BR112012030778A2 - processo para a preparação de uma mistura de agentes quelantes - Google Patents
processo para a preparação de uma mistura de agentes quelantesInfo
- Publication number
- BR112012030778A2 BR112012030778A2 BR112012030778A BR112012030778A BR112012030778A2 BR 112012030778 A2 BR112012030778 A2 BR 112012030778A2 BR 112012030778 A BR112012030778 A BR 112012030778A BR 112012030778 A BR112012030778 A BR 112012030778A BR 112012030778 A2 BR112012030778 A2 BR 112012030778A2
- Authority
- BR
- Brazil
- Prior art keywords
- derivative
- amino acid
- preparing
- formula
- mixture
- Prior art date
Links
- 239000002738 chelating agent Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 title abstract 2
- CHEXFUSQDLIYJQ-WNQIDUERSA-N OC(=O)[C@@H](N)CC(O)=O.CCOOC(=O)CCC(=O)OOCC Chemical compound OC(=O)[C@@H](N)CC(O)=O.CCOOC(=O)CCC(=O)OOCC CHEXFUSQDLIYJQ-WNQIDUERSA-N 0.000 abstract 2
- 150000003862 amino acid derivatives Chemical class 0.000 abstract 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 abstract 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 2
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910001413 alkali metal ion Chemical group 0.000 abstract 1
- 229910052784 alkaline earth metal Chemical group 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical group 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 abstract 1
- 235000003704 aspartic acid Nutrition 0.000 abstract 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000004985 diamines Chemical class 0.000 abstract 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 abstract 1
- 229940043237 diethanolamine Drugs 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 125000001841 imino group Chemical group [H]N=* 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/04—Formation of amino groups in compounds containing carboxyl groups
- C07C227/10—Formation of amino groups in compounds containing carboxyl groups with simultaneously increasing the number of carbon atoms in the carbon skeleton
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/04—Formation of amino groups in compounds containing carboxyl groups
- C07C227/06—Formation of amino groups in compounds containing carboxyl groups by addition or substitution reactions, without increasing the number of carbon atoms in the carbon skeleton of the acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/26—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one amino group bound to the carbon skeleton, e.g. lysine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
processo para preparação de uma mistura dde agentes quelantes. a presente invenção se refere a um processo para a preparação de dietoxi succinato de ácido aspartico e um derivado de aminoácido da fórmula geral em que n é 1-10, m é o 0 ou 1, r é hidrogênio ou um íon de metal alcali ou metal alcalino terroso, compreendendo reagir maleato com dietanol amina sob condições alcalinas na presença de um catalisador lantanóide para formar dietoxi succinato de ácido aspártico seguido por adição de ácido aspártico que reage com maleato não reagido para formar ácido imino disuccínio, isto é, um derivado de aminoácido de fórmula i que m é 0, ou por meio da adição de um derivado de diamina da fórmula geral nh~ 2~ (ch~ 2~) ~ n~nh~ 2~ em que n é como definido acima, que reage com maleato não reagido para formar um derivado de aminoácido de fórmula i em que m é 1 e n é como definido acima.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI20105622A FI122829B (fi) | 2010-06-02 | 2010-06-02 | Menetelmä kelatointiaineiden seoksen valmistamiseksi |
| FI20105622 | 2010-06-02 | ||
| PCT/FI2011/050504 WO2011151517A2 (en) | 2010-06-02 | 2011-05-31 | Process for the preparation of a mixture of chelating agents |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR112012030778A2 true BR112012030778A2 (pt) | 2017-12-05 |
| BR112012030778B1 BR112012030778B1 (pt) | 2018-07-31 |
Family
ID=42308080
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112012030778-9A BR112012030778B1 (pt) | 2010-06-02 | 2011-05-31 | Processo para a preparação de uma mistura de agentes quelantes |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US9090536B2 (pt) |
| EP (1) | EP2576499B1 (pt) |
| CN (1) | CN102933544B (pt) |
| BR (1) | BR112012030778B1 (pt) |
| CA (1) | CA2801340C (pt) |
| CL (1) | CL2012003352A1 (pt) |
| ES (1) | ES2531186T3 (pt) |
| FI (1) | FI122829B (pt) |
| PL (1) | PL2576499T3 (pt) |
| RU (1) | RU2551285C2 (pt) |
| WO (1) | WO2011151517A2 (pt) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104447370B (zh) * | 2014-04-03 | 2015-09-23 | 石家庄开发区德赛化工有限公司 | 一种亚氨基二琥珀酸盐螯合剂的制备方法 |
| WO2016060685A1 (en) | 2014-10-17 | 2016-04-21 | Halliburton Energy Services, Inc. | Low ph metal-free preparation of aminated organic acid |
| RU2585020C1 (ru) * | 2015-06-16 | 2016-05-27 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Тверской государственный университет" | Способ получения комплексообразующего сорбента |
| MX2018014197A (es) | 2016-06-30 | 2019-02-25 | Halliburton Energy Services Inc | Acidos iminodialcanoicos sulfonatados formados por un iminodialquilnitrilo y una sultona y metodos para utilizarlos. |
| CN107162748A (zh) * | 2017-06-13 | 2017-09-15 | 山东远联化工有限公司 | 一种增效剂yl‑101及其应用 |
| WO2019002685A1 (en) | 2017-06-30 | 2019-01-03 | Kemira Oyj | PROCESS FOR THE PREPARATION OF A MIXTURE OF CHELATING AGENTS, MIXTURE OF CHELATING AGENTS AND METHODS OF USE THEREOF |
| RU2761831C2 (ru) * | 2017-06-30 | 2021-12-13 | Кемира Ойй | Способ получения смеси хелатообразующих агентов, смесь хелатообразующих агентов и способы ее применения |
| CN111393313A (zh) * | 2020-04-16 | 2020-07-10 | 河北协同环保科技股份有限公司 | 一种亚氨基二琥珀酸盐生产中提高转化率的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1710552A1 (ru) * | 1990-04-28 | 1992-02-07 | Тверской государственный университет | Способ получени солей комплексонов |
| JPH09143132A (ja) | 1995-11-21 | 1997-06-03 | Fuji Photo Film Co Ltd | アミン類とα， β−不飽和化合物の付加生成物の製造方法 |
| FI112075B (fi) | 1996-05-30 | 2003-10-31 | Kemira Chemicals Oy | N-bis- tai N-tris-[(1,2-dikarboksyyli-etoksi)-etyyli]amiinijohdannaiset, niiden valmistus ja käyttö |
| FI105932B (fi) * | 1996-05-30 | 2000-10-31 | Kemira Chemicals Oy | Menetelmä korkeasaanto- tai kierrätysmassan valkaisemiseksi |
| FI106258B (fi) * | 1998-03-09 | 2000-12-29 | Kemira Chemicals Oy | Menetelmiä N-bis-[2-(1,2-dikarboksi-etoksi)-etyyli]amiinijohdannaisen valmistamiseksi sekä menetelmien tuotteet ja niiden käytöt |
| FI117392B (fi) | 1999-03-02 | 2006-09-29 | Kemira Oyj | Monivaiheinen valkaisumenetelmä kemiallisen selluloosamassan valkaisemiseksi |
| DE60020318T2 (de) * | 1999-09-03 | 2006-05-18 | Nippon Shokubai Co., Ltd. | Zusammensetzung von Aminosäure-Derivaten und Verfahren zur Herstellung von einem Aminosäure-Derivat |
-
2010
- 2010-06-02 FI FI20105622A patent/FI122829B/fi active
-
2011
- 2011-05-31 WO PCT/FI2011/050504 patent/WO2011151517A2/en active Application Filing
- 2011-05-31 EP EP11728021.4A patent/EP2576499B1/en active Active
- 2011-05-31 PL PL11728021T patent/PL2576499T3/pl unknown
- 2011-05-31 CN CN201180025787.1A patent/CN102933544B/zh not_active Expired - Fee Related
- 2011-05-31 ES ES11728021T patent/ES2531186T3/es active Active
- 2011-05-31 US US13/639,575 patent/US9090536B2/en not_active Expired - Fee Related
- 2011-05-31 BR BR112012030778-9A patent/BR112012030778B1/pt not_active IP Right Cessation
- 2011-05-31 RU RU2012154341/04A patent/RU2551285C2/ru active
- 2011-05-31 CA CA2801340A patent/CA2801340C/en active Active
-
2012
- 2012-11-29 CL CL2012003352A patent/CL2012003352A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RU2012154341A (ru) | 2014-07-20 |
| BR112012030778B1 (pt) | 2018-07-31 |
| FI20105622A (fi) | 2011-12-03 |
| ES2531186T3 (es) | 2015-03-11 |
| US9090536B2 (en) | 2015-07-28 |
| CA2801340A1 (en) | 2011-12-08 |
| WO2011151517A3 (en) | 2012-03-22 |
| CL2012003352A1 (es) | 2013-07-12 |
| RU2551285C2 (ru) | 2015-05-20 |
| EP2576499B1 (en) | 2014-12-03 |
| FI122829B (fi) | 2012-07-31 |
| WO2011151517A2 (en) | 2011-12-08 |
| CA2801340C (en) | 2017-06-27 |
| CN102933544A (zh) | 2013-02-13 |
| US20130204035A1 (en) | 2013-08-08 |
| FI20105622A0 (fi) | 2010-06-02 |
| PL2576499T3 (pl) | 2015-04-30 |
| EP2576499A2 (en) | 2013-04-10 |
| CN102933544B (zh) | 2014-09-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] | ||
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 13A ANUIDADE. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2777 DE 26-03-2024 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |