ATE228109T1 - Verfahren zur raffination von butylacrylat - Google Patents
Verfahren zur raffination von butylacrylatInfo
- Publication number
- ATE228109T1 ATE228109T1 AT97925718T AT97925718T ATE228109T1 AT E228109 T1 ATE228109 T1 AT E228109T1 AT 97925718 T AT97925718 T AT 97925718T AT 97925718 T AT97925718 T AT 97925718T AT E228109 T1 ATE228109 T1 AT E228109T1
- Authority
- AT
- Austria
- Prior art keywords
- butyl acrylate
- butyl
- bottoms
- butanol
- heavies
- Prior art date
Links
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 3
- 238000007670 refining Methods 0.000 title abstract 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 6
- 238000004821 distillation Methods 0.000 abstract 3
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 abstract 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract 2
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 abstract 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/859,143 US6605738B1 (en) | 1996-05-29 | 1997-05-20 | Processes for refining butyl acrylate |
| PCT/US1997/008814 WO1998052904A1 (en) | 1997-05-20 | 1997-05-27 | Processes for refining butylacrylate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE228109T1 true ATE228109T1 (de) | 2002-12-15 |
Family
ID=25330156
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT97925718T ATE228109T1 (de) | 1997-05-20 | 1997-05-27 | Verfahren zur raffination von butylacrylat |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0984918B1 (de) |
| JP (1) | JP3934163B2 (de) |
| KR (1) | KR100462266B1 (de) |
| CN (1) | CN1099405C (de) |
| AT (1) | ATE228109T1 (de) |
| BR (1) | BR9714713A (de) |
| DE (1) | DE69717314T2 (de) |
| WO (1) | WO1998052904A1 (de) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1028109A1 (de) * | 1999-02-12 | 2000-08-16 | Dsm N.V. | Verfahren zur Herstellung von Epsilon-Caprolactam |
| JP2003521478A (ja) * | 1999-06-17 | 2003-07-15 | ユニオン・カーバイド・ケミカルズ・アンド・プラスティックス・テクノロジー・コーポレイション | 平衡律速反応を行う方法 |
| US6482976B1 (en) | 1999-06-17 | 2002-11-19 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for conducting equilibrium-limited reactions |
| US6180820B1 (en) * | 1999-09-14 | 2001-01-30 | Celanese International Corporation | Process for the production and purification of N-butyl acrylate |
| US6172258B1 (en) * | 1999-09-14 | 2001-01-09 | Celanese International Corporation | Process for the production and purification of n-butyl acrylate |
| JP2001181233A (ja) * | 1999-10-12 | 2001-07-03 | Nippon Shokubai Co Ltd | (メタ)アクリル酸エステルの製造方法 |
| US6649787B1 (en) | 1999-10-12 | 2003-11-18 | Nippon Shokubai Co., Ltd. | Method for preparing (meth) acrylic acid ester |
| WO2001085666A2 (en) * | 2000-05-09 | 2001-11-15 | Union Carbide Chemicals & Plastics Technology Corporation | Improved refining processes |
| EP1611082B1 (de) | 2003-02-28 | 2010-08-11 | Arkema Inc. | Verfahren zur durchführung von gleichgewichtsbegrenzten reaktionen |
| JP2008266159A (ja) * | 2007-04-17 | 2008-11-06 | Mitsubishi Chemicals Corp | アクリル酸ブチルの精製方法 |
| ATE519728T1 (de) * | 2008-01-18 | 2011-08-15 | Arkema Inc | Verfahren zur rückgewinnung eines sulfonsäurekatalysators und wertprodukten aus acrylatnachlauffraktionen |
| JP5169899B2 (ja) * | 2009-02-19 | 2013-03-27 | 東亞合成株式会社 | アクリル酸アルキルエステルの製造方法 |
| KR101144306B1 (ko) * | 2010-08-26 | 2012-05-11 | 주식회사 엘지화학 | 알킬(메트)아크릴레이트의 제조 방법 |
| FR3008971B1 (fr) * | 2013-07-29 | 2016-08-19 | Arkema France | Procede de production en continu d'acrylates legers par esterification d'un acide acrylique de grade ester brut |
| FR3014870B1 (fr) * | 2013-12-13 | 2015-12-11 | Arkema France | Procede de production d'esters (meth)acryliques |
| JP6287269B2 (ja) * | 2014-01-30 | 2018-03-07 | 三菱ケミカル株式会社 | アクリル酸ブチルの製造方法 |
| JP6522127B2 (ja) | 2014-11-28 | 2019-05-29 | プライメタルズ テクノロジーズ オーストリア ゲー・エム・ベー・ハーPrimetals Technologies Austria GmbH | クラウン制御を備える金属ストリップをキャスティングする方法 |
| KR102475938B1 (ko) * | 2015-02-27 | 2022-12-08 | 주식회사 쿠라레 | (메트)아크릴 수지 조성물의 제조 방법 |
| CN104844456B (zh) * | 2015-04-17 | 2017-06-13 | 江苏新东风化工科技有限公司 | 一种丙烯酸正丁酯废油回收工艺及装置 |
| CN110937997A (zh) * | 2019-12-09 | 2020-03-31 | 东营海德新材料有限公司 | 一种提高丙烯酸丁酯纯度的生产工艺 |
| CN113121348A (zh) * | 2021-03-15 | 2021-07-16 | 江苏新东风化工科技有限公司 | 一种丙烯酸正丁酯生产脱醚工艺 |
| WO2023006499A1 (de) | 2021-07-29 | 2023-02-02 | Basf Se | Verfahren zur kontinuierlichen destillation von acrylaten |
| CN118302405A (zh) * | 2021-11-25 | 2024-07-05 | 巴斯夫欧洲公司 | 用于生产c6-c12-烷基(甲基)丙烯酸酯的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2449811C2 (de) * | 1974-10-19 | 1983-01-05 | Hoechst Ag, 6000 Frankfurt | Verfahren zur kontinuierlichen Herstellung von dibutylätherfreiem n-Butylacrylat |
| DE2552987C2 (de) * | 1975-11-26 | 1983-09-29 | Hoechst Ag, 6230 Frankfurt | Verfahren zur kontinuierlichen Herstellung ätherfreier Acrylsäurealkylester |
| JPS5877845A (ja) * | 1981-11-02 | 1983-05-11 | Nippon Shokubai Kagaku Kogyo Co Ltd | アクリル酸エステルまたはメタクリル酸エステルの製造方法 |
| US4814493A (en) * | 1983-07-05 | 1989-03-21 | Hoechst Celanese Corporation | Process for production of alkyl acrylates |
| JPH089567B2 (ja) * | 1992-01-09 | 1996-01-31 | 株式会社日本触媒 | アクリル酸製造においてアクリル酸を高純度に精製する方法 |
| FR2723089B1 (fr) * | 1994-07-28 | 1996-09-06 | Atochem Elf Sa | Procede de fabrication de l'acrylate de butyle par esterification directe |
| DE19536178A1 (de) * | 1995-09-28 | 1997-04-03 | Basf Ag | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure |
-
1997
- 1997-05-27 AT AT97925718T patent/ATE228109T1/de not_active IP Right Cessation
- 1997-05-27 WO PCT/US1997/008814 patent/WO1998052904A1/en not_active Ceased
- 1997-05-27 DE DE69717314T patent/DE69717314T2/de not_active Expired - Lifetime
- 1997-05-27 BR BR9714713-3A patent/BR9714713A/pt not_active IP Right Cessation
- 1997-05-27 CN CN97182208A patent/CN1099405C/zh not_active Expired - Lifetime
- 1997-05-27 KR KR10-1999-7010423A patent/KR100462266B1/ko not_active Expired - Lifetime
- 1997-05-27 JP JP55031698A patent/JP3934163B2/ja not_active Expired - Lifetime
- 1997-05-27 EP EP97925718A patent/EP0984918B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| WO1998052904A1 (en) | 1998-11-26 |
| JP3934163B2 (ja) | 2007-06-20 |
| KR100462266B1 (ko) | 2004-12-17 |
| JP2002507194A (ja) | 2002-03-05 |
| KR20010012468A (ko) | 2001-02-15 |
| CN1099405C (zh) | 2003-01-22 |
| BR9714713A (pt) | 2000-07-04 |
| DE69717314D1 (de) | 2003-01-02 |
| EP0984918A1 (de) | 2000-03-15 |
| DE69717314T2 (de) | 2003-08-21 |
| EP0984918B1 (de) | 2002-11-20 |
| CN1254331A (zh) | 2000-05-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |