WO2017036036A1 - 一种高压脉冲协同超微粉碎生产全谷物粉的方法 - Google Patents
一种高压脉冲协同超微粉碎生产全谷物粉的方法 Download PDFInfo
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- WO2017036036A1 WO2017036036A1 PCT/CN2015/099640 CN2015099640W WO2017036036A1 WO 2017036036 A1 WO2017036036 A1 WO 2017036036A1 CN 2015099640 W CN2015099640 W CN 2015099640W WO 2017036036 A1 WO2017036036 A1 WO 2017036036A1
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- Prior art keywords
- flour
- suspension
- bran
- whole grain
- electric field
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- 235000013312 flour Nutrition 0.000 title claims abstract description 52
- 238000010298 pulverizing process Methods 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 239000000725 suspension Substances 0.000 claims abstract description 32
- 238000000034 method Methods 0.000 claims abstract description 18
- 150000004676 glycans Chemical class 0.000 claims abstract description 10
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 10
- 239000005017 polysaccharide Substances 0.000 claims abstract description 10
- 239000000084 colloidal system Substances 0.000 claims abstract description 9
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- 238000007873 sieving Methods 0.000 claims abstract description 5
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- 235000020985 whole grains Nutrition 0.000 claims description 35
- 230000005684 electric field Effects 0.000 claims description 24
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- 238000012545 processing Methods 0.000 claims description 16
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- 244000215068 Acacia senegal Species 0.000 claims description 3
- 229920000084 Gum arabic Polymers 0.000 claims description 3
- 229920002752 Konjac Polymers 0.000 claims description 3
- 239000000205 acacia gum Substances 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 239000000679 carrageenan Substances 0.000 claims description 3
- 235000010418 carrageenan Nutrition 0.000 claims description 3
- 229920001525 carrageenan Polymers 0.000 claims description 3
- 229940113118 carrageenan Drugs 0.000 claims description 3
- 239000000252 konjac Substances 0.000 claims description 3
- 235000019823 konjac gum Nutrition 0.000 claims description 3
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- 235000010987 pectin Nutrition 0.000 claims description 3
- 229920001277 pectin Polymers 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 229920001285 xanthan gum Polymers 0.000 claims description 3
- 239000000230 xanthan gum Substances 0.000 claims description 3
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- 229940082509 xanthan gum Drugs 0.000 claims description 3
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 3
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- 108010068370 Glutens Proteins 0.000 abstract description 7
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- 108090000623 proteins and genes Proteins 0.000 abstract description 7
- 102000004169 proteins and genes Human genes 0.000 abstract description 7
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- 235000021251 pulses Nutrition 0.000 description 20
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- 244000098338 Triticum aestivum Species 0.000 description 11
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- 235000016709 nutrition Nutrition 0.000 description 4
- 235000008429 bread Nutrition 0.000 description 3
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- 240000005979 Hordeum vulgare Species 0.000 description 2
- 235000007340 Hordeum vulgare Nutrition 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 2
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- 239000004382 Amylase Substances 0.000 description 1
- 235000007558 Avena sp Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 240000008620 Fagopyrum esculentum Species 0.000 description 1
- 235000009419 Fagopyrum esculentum Nutrition 0.000 description 1
- 206010019280 Heart failures Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000209056 Secale Species 0.000 description 1
- 235000007238 Secale cereale Nutrition 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 206010041235 Snoring Diseases 0.000 description 1
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- 235000007264 Triticum durum Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 125000003275 alpha amino acid group Chemical group 0.000 description 1
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- 208000019622 heart disease Diseases 0.000 description 1
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- 230000000968 intestinal effect Effects 0.000 description 1
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- 235000004213 low-fat Nutrition 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
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- 230000008855 peristalsis Effects 0.000 description 1
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- 229910052700 potassium Inorganic materials 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
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- 238000003860 storage Methods 0.000 description 1
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- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
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- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000011875 whole grain product Nutrition 0.000 description 1
- 241000228158 x Triticosecale Species 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D6/00—Other treatment of flour or dough before baking, e.g. cooling, irradiating, heating
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D13/00—Finished or partly finished bakery products
- A21D13/02—Products made from whole meal; Products containing bran or rough-ground grain
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D2/00—Treatment of flour or dough by adding materials thereto before or during baking
- A21D2/08—Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
- A21D2/14—Organic oxygen compounds
- A21D2/18—Carbohydrates
- A21D2/181—Sugars or sugar alcohols
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D2/00—Treatment of flour or dough by adding materials thereto before or during baking
- A21D2/08—Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
- A21D2/14—Organic oxygen compounds
- A21D2/18—Carbohydrates
- A21D2/183—Natural gums
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D6/00—Other treatment of flour or dough before baking, e.g. cooling, irradiating, heating
- A21D6/005—Irradiation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/198—Dry unshaped finely divided cereal products, not provided for in groups A23L7/117 - A23L7/196 and A23L29/00, e.g. meal, flour, powder, dried cereal creams or extracts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02B—PREPARING GRAIN FOR MILLING; REFINING GRANULAR FRUIT TO COMMERCIAL PRODUCTS BY WORKING THE SURFACE
- B02B5/00—Grain treatment not otherwise provided for
- B02B5/02—Combined processes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Definitions
- the present invention relates to a method for processing whole grain flour, and more particularly to a method for producing a fortified whole grain flour by pulsed electric field synergistic ultrafine pulverization.
- Whole grain flour refers to all edible parts of various grains such as wheat, corn, rice, oats, barley, and beans.
- the whole grain flour consists of three parts: the cortex, the endosperm and the germ, and the refined grain is used to obtain the bran and the secondary powder in the cortex and germ.
- Bran is a rough outer layer of whole grains. It contains a lot of minerals in grains and cellulose, unsaturated fatty acids, B vitamins, antioxidants, phytonutrients and other active ingredients. Its nutritional utility can not be ignored.
- the secondary powder contains a large amount of protein, but the protein has poor ductility and viscoelasticity.
- whole grain foods have a certain health-care function due to high dietary fiber, low fat, low saturated fatty acids, low cholesterol and low calories.
- minerals and vitamins such as calcium, magnesium, zinc, potassium and selenium contained in whole wheat have the function of promoting human growth and development.
- Dietary fiber can improve digestion, lower cholesterol, blood sugar and improve blood lipid metabolism. Reduce the risk of heart disease and reduce the risk of heart failure.
- Insoluble fiber can promote intestinal peristalsis and reduce obesity. For whole grain flour, how to find the best balance between taste, nutrition and safety, and achieve higher economic and social benefits, and become the focus of research.
- the current commercial whole grain flour is generally prepared by adding a mixture of bran and germ in a certain proportion in a special flour, and pulverizing a small amount using whole grains.
- Process technology for the direct production of whole grain flour or semi-whole grain flour using existing flour mills is also being studied.
- the methods for processing whole grain flours that have been publicly disclosed mainly include:
- Chinese invention patent CN 102438458 B discloses a method for preparing highly dispersible whole grain flour, which uses oc-amylase to hydrolyze whole grain flour and then heats it through a cooking extruder. The enzyme is depressurized in a pressurized manner, and the pellet at the exit of the extruder is finely ground to obtain a product;
- 200710138585.3 discloses a method for superfinely pulverizing whole wheat flour using ultraviolet and high frequency microwaves. Sterilization, after superfine pulverization The material is sterilized by the above method, and the finished product is obtained after measurement and packaging.
- Chinese invention patent application 20121032647 8.4 discloses a method for stabilizing bran, which is made from wheat as raw material, and is dried by ultraviolet microwave after hot steam treatment to obtain a finished product; In the preparation process of the whole wheat flour described in the invention patents CN101253954A and CN102150840A, the bran is subjected to extrusion and enzymatic treatment before the powdering.
- the Chinese invention patent application 201410007683.3 discloses a method for producing whole wheat flour by steam blasting technology. The method directly presses and heats the wheat grain, and the grain after the pressure is pulverized to obtain the whole wheat flour.
- the object of the present invention is to provide a pulse electric field synergistic ultrafine pulverization method for producing whole grain flour, and the process uses non-heat treatment technology to reduce damage to protein and starch.
- the obtained whole grain powder has high thermal stability, safety, comprehensive nutrition, bright color, good palatability, high application value, simple process and easy operation.
- a pulse electric field synergistic ultrafine pulverization method for producing whole grain flour comprises the following steps:
- the water content is less than 14%, and then sieved to obtain the treated bran and the secondary powder;
- the treated bran and the secondary powder obtained in the step (6) are uniformly mixed with the flour obtained in the step (1) to obtain a whole grain flour.
- Step (4) The polysaccharide colloid is gum arabic, konjac gum, carrageenan, xanthan gum or pectin.
- Step (5) The specific parameters of the high-voltage pulse processing are: a pulse frequency of 500-1500 Hz, a pulse width of 20-40 s, a flow rate of 300-600 IJh, and an electric field strength of 10-50.
- the kV/cm and pulse processing time are 70-550 s.
- Step (1) of the cleaning including screening, stone removal, magnetic separation, air selection and wheat.
- Step (2) The sieving is a 60 mesh sieve.
- the sieving described in step (6) is a sieve having a mesh size of 80 mesh.
- the centrifugation described in the step (6) is specifically: centrifuging at 3000-5000 r/min for 5-15 min.
- the present invention can significantly improve the rough taste of the whole grain flour, prolong the shelf life and storage stability of the whole grain flour, and improve the thermal stability of the whole wheat flour while reducing the damage of the starch content.
- the pulse electric field effect of the invention can promote the snoring of the amino acid side chain, facilitate the access of the polysaccharide molecule, thereby increasing the protein strength, ductility and viscoelasticity of the whole grain flour, thereby improving the application range thereof. Improve the quality of whole grain products.
- the steamed bread made from the whole grain powder treated by the present invention has a reduced mouth roughness, an increase in viscoelasticity and chewiness, and an increase in the aspect ratio of the steamed bread; and the untreated whole grain flour under the same conditions, The palatability and viscoelasticity are poor, and the height to diameter ratio is low.
- the prepared bread has uniform voids, good mouthfeel and is not easy to age; the noodles produced are obviously reduced in the broken rate, the toughness of the noodles is large, and the cooking loss rate is decreased.
- the pulsed electric field can effectively blunt the enzyme and preserve the original flavor, color, taste and nutritional value of the food to the utmost extent.
- FIG. 2 is a flow chart of a method for producing a fortified whole grain flour by pulsed electric field synergistic ultrafine pulverization according to an embodiment of the present invention.
- the wheat (hard wheat) grain is obtained by the above-mentioned milling to obtain bran, secondary powder and flour, and the bran and the secondary powder are ultra-finely pulverized, and after passing through a 60 mesh sieve, a 20% suspension is prepared, and a mixer is used. Keep the suspension even. Add the suspension to the 0.2%.
- the flow rate is 300 IJh
- the pulse frequency is 1500 Hz
- the electric field strength is 50 kV/cm
- the processing time is 70 ⁇ 8.
- the treated bran and secondary powder suspension were centrifuged at 5000 r/min for 15 min, and the supernatant was removed, and the precipitate was at 30 °C. Dry at C to a moisture content of 14% or less, grind through a 80 mesh sieve, and mix well with the flour in a mixer to obtain whole wheat flour.
- the whole wheat flour has a bran star content of 15%, a particle size D50 ( ⁇ ) of 13.92, a gluten index of 82, and a broken starch content of 8%.
- only superfinely pulverized whole wheat flour has a bran star content of 28%, a particle size D50 of 36.88, a gluten index of 66, and a broken starch content of 24%;
- the wheat (medium-quality wheat) grain is obtained by the above-mentioned milling to obtain bran, secondary powder and flour, and the bran and the secondary powder are ultra-finely pulverized, and after passing through a 60 mesh sieve, a 25% suspension is prepared, and used.
- the mixer keeps the suspension even.
- the suspension was added to 0.4%.
- set the pulse electric field parameters to be: pulse width 40 ⁇ 8 , flow rate 600 IJh, pulse frequency 1000 Hz, electric field strength 30 kV/cm, processing time 500 .
- the treated bran and secondary powder suspension were centrifuged at 3000 r/min for 10 min, and the supernatant was removed, and the precipitate was at 37. Dry to a moisture content of 14% or less, grind through a 80 mesh sieve, and mix well with the flour in the mixer to obtain whole wheat flour.
- the whole wheat flour has a bran star content of 12% and a particle size D50 ( ⁇ ) of 15.04. , gluten index 74, broken starch content of 9%.
- only superfinely pulverized whole wheat flour has a bran star content of 25%, a particle size D50 of 30.12, a gluten index of 62, and a broken starch content of 21%; the comparative data is shown in Fig. 1.
- the wheat (soft wheat) grain is obtained by the above-mentioned milling to obtain bran, secondary powder and flour, and the bran and the secondary powder are ultra-finely pulverized, and after passing through a 60 mesh sieve, a 30% suspension is prepared, and a mixer is used. Keep the suspension even. Add the suspension to the mouth by 0.5%.
- the treated bran and secondary powder suspension were centrifuged at 5000 r/min for 5 min, and the supernatant was removed, and the precipitate was at 37. Dry to a moisture content of 14% or less, grind the 80 mesh sieve, and mix it with the flour in the mixer to obtain whole wheat flour.
- the whole wheat flour has a bran star content of 12% and a particle size D50 of 28.32.
- Gluten index 66 the broken starch content is 12%.
- only superfinely pulverized whole wheat flour has a bran star content of 24%, a particle size D50 of 3 6.88, a gluten index of 54 and a broken starch content of 29%; the comparative data is shown in Fig. 1.
- the above embodiments are preferred embodiments of the present invention, but the embodiments of the present invention are not limited by the examples, and the polysaccharide colloid of the present invention may also be gum arabic, xanthan gum or other polysaccharide colloids.
- the grain may be oat, wheat, corn, rice, barley, rye, sorghum, triticale, sweet sorghum or bitter buckwheat. Any other changes, modifications, substitutions, and modifications made without departing from the spirit and principles of the present invention. Combinations, simplifications, and equivalent replacements are all included in the scope of the present invention.
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Molecular Biology (AREA)
- Cereal-Derived Products (AREA)
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US15/755,162 US10785983B2 (en) | 2015-08-28 | 2015-12-29 | Method for producing intensified whole-cereal flour by means of pulsed electric fields in collaboration with ultrafine pulverization |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510547007.X | 2015-08-28 | ||
CN201510547007.XA CN105076977B (zh) | 2015-08-28 | 2015-08-28 | 一种脉冲电场协同超微粉碎生产强化全谷物粉的方法 |
Publications (1)
Publication Number | Publication Date |
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WO2017036036A1 true WO2017036036A1 (zh) | 2017-03-09 |
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EP3841890A4 (en) * | 2019-05-22 | 2021-12-29 | Mizkan Holdings Co., Ltd. | Insoluble dietary fiber-containing solid composition and method for manufacturing same |
CN113100390B (zh) * | 2021-04-30 | 2023-12-01 | 淮阴工学院 | 一种杂粮面条的制备方法 |
CN116099590A (zh) * | 2022-12-30 | 2023-05-12 | 和县万谷粮油有限责任公司 | 一种降低碎米率的大米加工方法 |
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