BRPI0408730A - processo e aparelhagem para separar um óxido de propileno purificado - Google Patents
processo e aparelhagem para separar um óxido de propileno purificadoInfo
- Publication number
- BRPI0408730A BRPI0408730A BRPI0408730-5A BRPI0408730A BRPI0408730A BR PI0408730 A BRPI0408730 A BR PI0408730A BR PI0408730 A BRPI0408730 A BR PI0408730A BR PI0408730 A BRPI0408730 A BR PI0408730A
- Authority
- BR
- Brazil
- Prior art keywords
- propylene oxide
- purified
- propylene
- separating
- product
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/38—Steam distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/40—Extractive distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
"PROCESSO E APARELHAGEM PARA SEPARAR UM óXIDO DE PROPILENO PURIFICADO". A presente invenção refere-se a um processo para separar um óxido de propileno purificado de um produto de epoxidação bruto produzido, preferivelmente, em uma reação de epoxidação de propileno com peróxido de hidrogênio. O processo envolve remover água em massa, metanol em massa e propileno não reagido do produto de epoxidação bruto e em seguida submeter o produto de óxido de propileno resultante a destilação extrativa com água como solvente de extração. Sob condições de destilação, incluindo uma temperatura de fundos maiores que cerca de 55<198>C e menor que cerca de 75<198>C, é obtida uma corrente de destilado de topo ou de derivação contendo um óxido de propileno purificado com baixa perda de rendimento de óxido de propileno a propileno glicóis e outros pesados de glicóis. o óxido de propileno purificado pode ser adicionalmente purificado através de uma destilação de acabamento de maneira a obter óxido de propileno atendendo aos requisitos de pureza grau comercial.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US45550603P | 2003-03-18 | 2003-03-18 | |
PCT/US2004/006529 WO2004083196A1 (en) | 2003-03-18 | 2004-03-04 | Purification of propylene oxide resulting from epoxidation of propylene with hydrogen peroxide |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0408730A true BRPI0408730A (pt) | 2006-03-07 |
BRPI0408730B1 BRPI0408730B1 (pt) | 2016-03-22 |
Family
ID=33030012
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0408730A BRPI0408730B1 (pt) | 2003-03-18 | 2004-03-04 | processo e aparelhagem para separar um óxido de propileno purificado |
Country Status (11)
Country | Link |
---|---|
US (1) | US7594979B2 (pt) |
EP (2) | EP1606273B1 (pt) |
JP (1) | JP4673297B2 (pt) |
KR (1) | KR101071025B1 (pt) |
CN (2) | CN103819427A (pt) |
AT (1) | ATE446958T1 (pt) |
BR (1) | BRPI0408730B1 (pt) |
DE (1) | DE602004023825D1 (pt) |
ES (1) | ES2335768T3 (pt) |
MX (1) | MXPA05009935A (pt) |
WO (1) | WO2004083196A1 (pt) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060006054A1 (en) * | 2004-07-07 | 2006-01-12 | Basf Aktiengesellshaft | Separation of propylene oxide from a mixture comprising propylene oxide and methanol |
CN101084176B (zh) * | 2004-12-20 | 2012-12-05 | 赢创德固赛有限公司 | 回收甲醇的方法 |
SG157421A1 (en) * | 2005-01-14 | 2009-12-29 | Dow Global Technologies Inc | Reclamation of a titanosilicate, and reconstitution of an active oxidation catalyst |
WO2006075777A1 (ja) * | 2005-01-14 | 2006-07-20 | Sumitomo Chemical Company, Limited | プロピレンオキサイドの製造方法 |
JP4963022B2 (ja) * | 2005-11-25 | 2012-06-27 | 株式会社日本触媒 | エポキシ化合物の製造方法 |
KR100846435B1 (ko) * | 2006-12-22 | 2008-07-16 | 한화석유화학 주식회사 | 옥시란 화합물의 제조 방법 |
US7718040B2 (en) * | 2007-03-23 | 2010-05-18 | Lyondell Chemical Technology, L.P. | Propylene oxide recovery process |
MX2013000535A (es) | 2010-07-14 | 2013-02-11 | Dow Global Technologies Llc | Proceso y ensamble para producir oxidos de alquileno y eteres de glicol. |
CN102442980B (zh) * | 2010-10-11 | 2014-08-13 | 中国石油化工股份有限公司 | 环氧丙烷粗产品的精制方法和环氧丙烷的制备方法 |
US8785670B2 (en) * | 2010-12-07 | 2014-07-22 | Basf Se | Process for the production of propylene oxide |
CN103172486B (zh) * | 2011-12-22 | 2015-07-29 | 中国石油化工股份有限公司 | 一种从直接环氧化反应产物中回收丙烯的方法 |
CN103788025B (zh) * | 2012-10-29 | 2015-10-28 | 中国石油化工股份有限公司 | 一种精制环氧丙烷的方法 |
CN102993128B (zh) * | 2012-11-26 | 2015-01-28 | 中国化学赛鼎宁波工程有限公司 | 从环氧丙烷-二氧化碳共聚物洗涤液中回收环氧丙烷的设备及其方法 |
SG11201508817PA (en) * | 2013-04-29 | 2015-11-27 | Basf Se | Part-stream distillation |
US9593090B2 (en) * | 2013-07-29 | 2017-03-14 | Lyondell Chemical Technology, L.P. | Alkylene oxide separation systems, methods, and apparatuses |
WO2016066629A1 (en) * | 2014-10-27 | 2016-05-06 | Basf Se | Part-stream distillation |
ES2772695T3 (es) * | 2015-12-02 | 2020-07-08 | Evonik Operations Gmbh | Procedimiento para la epoxidación de propeno |
CN105712953A (zh) * | 2016-01-26 | 2016-06-29 | 江苏怡达化学股份有限公司 | 一种预纯化环氧丙烷的方法 |
CN106220589B (zh) * | 2016-07-27 | 2018-11-27 | 常州大学 | 一种环氧丙烷、甲醇、水体系的分离方法及分离装置 |
CN113968831B (zh) * | 2020-07-24 | 2024-02-09 | 中国石油化工股份有限公司 | 环氧丙烷精制方法和环氧丙烷物流的分离方法和环氧化反应产物分离方法及丙烯环氧化方法 |
US11691955B2 (en) | 2021-08-30 | 2023-07-04 | Saudi Arabian Oil Company | Process for recovering propylene oxide and carbon dioxide in PPC polyol production |
Family Cites Families (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3337425A (en) * | 1964-02-12 | 1967-08-22 | Monsanto Co | Extraction distillation of olefin oxides with a hydrocarbon solvent |
US3843488A (en) * | 1966-10-12 | 1974-10-22 | Halcon International Inc | Separation of propylene oxide from other hydrocarbons |
US3464897A (en) * | 1967-06-02 | 1969-09-02 | Atlantic Richfield Co | Separation of propylene oxide from other hydrocarbons |
US3578568A (en) * | 1968-11-29 | 1971-05-11 | Atlantic Richfield Co | Purification of low molecular weight epoxides by extractive distillation with a glycol or glycol ether |
US4140588A (en) * | 1977-08-05 | 1979-02-20 | Halcon Research And Development Corporation | Purification of propylene oxide by extractive distillation |
US5000825A (en) * | 1989-03-23 | 1991-03-19 | Arco Chemical Technology, Inc. | Monoepoxide purification |
DE3934971C1 (pt) * | 1989-10-20 | 1991-01-24 | Schott Glaswerke, 6500 Mainz, De | |
US4971661A (en) * | 1989-10-20 | 1990-11-20 | Texaco Chemical Company | Purification of propylene oxide using an aqueous acetone extractive distillatin agent |
FR2655115B1 (fr) * | 1989-11-30 | 1993-01-22 | Valeo | Amortisseur de vibrations, notamment pour vehicule automobile. |
US5006206A (en) * | 1990-03-12 | 1991-04-09 | Arco Chemical Technology, Inc. | Propylene oxide purification |
JP3038351B2 (ja) * | 1990-03-12 | 2000-05-08 | アルコ ケミカル テクノロジー インコーポレーテッド | 低級アルキレンオキシドの精製法 |
US5133839A (en) * | 1991-07-25 | 1992-07-28 | Arco Chemical Technology, L.P. | Lower alkylene oxide purification |
US5139622A (en) * | 1991-10-03 | 1992-08-18 | Texaco Chemical Company | Purification of propylene oxide by extractive distillation |
US5116465A (en) * | 1991-11-01 | 1992-05-26 | Texaco Chemical Company | Removal of water, methanol and acetone from propylene oxide by extractive distillation |
US5160587A (en) * | 1991-11-01 | 1992-11-03 | Texaco Chemical Company | Extractive distillation of propylene oxide |
US5116466A (en) * | 1991-11-01 | 1992-05-26 | Texaco Chemical Company | Propylene oxide purification by extractive distillation |
US5116467A (en) * | 1991-11-01 | 1992-05-26 | Texaco Chemical Company | Water and acetone removal from propylene oxide by extractive distillation |
US5145563A (en) * | 1991-11-01 | 1992-09-08 | Texaco Chemical Company | Dehydration of propylene oxide by extracting distillation |
US5145561A (en) * | 1991-11-01 | 1992-09-08 | Texaco Chemical Company | Removal of water and methanol from propylene oxide by extractive distillation |
US5340446A (en) * | 1992-10-23 | 1994-08-23 | Texaco Chemical Company | Purification of propylene oxide by cosolvent extractive distillation |
US5464505A (en) * | 1994-05-31 | 1995-11-07 | Texaco Chemical Inc. | Use of propylene oxide adducts in the purification of propylene oxide by extractive distillation |
US5453160A (en) * | 1994-05-31 | 1995-09-26 | Texaco Chemical Inc. | Use of mixed polyoxypropylene glycols in the extractive distillation of propylene oxide |
CA2159281A1 (en) * | 1995-01-25 | 1996-07-26 | Huntsman Specialty Chemicals Corporation | Controlled continuous purification of propylene oxide bt extractive distillation |
US5620568A (en) * | 1996-06-03 | 1997-04-15 | Texaco Chemical, Inc. | Extractive distillation of propylene oxide using propanol |
IT1290847B1 (it) | 1996-12-12 | 1998-12-14 | Enichem Spa | Procedimento in continuo per la preparazione di ossidi olefinici |
US6024840A (en) * | 1997-08-08 | 2000-02-15 | Arco Chemical Technology, L.P. | Propylene oxide purification |
US5863391A (en) | 1997-08-15 | 1999-01-26 | Arco Chemical Technology, L.P. | Purification of a methanol stream |
US5849938A (en) | 1997-09-02 | 1998-12-15 | Arco Chemical Technology, L.P. | Separation of methanol and propylene oxide from a reaction mixture |
EP1122248A1 (de) * | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
FR2810981B1 (fr) | 2000-06-28 | 2002-12-20 | Solvay | Procede continu de fabrication d'oxiranne comprenant des etapes de purification |
IT1318680B1 (it) | 2000-08-11 | 2003-08-27 | Enichem Spa | Processo per la produzione in continuo di ossidi olefinici. |
US6596883B2 (en) * | 2001-08-23 | 2003-07-22 | Degussa Ag | Process for the epoxidation of olefins |
JP2003238548A (ja) * | 2002-02-15 | 2003-08-27 | Sumitomo Chem Co Ltd | プロピレンオキサイドの精製方法 |
US7323579B2 (en) * | 2004-07-07 | 2008-01-29 | Basf Aktiengesellschaft | Separation of propylene oxide from a mixture comprising propylene oxide and methanol |
-
2004
- 2004-03-04 AT AT04717406T patent/ATE446958T1/de not_active IP Right Cessation
- 2004-03-04 CN CN201410033716.1A patent/CN103819427A/zh active Pending
- 2004-03-04 EP EP04717406A patent/EP1606273B1/en not_active Expired - Lifetime
- 2004-03-04 CN CNA2004800039345A patent/CN1747945A/zh active Pending
- 2004-03-04 WO PCT/US2004/006529 patent/WO2004083196A1/en active Application Filing
- 2004-03-04 ES ES04717406T patent/ES2335768T3/es not_active Expired - Lifetime
- 2004-03-04 JP JP2006509058A patent/JP4673297B2/ja not_active Expired - Lifetime
- 2004-03-04 BR BRPI0408730A patent/BRPI0408730B1/pt active IP Right Grant
- 2004-03-04 EP EP09152592A patent/EP2168953A1/en not_active Withdrawn
- 2004-03-04 US US10/541,171 patent/US7594979B2/en active Active
- 2004-03-04 MX MXPA05009935A patent/MXPA05009935A/es active IP Right Grant
- 2004-03-04 DE DE602004023825T patent/DE602004023825D1/de not_active Expired - Lifetime
-
2005
- 2005-09-16 KR KR1020057017367A patent/KR101071025B1/ko active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
DE602004023825D1 (de) | 2009-12-10 |
BRPI0408730B1 (pt) | 2016-03-22 |
ES2335768T3 (es) | 2010-04-05 |
JP4673297B2 (ja) | 2011-04-20 |
MXPA05009935A (es) | 2005-11-04 |
KR101071025B1 (ko) | 2011-10-06 |
JP2006520821A (ja) | 2006-09-14 |
ATE446958T1 (de) | 2009-11-15 |
WO2004083196A1 (en) | 2004-09-30 |
US7594979B2 (en) | 2009-09-29 |
KR20050114240A (ko) | 2005-12-05 |
CN103819427A (zh) | 2014-05-28 |
US20060113180A1 (en) | 2006-06-01 |
EP1606273A1 (en) | 2005-12-21 |
EP1606273B1 (en) | 2009-10-28 |
EP2168953A1 (en) | 2010-03-31 |
CN1747945A (zh) | 2006-03-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B15K | Others concerning applications: alteration of classification |
Free format text: PARA: INT. CL. C07D 301/32; B01J 8/00 Ipc: C07D 301/32 (2011.01), B01J 8/00 (2011.01) |
|
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 22/03/2016, OBSERVADAS AS CONDICOES LEGAIS. |