BR112014030076A2 - método para produção de composto de politiol, composição polimerizável para material ótico, e usos dos mesmos - Google Patents
método para produção de composto de politiol, composição polimerizável para material ótico, e usos dos mesmosInfo
- Publication number
- BR112014030076A2 BR112014030076A2 BR112014030076A BR112014030076A BR112014030076A2 BR 112014030076 A2 BR112014030076 A2 BR 112014030076A2 BR 112014030076 A BR112014030076 A BR 112014030076A BR 112014030076 A BR112014030076 A BR 112014030076A BR 112014030076 A2 BR112014030076 A2 BR 112014030076A2
- Authority
- BR
- Brazil
- Prior art keywords
- polymerizable composition
- polythiol compound
- optical material
- following formula
- temperature
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 239000000463 material Substances 0.000 title abstract 2
- 230000003287 optical effect Effects 0.000 title abstract 2
- 229920005862 polyol Polymers 0.000 title 1
- -1 polyol compound Chemical class 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 8
- 229920006295 polythiol Polymers 0.000 abstract 5
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 abstract 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 4
- 150000005846 sugar alcohols Polymers 0.000 abstract 2
- DGVVWUTYPXICAM-UHFFFAOYSA-N β‐Mercaptoethanol Chemical compound OCCS DGVVWUTYPXICAM-UHFFFAOYSA-N 0.000 abstract 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
- C08G18/3855—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
- C08G18/3876—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing mercapto groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
- C07C319/08—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
- C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C335/30—Isothioureas
- C07C335/32—Isothioureas having sulfur atoms of isothiourea groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
- C08G18/7628—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group
- C08G18/7642—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group containing at least two isocyanate or isothiocyanate groups linked to the aromatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate groups, e.g. xylylene diisocyanate or homologues substituted on the aromatic ring
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
- G02B1/041—Lenses
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012179896 | 2012-08-14 | ||
| PCT/JP2013/001207 WO2014027427A1 (ja) | 2012-08-14 | 2013-02-28 | ポリチオール化合物の製造方法、光学材料用重合性組成物およびその用途 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR112014030076A2 true BR112014030076A2 (pt) | 2017-06-27 |
Family
ID=50685489
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112014030076A BR112014030076A2 (pt) | 2012-08-14 | 2013-02-28 | método para produção de composto de politiol, composição polimerizável para material ótico, e usos dos mesmos |
| BR112015000373A BR112015000373A2 (pt) | 2012-08-14 | 2013-02-28 | metódo para produzir composto de politiol, composição polimerizável para material ótico e usos dos mesmos |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112015000373A BR112015000373A2 (pt) | 2012-08-14 | 2013-02-28 | metódo para produzir composto de politiol, composição polimerizável para material ótico e usos dos mesmos |
Country Status (7)
| Country | Link |
|---|---|
| US (4) | US9181179B2 (enExample) |
| EP (4) | EP3093282B1 (enExample) |
| KR (4) | KR101879962B1 (enExample) |
| CN (4) | CN105906773B (enExample) |
| BR (2) | BR112014030076A2 (enExample) |
| IN (2) | IN2014DN09746A (enExample) |
| WO (2) | WO2014027428A1 (enExample) |
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| JP5373226B1 (ja) | 2012-08-14 | 2013-12-18 | 三井化学株式会社 | ポリチオール組成物、光学材料用重合性組成物およびその用途 |
| WO2014136663A1 (ja) | 2013-03-04 | 2014-09-12 | 三菱瓦斯化学株式会社 | 光学材料用組成物及びそれを用いた光学材料 |
| EP2801586B1 (de) | 2013-05-07 | 2016-04-13 | Bruno Bock Chemische Fabrik GmbH & Co. KG | Gießharz auf Polythiourethanbasis mit hoher Bruchfestigkeit und niedrigem spezifischen Gewicht |
| CN105683160B (zh) | 2013-11-01 | 2018-02-16 | 三菱瓦斯化学株式会社 | 多硫醇化合物及其制造方法 |
| TWI699389B (zh) * | 2014-07-18 | 2020-07-21 | 日商三菱瓦斯化學股份有限公司 | 聚硫醇組成物及其製造方法 |
| CN104402783B (zh) * | 2014-12-15 | 2015-08-12 | 黄河三角洲京博化工研究院有限公司 | 一种巯基化合物的制备方法 |
| JPWO2017175407A1 (ja) * | 2016-04-06 | 2019-02-14 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | 光学部材の製造方法 |
| CN105693575B (zh) * | 2016-04-08 | 2018-06-29 | 佛山汉维科技有限公司 | 一种分离纯化多元硫醇的方法与设备 |
| CN105949096B (zh) * | 2016-05-19 | 2018-03-02 | 湖北鼎龙控股股份有限公司 | 光学眼镜片材料、精制多元硫醇以及多元硫醇粗品的后处理方法 |
| EP3480185B1 (en) * | 2016-06-30 | 2021-04-14 | Hoya Lens Thailand Ltd. | Method for preparing polythiol compound, method for preparing curable composition, and method for producing cured product |
| WO2018003061A1 (ja) * | 2016-06-30 | 2018-01-04 | ホヤ レンズ タイランド リミテッド | 硬化物の製造方法、硬化物および眼鏡レンズ基材 |
| WO2018012803A1 (ko) * | 2016-07-14 | 2018-01-18 | 에스케이씨 주식회사 | 광학 재료용 방향족 폴리티올 화합물 |
| JP6632493B2 (ja) | 2016-08-05 | 2020-01-22 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法 |
| JP6633990B2 (ja) * | 2016-08-08 | 2020-01-22 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法 |
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| KR101885879B1 (ko) * | 2016-08-30 | 2018-08-07 | 에스케이씨 주식회사 | 광학 재료용 폴리티올 조성물 및 이의 제조방법 |
| US10365958B2 (en) * | 2016-09-13 | 2019-07-30 | Hewlett Packard Enterprise Development Lp | Storage drive management to fail a storage drive based on adjustable failure criteria |
| JP6851762B2 (ja) * | 2016-09-30 | 2021-03-31 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | 光学材料用ポリチオール化合物の製造方法 |
| JP2018058922A (ja) * | 2016-09-30 | 2018-04-12 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | 光学材料の製造方法 |
| CN106831511B (zh) * | 2017-01-24 | 2018-05-25 | 郯城博化化工科技有限公司 | 一种多元硫醇化合物的制备方法 |
| KR101893558B1 (ko) * | 2017-02-03 | 2018-08-30 | 에스케이씨 주식회사 | 플라스틱 렌즈용 중합성 조성물 |
| US20200031986A1 (en) * | 2017-02-15 | 2020-01-30 | Keun Sik Kim | Polyol or polythiol compound, preparation method therefor, transparent polyurethane-based resin prepared therefrom, and optical body |
| CN110446696A (zh) * | 2017-03-24 | 2019-11-12 | 三井化学株式会社 | 多元硫醇化合物的制造方法、聚合性组合物及其用途 |
| KR101902974B1 (ko) * | 2017-03-31 | 2018-10-02 | 에스케이씨 주식회사 | 폴리티올 화합물의 탈수 방법 |
| CN107235876B (zh) * | 2017-06-30 | 2019-01-18 | 山东益丰生化环保股份有限公司 | 一种多巯基化合物粗产物的后处理方法 |
| KR101996981B1 (ko) * | 2017-10-18 | 2019-07-05 | 에스케이씨 주식회사 | 플라스틱 렌즈용 중합성 조성물 |
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| JP6797855B2 (ja) * | 2018-03-29 | 2020-12-09 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法 |
| JP6797856B2 (ja) * | 2018-03-29 | 2020-12-09 | ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ | ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法 |
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| KR102034214B1 (ko) * | 2018-04-25 | 2019-10-18 | 에스케이씨 주식회사 | 보관안정성이 개선된 폴리티올의 제조방법 |
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| CN110305049B (zh) * | 2019-07-08 | 2021-05-28 | 山东益丰生化环保股份有限公司 | 一种生产低色度聚硫醇化合物的方法 |
| US12269913B2 (en) | 2019-07-17 | 2025-04-08 | Mitsui Chemicals, Inc. | Polythiol composition and applications thereof |
| CN110835409B (zh) * | 2019-12-03 | 2020-08-28 | 山东益丰生化环保股份有限公司 | 一种利用微通道反应器连续反应生产聚硫醇的方法 |
| US11578038B2 (en) * | 2019-12-13 | 2023-02-14 | Skc Co., Ltd. | Method for preparing polythiol composition |
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| JP7437932B2 (ja) * | 2019-12-27 | 2024-02-26 | 三井化学株式会社 | 廃水処理方法 |
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| KR102122703B1 (ko) | 2020-04-09 | 2020-06-26 | 주식회사 대원에프엔씨 | 폴리티올 화합물의 제조 방법과 이를 포함한 광학 재료용 중합성 조성물 및 광학 렌즈 |
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| CN114765982B (zh) | 2020-11-13 | 2024-06-28 | 三井化学株式会社 | 多硫醇组合物、聚合性组合物、树脂、成型体、光学材料及透镜 |
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| JPWO2024070537A1 (enExample) | 2022-09-26 | 2024-04-04 | ||
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| US5191055A (en) | 1988-12-22 | 1993-03-02 | Mitsui Toatsu Chemicals, Inc. | Mercapto compound, a high refractive index resin and lens and a process for preparing them |
| JP2621991B2 (ja) | 1988-12-22 | 1997-06-18 | 三井東圧化学株式会社 | メルカプト化合物及びその製造方法 |
| US5087758A (en) | 1988-12-22 | 1992-02-11 | Mitsui Toatsu Chemicals, Inc. | Mercapto compound, a high refractive index resin and lens and a process for preparing them |
| US5608115A (en) | 1994-01-26 | 1997-03-04 | Mitsui Toatsu Chemicals, Inc. | Polythiol useful for preparing sulfur-containing urethane-based resin and process for producing the same |
| JP4426017B2 (ja) | 1999-07-27 | 2010-03-03 | 三井化学株式会社 | 有機メルカプト化合物の製造方法 |
| CN1171924C (zh) * | 2002-11-05 | 2004-10-20 | 浙江大学 | 一种制备聚硫代氨基甲酸酯光学塑料的方法 |
| WO2007088556A1 (en) * | 2006-01-31 | 2007-08-09 | Shriram Institute For Industrial Research | An improved lens of diethyleνε glycol bis allyl carbonate cr-39 and a process for preparation thereof |
| US20090264613A1 (en) | 2006-04-19 | 2009-10-22 | Mitsui Chemicals, Inc. | Process for producing (poly)thiol compound for use as optical material, and polymerizable composition containing the compound |
| KR20110033960A (ko) | 2006-04-20 | 2011-04-01 | 미쓰이 가가쿠 가부시키가이샤 | 광학재료용 폴리티올 화합물의 제조방법 및 그것을 포함하는 중합성 조성물 |
| KR101016322B1 (ko) | 2008-12-30 | 2011-02-22 | 주식회사 포스코 | 이송 벨트 가이드 장치 |
| CN101614831B (zh) * | 2009-08-11 | 2010-10-27 | 杭州新顺化工有限公司 | 高折射率树脂镜片及其制备方法 |
| KR20120058635A (ko) | 2010-08-13 | 2012-06-08 | 주식회사 케이오씨솔루션 | 광학렌즈용 폴리티올 화합물의 제조법 및 이를 포함하는 수지 조성물 |
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2013
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- 2013-02-28 KR KR1020167004566A patent/KR101879962B1/ko active Active
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- 2013-02-28 KR KR1020167004565A patent/KR20160028486A/ko not_active Withdrawn
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