CA1210221A - Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute purete - Google Patents
Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute pureteInfo
- Publication number
- CA1210221A CA1210221A CA000433086A CA433086A CA1210221A CA 1210221 A CA1210221 A CA 1210221A CA 000433086 A CA000433086 A CA 000433086A CA 433086 A CA433086 A CA 433086A CA 1210221 A CA1210221 A CA 1210221A
- Authority
- CA
- Canada
- Prior art keywords
- trichlorosilane
- silicon
- reaction
- hydrogen
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 239000005052 trichlorosilane Substances 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims abstract description 8
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 5
- 229920001296 polysiloxane Polymers 0.000 title 1
- 239000007789 gas Substances 0.000 claims abstract description 43
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000000203 mixture Substances 0.000 claims abstract description 26
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 239000005049 silicon tetrachloride Substances 0.000 claims abstract description 23
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 19
- 239000010703 silicon Substances 0.000 claims abstract description 19
- 239000001257 hydrogen Substances 0.000 claims abstract description 18
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 18
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 230000009467 reduction Effects 0.000 claims abstract description 15
- 238000010791 quenching Methods 0.000 claims abstract description 14
- 230000000171 quenching effect Effects 0.000 claims abstract description 12
- 239000011541 reaction mixture Substances 0.000 claims abstract description 10
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052802 copper Inorganic materials 0.000 claims abstract description 6
- 239000010949 copper Substances 0.000 claims abstract description 6
- 239000003054 catalyst Substances 0.000 claims abstract description 4
- 239000012429 reaction media Substances 0.000 claims abstract description 4
- 239000011261 inert gas Substances 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 2
- 238000011403 purification operation Methods 0.000 claims 1
- 238000000354 decomposition reaction Methods 0.000 abstract description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 20
- 238000006722 reduction reaction Methods 0.000 description 14
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 9
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical class ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 5
- 229910052786 argon Inorganic materials 0.000 description 5
- 239000011863 silicon-based powder Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 230000009466 transformation Effects 0.000 description 4
- 238000005755 formation reaction Methods 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 229910003822 SiHCl3 Inorganic materials 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical compound Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 description 2
- ZFAYZXMSTVMBLX-UHFFFAOYSA-J silicon(4+);tetrachloride Chemical compound [Si+4].[Cl-].[Cl-].[Cl-].[Cl-] ZFAYZXMSTVMBLX-UHFFFAOYSA-J 0.000 description 2
- 239000005046 Chlorosilane Substances 0.000 description 1
- 229910003910 SiCl4 Inorganic materials 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical group Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 1
- SLLGVCUQYRMELA-UHFFFAOYSA-N chlorosilicon Chemical compound Cl[Si] SLLGVCUQYRMELA-UHFFFAOYSA-N 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007323 disproportionation reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 150000003376 silicon Chemical class 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/107—Halogenated silanes
- C01B33/1071—Tetrachloride, trichlorosilane or silicochloroform, dichlorosilane, monochlorosilane or mixtures thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/09—Reaction techniques
- Y10S423/10—Plasma energized
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8212971A FR2530638A1 (fr) | 1982-07-26 | 1982-07-26 | Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute purete |
| FR82.12971 | 1982-07-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1210221A true CA1210221A (fr) | 1986-08-26 |
Family
ID=9276302
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000433086A Expired CA1210221A (fr) | 1982-07-26 | 1983-07-25 | Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute purete |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4836997A (show.php) |
| EP (1) | EP0100266B1 (show.php) |
| JP (1) | JPS5945920A (show.php) |
| CA (1) | CA1210221A (show.php) |
| DE (1) | DE3371190D1 (show.php) |
| FR (1) | FR2530638A1 (show.php) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112573522A (zh) * | 2020-12-14 | 2021-03-30 | 亚洲硅业(青海)股份有限公司 | 硅基电子特气的制备方法及硅基电子特气的生产系统 |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5422088A (en) * | 1994-01-28 | 1995-06-06 | Hemlock Semiconductor Corporation | Process for hydrogenation of tetrachlorosilane |
| US5869017A (en) * | 1997-05-12 | 1999-02-09 | Tokuyama Corporation | Method of producing trichlorosilane having a reduced content of dichlorosilane |
| RU2142909C1 (ru) * | 1998-07-30 | 1999-12-20 | Институт химии высокочистых веществ РАН | Способ получения высокочистого трихлорсилана и устройство для его осуществления |
| KR100385947B1 (ko) * | 2000-12-06 | 2003-06-02 | 삼성전자주식회사 | 원자층 증착 방법에 의한 박막 형성 방법 |
| DE102005005044A1 (de) * | 2005-02-03 | 2006-08-10 | Consortium für elektrochemische Industrie GmbH | Verfahren zur Herstellung von Trichlorsilan mittels thermischer Hydrierung von Siliciumtetrachlorid |
| DE102005024041A1 (de) * | 2005-05-25 | 2006-11-30 | City Solar Ag | Verfahren zur Herstellung von Silicium aus Halogensilanen |
| DE102005041137A1 (de) * | 2005-08-30 | 2007-03-01 | Degussa Ag | Reaktor, Anlage und großtechnisches Verfahren zur kontinuierlichen Herstellung von hochreinem Siliciumtetrachlorid oder hochreinem Germaniumtetrachlorid |
| DE102006043929B4 (de) * | 2006-09-14 | 2016-10-06 | Spawnt Private S.À.R.L. | Verfahren zur Herstellung von festen Polysilanmischungen |
| JP5601438B2 (ja) * | 2006-11-07 | 2014-10-08 | 三菱マテリアル株式会社 | トリクロロシランの製造方法およびトリクロロシラン製造装置 |
| RU2350558C2 (ru) * | 2007-05-02 | 2009-03-27 | Федеральное государственное унитарное предприятие "Горно-химический комбинат" | Способ получения трихлорсилана плазмохимическим гидрированием тетрахлорида кремния и устройство для его осуществления |
| DE102007041803A1 (de) * | 2007-08-30 | 2009-03-05 | Pv Silicon Forschungs Und Produktions Gmbh | Verfahren zur Herstellung von polykristallinen Siliziumstäben und polykristalliner Siliziumstab |
| US20100273010A1 (en) * | 2009-03-19 | 2010-10-28 | Robert Froehlich | Silicide-coated metal surfaces and methods of utilizing same |
| AU2010239350A1 (en) * | 2009-04-20 | 2011-11-10 | Ae Polysilicon Corporation | A reactor with silicide-coated metal surfaces |
| JP2012524022A (ja) * | 2009-04-20 | 2012-10-11 | エーイー ポリシリコン コーポレーション | 高純度ポリシリコンの製造方法及び装置 |
| TWI454309B (zh) * | 2009-04-20 | 2014-10-01 | Jiangsu Zhongneng Polysilicon Technology Dev Co Ltd | 用於將反應排出氣體冷卻之方法及系統 |
| KR20100117025A (ko) * | 2009-04-23 | 2010-11-02 | 스미또모 가가꾸 가부시키가이샤 | 포토레지스트 패턴 형성 방법 |
| DE102009037155B3 (de) * | 2009-08-04 | 2010-11-04 | Schmid Silicon Technology Gmbh | Verfahren und Anlage zur Herstellung von Trichlorsilan |
| KR20120124061A (ko) | 2010-01-26 | 2012-11-12 | 다우 코닝 코포레이션 | 오가노할로실란의 제조 방법 |
| US8722915B2 (en) | 2010-05-28 | 2014-05-13 | Dow Corning Corporation | Preparation of organohalosilanes |
| JP5726294B2 (ja) | 2010-05-28 | 2015-05-27 | ダウ コーニング コーポレーションＤｏｗ Ｃｏｒｎｉｎｇ Ｃｏｒｐｏｒａｔｉｏｎ | ジオルガノジハロシランの調製方法 |
| DE102010044755A1 (de) | 2010-09-08 | 2012-03-08 | Spawnt Private S.À.R.L. | Verfahren zur Herstellung von Silicium hoher Reinheit |
| US8765090B2 (en) | 2010-09-08 | 2014-07-01 | Dow Corning Corporation | Method for preparing a trihalosilane |
| JP2014501243A (ja) | 2010-12-17 | 2014-01-20 | ダウ コーニング コーポレーション | ジオルガノジハロシランの製造方法 |
| RU2013117809A (ru) | 2010-12-17 | 2015-01-27 | Дау Корнинг Корпорейшн | Способ получения тригалогенсилана |
| BR112013018039A2 (pt) | 2011-01-25 | 2019-09-24 | Dow Corning | método de preparação de um di-organo-di-halossilano |
| WO2013059686A1 (en) * | 2011-10-20 | 2013-04-25 | Rec Silicon Inc | Fouling reduction in hydrochlorosilane production |
| US20150030520A1 (en) * | 2012-03-14 | 2015-01-29 | Centrotherm Photovoltaics Usa, Inc. | Trichlorosilane production |
| FR2991988B1 (fr) | 2012-06-15 | 2015-08-07 | Laurent Laroche | Procede de preparation d'objets en hydrogel biocompatible pour leur application dans le domaine medical, et plus particulierement en ophtalmologie |
| CN104736547A (zh) | 2012-08-13 | 2015-06-24 | 道康宁公司 | 通过使氢、卤硅烷和有机卤化物在铜催化剂上以两步法反应制备有机卤硅烷的方法 |
| US9422316B2 (en) | 2012-10-16 | 2016-08-23 | Dow Corning Corporation | Method of preparing halogenated silahydrocarbylenes |
| DE102013207444A1 (de) * | 2013-04-24 | 2014-10-30 | Evonik Degussa Gmbh | Verfahren und Vorrichtung zur Herstellung von Polychlorsilanen |
| JP6479794B2 (ja) | 2013-11-12 | 2019-03-06 | ダウ シリコーンズ コーポレーション | ハロシランを製造する方法 |
| WO2016099690A1 (en) | 2014-12-18 | 2016-06-23 | Dow Corning Corporation | Method for producing aryl-functional silanes |
| CN113072074A (zh) * | 2021-04-25 | 2021-07-06 | 森松（江苏）重工有限公司 | 还原炉的炉筒冷却方法、装置及多晶硅还原生产方法 |
| CN113912066A (zh) * | 2021-09-09 | 2022-01-11 | 全椒亚格泰电子新材料科技有限公司 | 一种制备氯代硅烷的方法 |
| CN116835599A (zh) * | 2023-07-03 | 2023-10-03 | 四川永祥能源科技有限公司 | 一种高沸物回收方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3069239A (en) * | 1958-10-28 | 1962-12-18 | Westinghouse Electric Corp | Purification of halogenated silicon compounds |
| GB883326A (en) * | 1959-04-08 | 1961-11-29 | Bbc Brown Boveri & Cie | Method of producing trichlorsilane |
| FR1239350A (fr) * | 1959-06-24 | 1960-12-16 | Pechiney | Perfectionnement à la fabrication industrielle du trichlorosilane |
| DE1129145B (de) * | 1960-07-07 | 1962-05-10 | Knapsack Ag | Verfahren zur Herstellung von hochreinem Silicium |
| FR1292508A (fr) * | 1960-07-07 | 1962-05-04 | Knapsack Ag | Procédé de fabrication de silicium de grande pureté |
| US3899573A (en) * | 1971-10-18 | 1975-08-12 | Exxon Research Engineering Co | Production of fine powders |
| US4309259A (en) * | 1980-05-09 | 1982-01-05 | Motorola, Inc. | High pressure plasma hydrogenation of silicon tetrachloride |
| US4321246A (en) * | 1980-05-09 | 1982-03-23 | Motorola, Inc. | Polycrystalline silicon production |
| DE3024319C2 (de) * | 1980-06-27 | 1983-07-21 | Wacker-Chemitronic Gesellschaft für Elektronik-Grundstoffe mbH, 8263 Burghausen | Kontinuierliches Verfahren zur Herstellung von Trichlorsilan |
| JPS57156318A (en) * | 1981-03-16 | 1982-09-27 | Koujiyundo Silicon Kk | Production of trichlorosilane |
| US4451436A (en) * | 1983-02-01 | 1984-05-29 | Hare Louis R O | Nitrogen fixation by plasma and catalyst |
-
1982
- 1982-07-26 FR FR8212971A patent/FR2530638A1/fr active Granted
-
1983
- 1983-07-13 DE DE8383401454T patent/DE3371190D1/de not_active Expired
- 1983-07-13 EP EP83401454A patent/EP0100266B1/fr not_active Expired
- 1983-07-25 CA CA000433086A patent/CA1210221A/fr not_active Expired
- 1983-07-25 JP JP58134511A patent/JPS5945920A/ja active Granted
- 1983-07-25 US US06/516,843 patent/US4836997A/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112573522A (zh) * | 2020-12-14 | 2021-03-30 | 亚洲硅业(青海)股份有限公司 | 硅基电子特气的制备方法及硅基电子特气的生产系统 |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2530638A1 (fr) | 1984-01-27 |
| FR2530638B1 (show.php) | 1985-02-22 |
| DE3371190D1 (en) | 1987-06-04 |
| JPS6261530B2 (show.php) | 1987-12-22 |
| EP0100266B1 (fr) | 1987-04-29 |
| JPS5945920A (ja) | 1984-03-15 |
| EP0100266A1 (fr) | 1984-02-08 |
| US4836997A (en) | 1989-06-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |