | 2021-07-27 |
| CA2878356A1 (en) | 2014-01-16 |
| CL2015000013A1 (es) | 2015-06-12 |
| WO2014009411A1 (en) | 2014-01-16 |
| JP2015527967A (ja) | 2015-09-24 |
| KR102040743B1 (ko) | 2019-11-05 |
| CN104411639B (zh) | 2018-06-29 |
| KR20150030757A (ko) | 2015-03-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20180416 |