ATE296808T1 - Verfahren zur herstellung von thiobarbitursäurederivaten - Google Patents
Verfahren zur herstellung von thiobarbitursäurederivatenInfo
- Publication number
- ATE296808T1 ATE296808T1 AT00906277T AT00906277T ATE296808T1 AT E296808 T1 ATE296808 T1 AT E296808T1 AT 00906277 T AT00906277 T AT 00906277T AT 00906277 T AT00906277 T AT 00906277T AT E296808 T1 ATE296808 T1 AT E296808T1
- Authority
- AT
- Austria
- Prior art keywords
- hydrogenolysis
- acid derivatives
- alkali metal
- formula
- thiobarbituric acid
- Prior art date
Links
- RVBUGGBMJDPOST-UHFFFAOYSA-N 2-thiobarbituric acid Chemical class O=C1CC(=O)NC(=S)N1 RVBUGGBMJDPOST-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 6
- 238000007327 hydrogenolysis reaction Methods 0.000 abstract 4
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000012442 inert solvent Substances 0.000 abstract 2
- RRKHIAYNPVQKEF-UHFFFAOYSA-N Pyriftalid Chemical compound COC1=CC(OC)=NC(SC=2C=3C(=O)OC(C)C=3C=CC=2)=N1 RRKHIAYNPVQKEF-UHFFFAOYSA-N 0.000 abstract 1
- 229910001413 alkali metal ion Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 abstract 1
- 230000011987 methylation Effects 0.000 abstract 1
- 238000007069 methylation reaction Methods 0.000 abstract 1
- 125000002653 sulfanylmethyl group Chemical group [H]SC([H])([H])[*] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
- C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
- C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
- C07D239/60—Three or more oxygen or sulfur atoms
- C07D239/66—Thiobarbituric acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
- C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
- C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
- C07D239/60—Three or more oxygen or sulfur atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH22499 | 1999-02-05 | ||
| PCT/EP2000/000872 WO2000046213A2 (en) | 1999-02-05 | 2000-02-03 | Method of producing thiobarbituric acid derivatives |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE296808T1 true ATE296808T1 (de) | 2005-06-15 |
Family
ID=4182122
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT00906277T ATE296808T1 (de) | 1999-02-05 | 2000-02-03 | Verfahren zur herstellung von thiobarbitursäurederivaten |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US6673925B2 (de) |
| EP (1) | EP1165524B1 (de) |
| JP (1) | JP3602796B2 (de) |
| KR (1) | KR100453755B1 (de) |
| CN (1) | CN1151137C (de) |
| AT (1) | ATE296808T1 (de) |
| AU (1) | AU752278B2 (de) |
| BR (1) | BR0008029B1 (de) |
| CA (1) | CA2358940C (de) |
| DE (1) | DE60020539T2 (de) |
| ES (1) | ES2243233T3 (de) |
| HU (1) | HUP0200090A3 (de) |
| IL (1) | IL144354A0 (de) |
| PL (1) | PL197892B1 (de) |
| RU (1) | RU2242467C2 (de) |
| TW (1) | TWI220428B (de) |
| UA (1) | UA71600C2 (de) |
| WO (1) | WO2000046213A2 (de) |
| ZA (1) | ZA200106299B (de) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3507483B1 (ja) | 2000-07-21 | 2004-03-15 | シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト | ４，６−ジメトキシ−２−（メチルスルホニル）−１，３−ピリミジンの製造方法 |
| AR033765A1 (es) * | 2001-05-22 | 2004-01-07 | Syngenta Participations Ag | Procedimiento para la preparacion de derivados 3-alquil-3h-isobenzofuran-1-ona 7-sustituidos. |
| US9527820B1 (en) | 2016-05-05 | 2016-12-27 | King Saud University | Diethylammonium salts of phenyl-substituted thiobarbituric acid as anti-diabetic agents |
| CN116675678A (zh) * | 2023-06-06 | 2023-09-01 | 顺毅南通化工有限公司 | 一种环酯草醚的合成方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1466177A (en) | 1973-03-23 | 1977-03-02 | Sandoz Ltd | 4-hydroxy-pyrimidine derivatives |
| US4057634A (en) | 1974-01-24 | 1977-11-08 | Hoechst Aktiengesellschaft | Antiprotozoal(1-alkyl-5-nitro-imidazolyl-2-alkyl)-pyridazines |
| DE2403340A1 (de) * | 1974-01-24 | 1975-07-31 | Hoechst Ag | (1-alkyl-5-nitro-imidazolyl-2-alkyl)- heteroaryl-verbindungen und verfahren zu ihrer herstellung |
| US4923501A (en) * | 1987-11-04 | 1990-05-08 | Kumiai Chemical Industry Co., Ltd. | Pyrimidine derivatives, processes for their production, and herbicidal method and compositions |
| CA2076690C (en) * | 1991-08-30 | 2003-01-07 | Jean-Paul Roduit | Process for the production of 2-(methylthio)-disodium barbiturate |
| KR100233068B1 (ko) * | 1991-11-26 | 1999-12-01 | 하인즈 모제르 | 2-치환된 4,6-디알콕시피리미딘의 제조방법 |
| EP0565951A1 (de) * | 1992-04-13 | 1993-10-20 | Nihon Bayer Agrochem K.K. | Herbizides wirksam Pyrimidinylthioalkanderivate |
| RU2078080C1 (ru) * | 1994-02-02 | 1997-04-27 | Акатьев Виталий Евгеньевич | Способ получения тиобарбитуровой кислоты |
-
2000
- 2000-02-02 TW TW089101784A patent/TWI220428B/zh not_active IP Right Cessation
- 2000-02-03 RU RU2001123929/04A patent/RU2242467C2/ru not_active IP Right Cessation
- 2000-02-03 DE DE60020539T patent/DE60020539T2/de not_active Expired - Lifetime
- 2000-02-03 WO PCT/EP2000/000872 patent/WO2000046213A2/en not_active Ceased
- 2000-02-03 AT AT00906277T patent/ATE296808T1/de active
- 2000-02-03 IL IL14435400A patent/IL144354A0/xx not_active IP Right Cessation
- 2000-02-03 ES ES00906277T patent/ES2243233T3/es not_active Expired - Lifetime
- 2000-02-03 PL PL349726A patent/PL197892B1/pl unknown
- 2000-02-03 JP JP2000597283A patent/JP3602796B2/ja not_active Expired - Fee Related
- 2000-02-03 BR BRPI0008029-2A patent/BR0008029B1/pt not_active IP Right Cessation
- 2000-02-03 CA CA002358940A patent/CA2358940C/en not_active Expired - Fee Related
- 2000-02-03 CN CNB008034508A patent/CN1151137C/zh not_active Expired - Fee Related
- 2000-02-03 AU AU28014/00A patent/AU752278B2/en not_active Ceased
- 2000-02-03 HU HU0200090A patent/HUP0200090A3/hu unknown
- 2000-02-03 KR KR10-2001-7009512A patent/KR100453755B1/ko not_active Expired - Fee Related
- 2000-02-03 EP EP00906277A patent/EP1165524B1/de not_active Expired - Lifetime
- 2000-03-02 UA UA2001096117A patent/UA71600C2/uk unknown
-
2001
- 2001-07-31 ZA ZA200106299A patent/ZA200106299B/en unknown
- 2001-08-20 US US09/936,330 patent/US6673925B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR20020011961A (ko) | 2002-02-09 |
| TWI220428B (en) | 2004-08-21 |
| BR0008029A (pt) | 2001-11-13 |
| UA71600C2 (uk) | 2004-12-15 |
| EP1165524B1 (de) | 2005-06-01 |
| HUP0200090A3 (en) | 2002-12-28 |
| CA2358940A1 (en) | 2000-08-10 |
| DE60020539T2 (de) | 2006-04-27 |
| IL144354A0 (en) | 2002-05-23 |
| DE60020539D1 (de) | 2005-07-07 |
| ZA200106299B (en) | 2002-09-27 |
| AU2801400A (en) | 2000-08-25 |
| KR100453755B1 (ko) | 2004-10-20 |
| RU2242467C2 (ru) | 2004-12-20 |
| US20020095037A1 (en) | 2002-07-18 |
| ES2243233T3 (es) | 2005-12-01 |
| HUP0200090A2 (hu) | 2002-11-28 |
| JP2003520762A (ja) | 2003-07-08 |
| EP1165524A2 (de) | 2002-01-02 |
| CA2358940C (en) | 2009-04-07 |
| JP3602796B2 (ja) | 2004-12-15 |
| US6673925B2 (en) | 2004-01-06 |
| WO2000046213A2 (en) | 2000-08-10 |
| AU752278B2 (en) | 2002-09-12 |
| BR0008029B1 (pt) | 2010-06-15 |
| PL197892B1 (pl) | 2008-05-30 |
| CN1151137C (zh) | 2004-05-26 |
| CN1339029A (zh) | 2002-03-06 |
| WO2000046213A3 (en) | 2000-12-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification |
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