WO2017092187A1 - 一种接骨木食醋的制备方法 - Google Patents

一种接骨木食醋的制备方法 Download PDF

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WO2017092187A1
WO2017092187A1 PCT/CN2016/075462 CN2016075462W WO2017092187A1 WO 2017092187 A1 WO2017092187 A1 WO 2017092187A1 CN 2016075462 W CN2016075462 W CN 2016075462W WO 2017092187 A1 WO2017092187 A1 WO 2017092187A1
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vinegar
elderberry
elderflower
preparing
water
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孙茜妍
余永建
朱胜虎
梁潇滢
李童
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江苏恒顺醋业股份有限公司
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/35Caprifoliaceae (Honeysuckle family)

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  • the invention belongs to the field of food processing, and in particular relates to a preparation method of elderberry vinegar.
  • the existing vinegar is mostly based on condiments, and it does not exert its efficacy of enhancing resistance and health care.
  • the existing vinegar beverage products are mostly blended fruit vinegar drinks.
  • the high sugar content is not conducive to health, and the flavor is single, and the market prospect is not broad.
  • the object of the present invention is to provide an elderberry vinegar which has unique flavor, low sugar, enhanced resistance, health care function, and is in line with the current healthy diet and disease prevention, and a preparation method thereof.
  • a preparation method of elderberry vinegar characterized in that the method comprises the following steps:
  • the step (1) of the elderberry flower extraction method is: selecting fresh elderflower, adding water and boiling for 20 minutes to extract twice, the first water addition amount is 20 times the weight of the elderflower, and the second time is elderberry 10 times the weight of the flower, after filtration, the combined filtrate was added to a concentrator, and concentrated to 1.5-2.0 g of the original decoction piece per 1 mL of the concentrated liquid to obtain an Elderflower concentrate.
  • step (1) is concentrated to concentration under reduced pressure, and the pressure is -0.07 to -0.09 MPa, and the temperature is 35 to 45 °C.
  • the acidity of the brewed vinegar in the step (3) is ⁇ 4.9%.
  • the fructose syrup soluble solid matter is ⁇ 71%.
  • the ratio of each component in the step (3) is: adding 60 to 100 g of the concentrated liquid obtained in the step (1) per liter of the mixture, 80 to 150 g of the raspberry juice obtained in the step (2), and 10 to 35 g of the fruit grape. Syrup, 2 ⁇ 15g Honey, 3 ⁇ 8g citric acid, 400 ⁇ 500g brewed vinegar, add water to 1 liter.
  • the sterilization is performed by ultra-high temperature instantaneous sterilization: the temperature is 120 to 130 ° C, and the sterilization is 3 to 5 s.
  • This product is low in sugar and suitable for a wide range of people.
  • a method for preparing elderberry vinegar comprises the following steps:
  • a method for preparing elderberry vinegar comprises the following steps:
  • a method for preparing elderberry vinegar comprises the following steps:
  • Case selection 50 patients with simple influenza were selected, including 25 males and 25 females.
  • diagnostic criteria refer to "influenza diagnostic criteria and treatment principles.”
  • test group used any one of the above-mentioned Examples 1 to 3, elderberry vinegar, twice a day, 10 ml each time; the control group took Ban GmbH granules twice a day, each time 10 g; 7 days For a course of treatment, after a course of treatment, the effect is counted.
  • Clinical recovery The clinical symptoms and signs of TCM disappear or disappear, and the symptom score is reduced by ⁇ 95%.
  • Example 1 Example 2
  • Example 3 Proanthocyanidin content 0.640mg/mL 1.225mg/mL 0.884mg/mL

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Abstract

一种接骨木食醋的制备方法,包括:(1)接骨木花水提、过滤、浓缩得浓缩液;(2)接骨木莓压榨得莓汁;(3)浓缩液与莓汁、果葡糖浆、蜂蜜、柠檬酸、酿造食醋及水混合;(4)混合物冷藏、过滤;(5)滤液灌装、灭菌即得。

Description

一种接骨木食醋的制备方法 技术领域
本发明属于食品加工领域,尤其涉及一种接骨木食醋的制备方法。
背景技术
现有食醋多以调味品为主,并未发挥其增强抵抗力,养生保健的功效。而现有的醋饮料产品多为调配型果醋饮料,糖分过高不利于健康,且风味单一,市场前景不广阔。
发明内容
为了克服现有技术的不足,本发明的目的在于提供一种风味独特,低糖,增强抵抗力,具有保健作用,符合现今健康饮食,预防疾病的接骨木食醋及其制备方法。
为达到上述目的,本发明是通过以下的技术方案来实现的。
一种接骨木食醋的制备方法,其特征在于,包括以下步骤:
(1)选择新鲜的接骨木花,加水煮沸提取2-3次,每次20-30min,过滤后合并滤液,浓缩得浓缩液;
(2)选择新鲜成熟的接骨木莓,压榨取汁均质得莓汁;
(3)将步骤(1)所得浓缩液与步骤(2)所得莓汁和果葡糖浆、蜂蜜、柠檬酸、酿造食醋与水混合均匀;
(4)将步骤(3)所得混合物于4℃冷藏24~48h,然后过滤;
(5)将步骤(4)所得滤液灌装,灭菌既得。
进一步地所述步骤(1)接骨木花的提取方法为:选择新鲜的接骨木花,加水煮沸20min提取两次,第一次加水量为接骨木花重量的20倍,第二次为接骨木花重量的10倍,过滤后合并滤液加入到浓缩器中,浓缩至每1mL浓缩液相当于原饮片的1.5-2.0g,得接骨木花浓缩液。
进一步地所述步骤(1)中浓缩为减压浓缩,压力为-0.07~-0.09Mpa,温度为35~45℃。
进一步地所述步骤(3)中酿造食醋的酸度≥4.9%。
进一步地所述步骤(3)中果葡糖浆可溶性固形物≥71%。
进一步地所述步骤(3)中各组分的配比为:按每升混合物中加入60~100g步骤(1)所得浓缩液,80~150g步骤(2)所得莓汁,10~35g果葡糖浆,2~15g 蜂蜜,3~8g柠檬酸,400~500g酿造食醋,加水至1升。
进一步地所述步骤(5)中灭菌采用超高温瞬时灭菌灌装:温度120~130℃,灭菌3~5s。
有益效果:与现有技术相比,本发明的优点在于:
1)利用新鲜的接骨木花和莓为原料,风味特殊;
2)具有增强抵抗力,缓解流感症状的功效,符合现今健康饮食的要求;
3)本品低糖,适用人群广泛。
具体实施方式
下面结合实例对本发明作进一步的详细说明。
实施例1
一种接骨木食醋的制备方法,包括以下步骤:
(1)选择新鲜的接骨木花,加水煮沸20min提取两次,第一次加水量为接骨木花重量的20倍,第二次为接骨木花重量的10倍,过滤后合并滤液加入到浓缩器中,减压浓缩,压力-0.08Mpa,温度40℃,浓缩至每1mL浓缩液相当于原饮片的1.5g,得接骨木花浓缩液;
(2)选择新鲜成熟的接骨木莓,压榨取汁均质得莓汁;
(3)按配制1升混合物将60g步骤(1)所得浓缩液,80g步骤(2)所得莓汁,10g果葡糖浆,2g蜂蜜,3g柠檬酸,400g酿造食醋混合,加水至1升,混合均匀,其中酿造食醋酸度≥4.9%,果葡糖浆可溶性固形物≥71%;
(4)将步骤(3)所得混合物于4℃冷藏24~48h,然后过滤;
(5)将步骤(4)所得滤液灌装,采用超高温瞬时灭菌灌装:温度120~130℃,灭菌3~5s。
实施例2
一种接骨木食醋的制备方法,包括以下步骤:
(1)选择新鲜的接骨木花,加水煮沸20min提取两次,第一次加水量为接骨木花重量的20倍,第二次为接骨木花重量的10倍,过滤后合并滤液加入到浓缩器中,减压浓缩,压力-0.07Mpa,温度45℃,浓缩至每1mL浓缩液相当于原饮片的2.0g,得接骨木花浓缩液;
(2)选择新鲜成熟的接骨木莓,压榨取汁均质得莓汁;
(3)按配制1升混合物将100g步骤(1)所得浓缩液,150g步骤(2)所得莓 汁,35g果葡糖浆,15g蜂蜜,8g柠檬酸,450g酿造食醋混合,加水至1升,混合均匀,其中酿造食醋酸度≥4.9%,果葡糖浆可溶性固形物≥71%;
(4)将步骤(3)所得混合物于4℃冷藏24~48h,然后过滤;
(5)将步骤(4)所得滤液灌装,采用超高温瞬时灭菌灌装:温度120~130℃,灭菌3~5s。
实施例3
一种接骨木食醋的制备方法,包括以下步骤:
(1)选择新鲜的接骨木花,加水煮沸20min提取两次,第一次加水量为接骨木花重量的20倍,第二次为接骨木花重量的10倍,过滤后合并滤液加入到浓缩器中,减压浓缩,压力-0.09Mpa,温度35℃,浓缩至每1mL浓缩液相当于原饮片的2.0g,得接骨木花浓缩液;
(2)选择新鲜成熟的接骨木莓,压榨取汁均质得莓汁;
(3)按配制1升混合物将70g步骤(1)所得浓缩液,100g步骤(2)所得莓汁,15g果葡糖浆,7g蜂蜜,4g柠檬酸,500g酿造食醋混合,加水至1升,混合均匀,其中酿造食醋酸度≥4.9%,果葡糖浆可溶性固形物≥71%;
(4)将步骤(3)所得混合物于4℃冷藏24~48h,然后过滤;
(5)将步骤(4)所得滤液灌装,采用超高温瞬时灭菌灌装:温度120~130℃,灭菌3~5s。
下面通过服用临床病例对本发明的的有益效果作进一步的详细说明:
1、病例选择:选择50例单纯型流行性感冒患者,男25例,女25例。
2、诊断标准:参照《流行性感冒诊断标准及处理原则》。
3、治疗方法:试验组采用上述实施例1至实施例3中任一种接骨木食醋,每日二次,每次10ml;对照组服用板蓝根冲剂,每天两次,每次10g;7天为一疗程,一个疗程后,统计疗效。
4、疗效评定标准:
疗效评定(参照《中药新药临床研究指导原则》)
临床痊愈:中医临床症状、体征消失或基本消失,症状积分减少≥95%。
显效:中医临床症状、体征明显改善,症状积分减少≥70%。
有效:中医临床症状、体征均有好转,症状积分减少≥30%。
无效:中医临床症状、体征均无明显改善,甚或加重,症状积分减少不足30%。
试验组与对照组疗效比较,见表1。
表1试验组与对照组疗效比较
Figure PCTCN2016075462-appb-000001
试验组(接骨木食醋)25例,总有效率达92%,与对照组(板蓝根冲剂)25例总有效率80%,进行比较,试验组优于对照组。说明本发明增强抵抗力,缓解流感效显著,具有良好的推广价值。
对于以上实施例,对接骨木食醋中的前花青素成分进行了测定,测定方法依据国家标准GB22244-2008,检测结果如表2所示:
表2
检测项目 实施例1 实施例2 实施例3
前花青素含量 0.640mg/mL 1.225mg/mL 0.884mg/mL
本发明按照上述实施例进行了说明,应当理解,上述实施例不以任何形式限定本发明,凡采用等同替换或等效变换方式所获得的技术方案,均落在本发明的保护范围之内。

Claims (7)

  1. 一种接骨木食醋的制备方法,其特征在于,包括以下步骤:
    (1)选择新鲜的接骨木花,加水煮沸提取2-3次,每次20-30min,过滤后合并滤液,浓缩得浓缩液;
    (2)选择新鲜成熟的接骨木莓,压榨取汁均质得莓汁;
    (3)将步骤(1)所得浓缩液与步骤(2)所得莓汁和果葡糖浆、蜂蜜、柠檬酸、酿造食醋与水混合均匀;
    (4)将步骤(3)所得混合物于4℃冷藏24~48h,然后过滤;
    (5)将步骤(4)所得滤液灌装,灭菌既得。
  2. 根据权利要求1所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(1)接骨木花的提取方法为:选择新鲜的接骨木花,加水煮沸20min提取两次,第一次加水量为接骨木花重量的20倍,第二次为接骨木花重量的10倍,过滤后合并滤液加入到浓缩器中,浓缩至每1mL浓缩液相当于原饮片的1.5-2.0g,得接骨木花浓缩液。
  3. 根据权利要求1或2所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(1)中浓缩为减压浓缩,压力为-0.07~-0.09Mpa,温度为35~45℃。
  4. 根据权利要求1所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(3)中酿造食醋的酸度≥4.9%。
  5. 根据权利要求1所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(3)中果葡糖浆可溶性固形物≥71%。
  6. 根据权利要求1所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(3)中各组分的配比为:按每升混合物中加入60~100g步骤(1)所得浓缩液,80~150g步骤(2)所得莓汁,10~35g果葡糖浆,2~15g蜂蜜,3~8g柠檬酸,400~500g酿造食醋,加水至1升。
  7. 根据权利要求1所述的一种接骨木食醋的制备方法,其特征在于,所述步骤(5)中灭菌采用超高温瞬时灭菌灌装:温度120~130℃,灭菌3~5s。
PCT/CN2016/075462 2015-12-01 2016-03-03 一种接骨木食醋的制备方法 WO2017092187A1 (zh)

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