WO2018178929A3 - Procédé de purification de nanotubes de carbone bruts - Google Patents

Procédé de purification de nanotubes de carbone bruts Download PDF

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Publication number
WO2018178929A3
WO2018178929A3 PCT/IB2018/052192 IB2018052192W WO2018178929A3 WO 2018178929 A3 WO2018178929 A3 WO 2018178929A3 IB 2018052192 W IB2018052192 W IB 2018052192W WO 2018178929 A3 WO2018178929 A3 WO 2018178929A3
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WO
WIPO (PCT)
Prior art keywords
carbon nanotubes
order
raw carbon
purification
raw
Prior art date
Application number
PCT/IB2018/052192
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English (en)
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WO2018178929A2 (fr
Inventor
Ali DARWICHE
Martin Dontigny
Naoyuki Kondo
Abdelbast Guerfi
Karim Zaghib
Julien Beausoleil
Alexander Korzhenko
Original Assignee
HYDRO-QUéBEC
Arkema France
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Filing date
Publication date
Application filed by HYDRO-QUéBEC, Arkema France filed Critical HYDRO-QUéBEC
Priority to JP2019553296A priority Critical patent/JP7171608B2/ja
Priority to CN201880034976.7A priority patent/CN110662715B/zh
Priority to EP18721140.4A priority patent/EP3601161A2/fr
Priority to KR1020197031989A priority patent/KR102666434B1/ko
Priority to CA3057746A priority patent/CA3057746A1/fr
Priority to US16/498,537 priority patent/US11661344B2/en
Publication of WO2018178929A2 publication Critical patent/WO2018178929A2/fr
Publication of WO2018178929A3 publication Critical patent/WO2018178929A3/fr
Priority to JP2022176379A priority patent/JP7429760B2/ja
Priority to US18/298,075 priority patent/US20230339758A1/en

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/168—After-treatment
    • C01B32/17—Purification
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • H01M4/587—Carbonaceous material, e.g. graphite-intercalation compounds or CFx for inserting or intercalating light metals
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/06—Multi-walled nanotubes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/22—Electronic properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/26—Mechanical properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/30—Purity
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/32—Specific surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Electric Double-Layer Capacitors Or The Like (AREA)

Abstract

La présente invention propose un procédé destiné à purifier des nanotubes de carbone bruts pour atteindre un taux d'impuretés métalliques compris entre 5 ppm et 200 ppm. Le procédé comprend une augmentation de la masse volumique apparente des nanotubes de carbone bruts par compactage pour produire des nanotubes de carbone compactés. Le procédé comprend également un frittage des nanotubes de carbone compactés par soumission à un traitement thermique sous une atmosphère gazeuse afin d'enlever au moins une partie des impuretés métalliques contenues dans les nanotubes de carbone bruts, en produisant de ce fait des nanotubes de carbone purifiés. Ces nanotubes de carbone purifiés sont directement utilisables comme des conducteurs électroniques servant comme additifs de base à un matériau d'électrode sans avoir besoin une quelconque étape ultérieure de purification. Le matériau d'électrode peut alors servir à fabriquer une électrode destinée à une batterie lithium-ion.
PCT/IB2018/052192 2017-03-31 2018-03-29 Procédé de purification de nanotubes de carbone bruts WO2018178929A2 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
JP2019553296A JP7171608B2 (ja) 2017-03-31 2018-03-29 粗カーボンナノチューブの精製のための方法
CN201880034976.7A CN110662715B (zh) 2017-03-31 2018-03-29 粗制碳纳米管的提纯方法
EP18721140.4A EP3601161A2 (fr) 2017-03-31 2018-03-29 Procédé de purification de nanotubes de carbone bruts
KR1020197031989A KR102666434B1 (ko) 2017-03-31 2018-03-29 미가공 탄소 나노튜브의 정제 방법
CA3057746A CA3057746A1 (fr) 2017-03-31 2018-03-29 Procede de purification de nanotubes de carbone bruts
US16/498,537 US11661344B2 (en) 2017-03-31 2018-03-29 Method for the purification of raw carbon nanotubes
JP2022176379A JP7429760B2 (ja) 2017-03-31 2022-11-02 粗カーボンナノチューブの精製のための方法
US18/298,075 US20230339758A1 (en) 2017-03-31 2023-04-10 Method for the purification of raw carbon nanotubes

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201762479688P 2017-03-31 2017-03-31
US62/479,688 2017-03-31
FR17/52749 2017-03-31
FR1752749A FR3064623A1 (fr) 2017-03-31 2017-03-31 Processus de purification de nanotubes de carbone bruts

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US16/498,537 A-371-Of-International US11661344B2 (en) 2017-03-31 2018-03-29 Method for the purification of raw carbon nanotubes
US18/298,075 Continuation US20230339758A1 (en) 2017-03-31 2023-04-10 Method for the purification of raw carbon nanotubes

Publications (2)

Publication Number Publication Date
WO2018178929A2 WO2018178929A2 (fr) 2018-10-04
WO2018178929A3 true WO2018178929A3 (fr) 2018-12-20

Family

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Application Number Title Priority Date Filing Date
PCT/IB2018/052192 WO2018178929A2 (fr) 2017-03-31 2018-03-29 Procédé de purification de nanotubes de carbone bruts

Country Status (7)

Country Link
US (2) US11661344B2 (fr)
EP (1) EP3601161A2 (fr)
JP (2) JP7171608B2 (fr)
CN (1) CN110662715B (fr)
CA (1) CA3057746A1 (fr)
FR (1) FR3064623A1 (fr)
WO (1) WO2018178929A2 (fr)

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FR3078201B1 (fr) 2018-02-19 2023-01-13 Arkema France Formulation de matiere active pour accumulateur li-s et procede de preparation
FR3091041A1 (fr) 2018-12-20 2020-06-26 Arkema France Composition conductrice electronique pour batterie au lithium tout solide
CN109502572A (zh) * 2018-12-29 2019-03-22 苏州第元素纳米技术有限公司 碳纳米管提纯方法
FR3094710A1 (fr) 2019-04-05 2020-10-09 Arkema France Procédé de préparation d’une composition pâteuse comprenant des nanotubes de carbone
CN111249765B (zh) * 2020-02-25 2021-04-06 中国科学院化学研究所 一种去除碳材料中金属离子的加压流体提取系统和方法
CN113443617B (zh) * 2021-08-19 2022-11-04 陕西六元碳晶股份有限公司 一种连续式碳纳米管的纯化装置及工艺
CN114014300A (zh) * 2021-11-24 2022-02-08 深圳市飞墨科技有限公司 碳纳米管及其纯化方法
CN115215327B (zh) * 2022-02-23 2023-10-03 无锡东恒新能源科技有限公司 一种用于碳纳米管提纯的装置及方法
CN114590796A (zh) * 2022-02-28 2022-06-07 诺瑞(深圳)新技术有限公司 碳纳米管的纯化方法和碳纳米管浆料的制备方法
CN116022775B (zh) * 2022-12-29 2024-02-09 蜂巢能源科技(上饶)有限公司 一种碳纳米管提纯方法及应用
CN116462188A (zh) * 2023-05-11 2023-07-21 清华大学 提高碳纳米管纯度的方法及碳纳米管和用途

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Publication number Publication date
US11661344B2 (en) 2023-05-30
JP7429760B2 (ja) 2024-02-08
US20230339758A1 (en) 2023-10-26
WO2018178929A2 (fr) 2018-10-04
JP7171608B2 (ja) 2022-11-15
US20210107791A1 (en) 2021-04-15
CN110662715A (zh) 2020-01-07
KR20190135032A (ko) 2019-12-05
CN110662715B (zh) 2023-10-27
JP2023009119A (ja) 2023-01-19
JP2020515497A (ja) 2020-05-28
EP3601161A2 (fr) 2020-02-05
CA3057746A1 (fr) 2018-10-04
FR3064623A1 (fr) 2018-10-05

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