WO2018205738A1 - 高硬挺度的纯棉漂白机织粘合衬及其生产方法 - Google Patents

高硬挺度的纯棉漂白机织粘合衬及其生产方法 Download PDF

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WO2018205738A1
WO2018205738A1 PCT/CN2018/078778 CN2018078778W WO2018205738A1 WO 2018205738 A1 WO2018205738 A1 WO 2018205738A1 CN 2018078778 W CN2018078778 W CN 2018078778W WO 2018205738 A1 WO2018205738 A1 WO 2018205738A1
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bleaching
stiffness
powder
shrinking
production method
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PCT/CN2018/078778
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English (en)
French (fr)
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曹平
王春梅
杨静新
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南通海汇科技发展有限公司
南通大学
上海市纺织工业技术监督所
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Publication of WO2018205738A1 publication Critical patent/WO2018205738A1/zh

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
    • D06M15/423—Amino-aldehyde resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/007—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by mechanical or physical treatments
    • D06N3/0077—Embossing; Pressing of the surface; Tumbling and crumbling; Cracking; Cooling; Heating, e.g. mirror finish
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/125—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyamides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N7/00—Flexible sheet materials not otherwise provided for, e.g. textile threads, filaments, yarns or tow, glued on macromolecular material
    • D06N7/0092—Non-continuous polymer coating on the fibrous substrate, e.g. plastic dots on fabrics
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/45—Shrinking resistance, anti-felting properties

Definitions

  • the invention relates to a high-stiffness pure cotton bleaching woven adhesive lining and a production method thereof.
  • the high-hardness lining cloth used in the production of outerwear, jackets, trousers and the like has the problems of low bending strength, high free and hydrolyzed formaldehyde, low tearing strength, etc., which affects both the quality of the garment and the performance of the garment. And use the effect.
  • the high-quality outerwear is made of high-quality eco-friendly high-rigidity cotton lining, which can enhance the garment's stiffness, elasticity and three-dimensionality, and enhance the comfort and safety of the garment.
  • the object of the present invention is to provide a bending strength ⁇ 8cm, free and hydrolyzed formaldehyde ⁇ 200mg/kg, a dimensional change rate of warp and weft washing of -1.0% to +0.5%, and a high stiffness of latitude tearing strength ⁇ 3N. Pure cotton bleached woven adhesive lining and production method thereof.
  • a high-hardness pure cotton bleaching woven adhesive lining characterized in that: the flexural strength of the adhesive lining is cm8cm, the free and hydrolyzed formaldehyde ⁇ 200mg/kg, and the dimensional change rate of the warp and weft washing is -1.0% ⁇ + 0.5%, turbulent tearing force ⁇ 3N.
  • the invention discloses a production method of high-hardness pure cotton bleaching woven adhesive lining, which comprises the following steps: grooving, singeing, scouring, oxygen bleaching or reoxygenation bleaching, tentering, stiffening and shrink-proof finishing, powder Point coating and other steps;
  • composition of the stiffening anti-shrinking finishing liquid is:
  • the cloth is fed through the flat web, the second dip and the rolling hard anti-shrinking finishing liquid, 130 ⁇ 150 °C loose drying, super feeding 2.0% ⁇ 3.0% upper needle board, eight grid hot air baking, the first The grid temperature is 155 ° C, the second grid temperature is 160 ° C, the third to fourth grid temperature is 165 ° C, and the fifth to eighth grid temperature is 170 ° C.
  • the two cylinders are cooled and dropped.
  • Powder coating treatment includes flat feeding cloth, No. 1 oil heating roller 225-245 ° C preheating, No. 2 oil heating roller 220 ⁇ 240 ° C preheating, engraving roller PA hot melt adhesive powder coating, engraving roller 45-65 °C hot water circulation, No. 3 oil hot roller 230 ⁇ 250 °C heating, infrared tenter setting, temperature ⁇ 25 ° C water cooling, package step; engraving roll mesh: 33 mesh / inch; fabric powder point
  • the coating amount is 20-25 g/m 2 to prevent reverse penetration; during the powder coating process, powder jumping, leaking points and half-grain heads cannot occur; the feeding speed is 18-22 m/min.
  • the invention has convenient process and excellent product performance, the bending strength of the adhesive lining is cm8cm, the free and hydrolyzed formaldehyde ⁇ 200mg/kg, the dimensional change rate of the warp and weft washing is -1.0% ⁇ +0.5%, and the latitudinal tearing strength ⁇ 3N, fully meets the excellent quality indicators and safety performance indicators of the production of garment outerwear.
  • the invention discloses a production method of high-hardness pure cotton bleaching woven adhesive lining, which comprises, in turn, grey fabric tumbling, singeing, scouring, oxygen bleaching or re-oxygen bleaching, tentering, stiffening shrink-proof finishing, powder coating, Quality inspection and other steps; the flexural strength of the bonded lining is cm8cm, the free and hydrolyzed formaldehyde ⁇ 200mg/kg, the dimensional change rate of the warp and weft washing is -1.0% ⁇ +0.5%, and the latitudinal tearing strength is ⁇ 3N.
  • composition of the stiffening anti-shrinking finishing liquid is:
  • the fabric is fed through the flat web, the second dip is rolled and the anti-shrinking finishing liquid is loosened, 130 ⁇ 150°C loose-drying, the super-feeding 2.5% upper needle board, and the eight-grid hot air baking, wherein the first temperature is 155 °C, the second grid temperature is 160 ° C, the third to fourth grid temperature is 165 ° C, and the fifth to eighth grid temperature is 170 ° C.
  • the two cylinders are cooled and dropped.
  • Powder coating treatment includes flat feeding cloth, No. 1 oil heating roller 225-245 ° C preheating, No. 2 oil heating roller 220 ⁇ 240 ° C preheating, engraving roller PA hot melt adhesive powder coating, engraving roller 45-65 °C hot water circulation, No. 3 oil heat roller 230 ⁇ 250 °C heating, infrared tenter setting, temperature ⁇ 25 ° C water cooling, package step; engraving roll mesh: 33 mesh / inch; fabric powder point
  • the coating amount is 229 ⁇ 1g/m 2 to prevent reverse penetration; during the powder coating process, powder jumping, leaking point and half grain head cannot occur; the feeding speed is 18-22 m/min.
  • the fabric of the cotton lining is of the order of 48.5 inches, the yarn count is 20s x 20s, and the density is 64 x 60 pieces/inch.
  • composition of the stiff anti-shrinking finishing liquid is:
  • the rest are the same as in the first embodiment.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Dispersion Chemistry (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Details Of Garments (AREA)

Abstract

本发明公开了一种高硬挺度的纯棉漂白机织粘合衬及其生产方法，生产流程包括坯布翻缝、烧毛、煮练、氧漂或复氧漂、拉幅、硬挺防缩整理、粉点涂层、质量检验等步骤；粘合衬的抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N。本发明工艺操作方便，产品性能优异，完全达到外衣服装的安全性能指标。

Description

高硬挺度的纯棉漂白机织粘合衬及其生产方法 技术领域
本发明涉及一种高硬挺度的纯棉漂白机织粘合衬及其生产方法。
 背景技术
现有的西服、茄克、裤子等外衣生产中使用的高硬挺度衬布，存在着抗弯强度低、游离和水解甲醛量高、撕破强力低等问题，既影响服装品质，也影响服装使用性能和使用效果。 高档外衣生产中使用了优良品质的生态友好的高硬挺度纯棉粘合衬，既可增强服装挺括性、弹性和立体感，又可增强服装的舒适性和安全性。
 技术问题
本发明的目的在于提供一种抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N的高硬挺度的纯棉漂白机织粘合衬及其生产方法。
 技术解决方案
一种高硬挺度的纯棉漂白机织粘合衬，其特征是：粘合衬的抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N。
一种高硬挺度的纯棉漂白机织粘合衬的生产方法,其特征是：依次包括坯布翻缝、烧毛、煮练、氧漂或复氧漂、拉幅、硬挺防缩整理、粉点涂层等步骤；
硬挺防缩整理时，硬挺防缩整理液的组成为：
醚化改性六羟树脂M—6      300～400g/L
10%PVA     300～400g/L
MgCl 2·6H 2O      15～25g/L
增白剂MST    2.0g/L
增白剂MST-B   5.0g/L
酸性红     0.00954g/L
酸性蓝     0.0213g/L
乙烯脲           4～6 g/L
PH           5.5～6.5
硬挺防缩整理时通过平幅进布，二浸一轧硬挺防缩整理液，130 ～ 150℃松式烘燥，超喂2.0% ～3.0％上针板，八格热风焙烘，其中第一格温度 155℃，第二格温度 160℃，第三～四格温度 165℃，第五～八格温度170℃，两个锡林冷却落布。
粉点涂层处理依次包括平幅进布、1号油热辊225-245℃预热、2号油热辊220～240℃预热、雕刻辊PA热熔胶粉点涂层、雕刻辊内通45-65℃的热水循环、3号油热辊230～250℃加热、红外线拉幅定形、温度≤ 25℃水冷却、卷装步骤；雕刻辊目数： 33 目/英寸；织物粉点涂层量20～25g/m 2，防止反面渗透；粉点涂层过程中，不能出现跳粉、漏点、半粒头；进布速度为 18～22m/min。
有益效果
本发明工艺操作方便，产品性能优异，粘合衬的抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N，完全达到服装外衣的生产的优等质量指标和安全性能指标。
 本发明的实施方式
实施例1：
一种高硬挺度的纯棉漂白机织粘合衬的生产方法，依次包括坯布翻缝、烧毛、煮练、氧漂或复氧漂、拉幅、硬挺防缩整理、粉点涂层、质量检验等步骤；粘合衬的抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N。
硬挺防缩整理时，硬挺防缩整理液的组成为：
醚化改性六羟树脂M—6      350g/L
10%PVA         350g/L
MgCl 2·6H 2O      18g/L
增白剂MST    2.0g/L
增白剂MST-B   5.0g/L
酸性红     0.00954g/L
酸性蓝     0.0213g/L
乙烯脲5 g/L
PH            6.0
硬挺防缩整理时通过平幅进布，二浸一轧硬挺防缩整理液，130 ～ 150℃松式烘燥，超喂2.5% 上针板，八格热风焙烘，其中第一格温度 155℃，第二格温度 160℃，第三～四格温度 165℃，第五～八格温度170℃，两个锡林冷却落布。
粉点涂层处理依次包括平幅进布、1号油热辊225-245℃预热、2号油热辊220～240℃预热、雕刻辊PA热熔胶粉点涂层、雕刻辊内通45-65℃的热水循环、3号油热辊230～250℃加热、红外线拉幅定形、温度≤ 25℃水冷却、卷装步骤；雕刻辊目数：33 目/英寸；织物粉点涂层量229±1g/m 2，防止反面渗透；粉点涂层过程中，不能出现跳粉、漏点、半粒头；进布速度为 18～22m/min。
纯棉衬布的坯布规格为：门幅为 48.5 英寸、纱支数为 20s×20s、密度为 64×60根/英寸。
实施例2：
硬挺防缩整理液的组成为：
醚化改性六羟树脂M—6      390g/L
10%PVA        390g/L
MgCl 2·6H 2O      23g/L
增白剂MST    2.0g/L
增白剂MST-B   5.0g/L
酸性红     0.00954g/L
酸性蓝     0.0213g/L
乙烯脲           4g/L
PH           5.8。
其余同实施例1。

Claims (3)

  1. 一种高硬挺度的纯棉漂白机织粘合衬,其特征是：粘合衬的抗弯强度≧8cm，游离和水解甲醛≤200mg/kg，经纬向水洗尺寸变化率为 -1.0%～+0.5%，纬向撕破强力≧3N。
  2. 一种权利要求1所述的高硬挺度的纯棉漂白机织粘合衬的生产方法,其特征是：依次包括坯布翻缝、烧毛、煮练、氧漂或复氧漂、拉幅、硬挺防缩整理、粉点涂层步骤；
    硬挺防缩整理时，硬挺防缩整理液的组成为：
    醚化改性六羟树脂M—6      300～400g/L
    10%PVA             300～400g/L
    MgCl 2·6H 2O      15～25g/L
    增白剂MST    2.0g/L
    增白剂MST-B   5.0g/L
    酸性红     0.00954g/L
    酸性蓝     0.0213g/L
    乙烯脲           4～6 g/L
    PH           5.5～6.5
    硬挺防缩整理时通过平幅进布，二浸一轧硬挺防缩整理液，130 ～ 150℃松式烘燥，超喂2.0%～3.0％上针板，八格热风焙烘，其中第一格温度 155℃，第二格温度 160℃，第三～四格温度 165℃，第五～八格温度170℃，两个锡林冷却落布。
  3. 根据权利要求2所述的高硬挺度的纯棉漂白机织粘合衬的生产方法,其特征是：粉点涂层处理依次包括平幅进布、1号油热辊225-245℃预热、2号油热辊220～240℃预热、雕刻辊PA热熔胶粉点涂层、雕刻辊内通45-65℃的热水循环、3号油热辊230～250℃加热、红外线拉幅定形、温度≤ 25℃水冷却、卷装步骤；雕刻辊目数： 33目/英寸；织物粉点涂层量20～25g/m 2，防止反面渗透；粉点涂层过程中，不能出现跳粉、漏点、半粒头；进布速度为 18～22m/min。
PCT/CN2018/078778 2017-05-08 2018-03-13 高硬挺度的纯棉漂白机织粘合衬及其生产方法 WO2018205738A1 (zh)

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CN116289005A (zh) * 2023-02-11 2023-06-23 福建省联丰盛漂染植绒有限公司 一种纯棉四面弹织物加工方法

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