WO2015037315A1 - 成膜装置および成膜方法 - Google Patents
成膜装置および成膜方法 Download PDFInfo
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- WO2015037315A1 WO2015037315A1 PCT/JP2014/068183 JP2014068183W WO2015037315A1 WO 2015037315 A1 WO2015037315 A1 WO 2015037315A1 JP 2014068183 W JP2014068183 W JP 2014068183W WO 2015037315 A1 WO2015037315 A1 WO 2015037315A1
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/56—Apparatus specially adapted for continuous coating; Arrangements for maintaining the vacuum, e.g. vacuum locks
- C23C14/564—Means for minimising impurities in the coating chamber such as dust, moisture, residual gases
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32082—Radio frequency generated discharge
- H01J37/32091—Radio frequency generated discharge the radio frequency energy being capacitively coupled to the plasma
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/34—Gas-filled discharge tubes operating with cathodic sputtering
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2237/00—Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
- H01J2237/32—Processing objects by plasma generation
- H01J2237/33—Processing objects by plasma generation characterised by the type of processing
- H01J2237/332—Coating
- H01J2237/3321—CVD [Chemical Vapor Deposition]
Definitions
- the present invention relates to a film forming apparatus, and more particularly to a film forming apparatus and a film forming method for performing film formation by sputtering on a resin workpiece.
- injection molded resin products are used as reflectors and instruments for automobile headlamps.
- film formation by sputtering using a metal such as aluminum as a target is performed for the purpose of providing a mirror finish or a metallic texture.
- a silicon oxide protective film or the like is formed by plasma CVD in order to prevent oxidation of the metal film. That is, the workpiece after film formation by sputtering is transferred to another film formation apparatus, and plasma CVD using a monomer gas such as HMDSO (hexa-methyl-di-siloxane) is performed in the chamber of the film formation apparatus.
- a protective film is formed on the surface after the film formation by sputtering.
- Patent Document 1 discloses a film forming apparatus in which a sputtering electrode and a composite film forming or polymerization film forming electrode are arranged at positions separated by a predetermined distance.
- a work and a sputtering electrode are arranged to face each other, and after introducing an inert gas into the chamber, direct current is applied to the sputtering electrode to perform film formation by sputtering.
- the film forming apparatus described in Patent Document 1 has a configuration in which a shutter is arranged on a target that is not used.
- the present invention has been made to solve the above-described problems, and an object thereof is to provide a film forming apparatus and a film forming method capable of completing a film forming process on a resin workpiece in a short time. To do.
- the invention described in claim 1 is a film forming apparatus for performing film formation by sputtering on a resin work, and a chamber for storing the work, and the inside of the chamber is 0.1 Pascal or more and 1.0 Pascal.
- Pressure reducing means for reducing the pressure to less than the pressure
- an inert gas supply unit for supplying an inert gas into the chamber, a target material, a sputtering electrode disposed in the chamber, and a surface area of the target material
- a DC power supply for applying a DC voltage to the sputter electrode is provided so that the input power is 25 watts or more per square centimeter.
- the invention according to claim 2 is the invention according to claim 1, further comprising a gas supply unit for supplying a gas having a dew point of 0 degrees Celsius or less into the chamber.
- the pressure reducing means includes a turbo molecular pump having a maximum exhaust speed of 300 liters or more per second.
- the invention according to claim 4 is the invention according to any one of claims 1 to 3, wherein a CVD electrode disposed in the chamber, a high-frequency power source for applying a high-frequency voltage to the CVD electrode, A source gas supply unit for supplying a source gas into the chamber; a shutter that is movable between a contact position that covers the target material by contacting the sputtering electrode; and a retreat position that is separated from the sputtering electrode; are further provided.
- the invention according to claim 5 is a film forming method for performing film formation by sputtering on a resin workpiece, and carrying in the injection molded resin workpiece into the chamber from the injection molding machine.
- a gas having a dew point of 0 degrees Celsius or less is supplied into the chamber.
- the chamber in the fifth aspect of the present invention, in the decompression step, is evacuated at an evacuation rate of 300 liters per second or more.
- a shutter arranging step of covering the target material with a shutter after the DC voltage applying step and before the venting step And a source gas supply step for supplying source gas into the chamber, and a high frequency application step for applying a high frequency voltage to the CVD electrode disposed in the chamber.
- suitable film formation can be performed even when the pressure in the chamber before film formation is about 0.1 Pascal or more and less than 1.0 Pascal. Is possible. For this reason, it is possible to reduce the time required for film formation, and it is possible to form a workpiece that is sent out from the injection molding machine at a constant interval in a manner linked with the production cycle of the workpiece by the injection molding machine.
- the moisture contained in the air can be reduced from adhering to the chamber, and the evacuation time during the next film formation process can be shortened. It becomes.
- film formation by sputtering and film formation by plasma CVD can be continuously performed in a short time in the same chamber.
- FIG. 1 is a schematic front view of a film forming apparatus according to the present invention. It is a side surface schematic diagram which shows the principal part of the film-forming apparatus which concerns on this invention. It is a side surface schematic diagram which shows the raising / lowering operation
- FIG. 1 is a schematic front view of a film forming apparatus according to the present invention
- FIG. 2 is a schematic side view showing an essential part thereof.
- the film forming apparatus performs film formation by sputtering and film formation by plasma CVD on a resin workpiece.
- the pressure in the chamber is set to a medium vacuum of 0.1 Pascal or more and less than 1.0 Pascal to shorten the time required for film formation.
- a DC voltage is applied to the sputter electrode so that the input power is 25 watts or more per square centimeter with respect to the surface area of the target material.
- This film forming apparatus includes a chamber 10 composed of a main body 11 and an opening / closing part 12.
- the opening / closing part 12 is movable between a loading / unloading position for loading an injection-molded resin workpiece W and a closed position constituting the chamber 10 sealed with the main body 11 via the packing 14. It has become.
- an opening for carrying the work W into and out of the chamber 10 is formed on the side surface of the chamber 10.
- a work placement portion 13 for placing the work W is disposed so as to pass through a passage hole formed in the opening / closing portion 12.
- the workpiece placement unit 13 is movable relative to the opening / closing unit 12 with the workpiece W placed thereon.
- this film forming apparatus includes a sputter electrode 23 composed of an electrode part 21 and a target material 22.
- the sputter electrode 23 is attached to the main body 11 in the chamber 10 via an insulating member (not shown).
- the main body 11 constituting the chamber 10 is grounded by a grounding portion 19.
- the sputter electrode 23 is connected to a DC power source 41.
- this DC power supply 41 what can apply a DC voltage to the sputter electrode 23 so that it may become input electric power of 25 watts or more per square centimeter with respect to the surface area of the target material 22 is used. That is, the DC power supply 41 inputs 25 watts or more per square centimeter as the input power to the sputtering electrode 23 with respect to the surface area of the target material 22.
- this film forming apparatus includes a CVD electrode 24.
- the CVD electrode 24 is attached to the main body 11 in the chamber 10 through an insulating member (not shown), like the sputtering electrode 23.
- the CVD electrode 24 is connected to a matching box 46 and a high frequency power source 45.
- the high frequency power supply 45 described above for example, one that generates a high frequency of about several tens of MHz (megahertz) can be used.
- the high frequency described in this specification means a frequency of 20 kHz (kilohertz) or more.
- the main body 11 constituting the chamber 10 is connected to a supply unit 33 of an inert gas such as argon via an on-off valve 31 and a flow rate adjustment valve 32.
- the main body 11 constituting the chamber 10 is connected to a source gas supply unit 36 such as HMDSO or HMDS (hexa-methyl-di-silazane) through an on-off valve 34 and a flow rate adjustment valve 35.
- the main body 11 constituting the chamber 10 is connected to a dry air supply unit 83 via an on-off valve 81 and a flow rate adjustment valve 82.
- main body 11 constituting the chamber 10 is connected to a turbo molecular pump 37 via an on-off valve 39, and the turbo molecular pump 37 is connected to an auxiliary pump 38 via an on-off valve 48. Further, the auxiliary pump 38 is also connected to the main body 11 constituting the chamber 10 through an on-off valve 49.
- turbo molecular pump 37 a pump having a maximum exhaust speed of 300 liters or more per second is used.
- the pump itself can be reduced in size while obtaining a large exhaust speed. For this reason, the film forming apparatus itself can be miniaturized.
- dry air supplied from the above-described dry air supply unit 83 one having a dew point of 0 degrees Celsius or less is used.
- an inert gas having a dew point of 0 degrees Celsius or less may be used.
- the film forming apparatus also includes a shutter 51 that can move up and down between a contact position that covers the target material 22 by contacting the sputter electrode 23 and a retracted position near the bottom of the chamber 10.
- the shutter 51 is made of a conductive material such as metal and a non-magnetic material.
- a material of the shutter 51 for example, aluminum can be adopted.
- the shutter 51 is lifted from the retracted position toward the contact position by driving the air cylinder 53 while being supported from below by the cylinder rod 54 of the air cylinder 53.
- the shutter 51 is supported at a contact position by a slide pin 62 (see FIGS. 7 to 9) at the tip of the cylinder rod in the air cylinder 61 fixed to the main body 11 in the chamber 10 by the L-shaped bracket 18.
- the air cylinder 53 functions as a shutter lifting mechanism that lifts the shutter 51 from the retracted position toward the contact position by supporting the shutter 51 from below.
- the air cylinder 61 supports the shutter 51 at the contact position. Functions as a shutter support mechanism.
- 3 to 6 are schematic side views showing the lifting and lowering operation of the shutter 51 by the shutter lifting and lowering mechanism.
- 7 to 9 are partially enlarged views showing the support operation of the shutter 51 by the shutter support mechanism.
- FIG. 3 shows a state in which the shutter 51 is disposed below the sputter electrode 23 at a retracted position near the bottom of the main body 11 constituting the chamber 10.
- the shutter 51 is supported by a support portion 52 attached to the bottom of the main body 11.
- the cylinder rod 54 of the air cylinder 53 is in a contracted state accommodated in the main body of the air cylinder 53.
- the shutter 51 When the shutter 51 is moved from the retracted position shown in FIG. 3 to a contact position that covers the target material 22 by contacting the sputter electrode 23, the shutter 51 is first supported by the cylinder rod 54 of the air cylinder 53. By extending the cylinder rod 54, the shutter 51 is raised to a position directly below the sputter electrode 23 as shown in FIG. In this state, as shown in FIG. 7, the lower surface of the target material 22 in the sputtering electrode 23 and the front surface of the shutter 51 are separated by a minute distance d.
- a concave portion 59 having a tapered surface is formed at the edge of the shutter 51.
- the recesses 59 are formed at the positions of the four corners of the rectangular shutter 51 in plan view.
- the air cylinder 61 described above is disposed at a position facing the recess 59 when the shutter 51 is raised by the action of the air cylinder 53.
- the air cylinder 61 is fixed to the main body 11 in the chamber 10 by an L-shaped metal fitting 18, and a slide pin 62 at the tip of the cylinder rod in the air cylinder 61 passes through the main body 11.
- a tapered portion having a shape corresponding to the tapered surface of the recess 59 formed in the shutter 51 is formed at the tip of the slide pin 62.
- the slide pin 62 at the tip of the cylinder rod in the air cylinder 61 is extended toward the shutter 51.
- the tip of the slide pin 62 is disposed at a position facing the upper end of the recess 59 formed in the shutter 51.
- the tip of the slide pin 62 enters the recess 59 formed in the shutter 51.
- the shutter 51 moves upward in accordance with the intrusion operation into the recess 59 at the tip of the slide pin 62.
- the shutter 51 is disposed at a contact position that covers the target material 22 by contacting the sputtering electrode 23, and is supported at that position.
- the cylinder rod 54 of the air cylinder 53 is lowered, and the cylinder rod 54 is brought into a contracted state accommodated in the main body of the air cylinder 53. Thereby, a space in which the workpiece W can be arranged is formed below the sputter electrode 23 and the shutter 51.
- the film forming operation by the film forming apparatus having the above configuration will be described.
- the injection-molded work W is transferred from the injection molding machine and transferred into the chamber 10.
- the opening / closing part 12 is moved to the loading / unloading position, and the work W placed on the work placing part 13 is opposed to the sputter electrode 23 in the chamber 10 as indicated by a virtual line in FIG. Place it at the position you want.
- the shutter 51 is disposed at a retracted position near the bottom of the chamber 10.
- four workpieces W are injection-molded and discharged in one shot from the preceding injection molding machine, and these four workpieces W are collectively carried into a film forming apparatus for film formation. Processing.
- the film forming operation can be performed efficiently, and adsorbed gas such as moisture can be prevented from adhering to the workpiece W.
- two injection molding machines and one film forming apparatus may be combined.
- eight workpieces having the same size as above are discharged from the injection molding machine in one shot, one injection molding machine and two film forming apparatuses may be combined. That is, the combination of the injection molding machine and the film forming apparatus may be considered according to the amount and size of the work discharged from the injection molding machine and the cycle time.
- the opening / closing part 12 is placed at the closed position, and the inside of the chamber 10 is depressurized from 0.1 Pascal to a medium vacuum of less than 1 Pascal.
- the turbo pump 37 having a maximum pumping speed of 300 liters per second or more is used, the chamber 10 has a time of about 20 seconds, from 0.1 Pascal to a medium vacuum of less than 1 Pascal.
- the pressure can be reduced. If necessary, the pressure is reduced at a high speed to about 100 Pascal using an auxiliary pump 38 such as a dry pump before the pressure is reduced by the turbo molecular pump 37.
- an inert gas such as argon is supplied into the chamber 10 from the inert gas supply unit 33 so that the degree of vacuum in the chamber 10 is 0.5 to 3 Pascals.
- the chamber 10 is filled with an inert gas.
- a DC voltage is applied from the DC power supply 41 to the sputter electrode 23. Thereby, a thin film of the target material 22 is formed on the surface of the workpiece W by a sputtering phenomenon.
- a DC voltage is applied from the DC power supply 41 to the sputtering electrode 23 so that the input power is 25 watts or more per square centimeter relative to the surface area of the target material 22 in the sputtering electrode 23.
- the input power is 25 watts or more per square centimeter relative to the surface area of the target material 22 in the sputtering electrode 23.
- This plasma polymerization is a kind of plasma CVD (Chemical Vapor Deposition).
- the work W placed on the work placement unit 13 is placed at a position facing the CVD electrode 24 in the chamber 10. 1 and 2, the shutter 51 is disposed at a contact position that covers the target material 22 by contacting the sputter electrode 23. In this state, the shutter 51 is supported by the slide pin 62 in the air cylinder 61 as shown in FIG. Further, the cylinder rod 54 of the air cylinder 53 is in a contracted state housed in the main body of the air cylinder 53 as shown in FIG.
- the source gas is supplied from the source gas supply unit 36 into the chamber 10, and the degree of vacuum in the chamber 10 is 0.1 to 10 Pascals.
- the inside is filled with raw material gas.
- a high frequency voltage is applied from the high frequency power supply 45 to the CVD electrode 24 via the matching box 46 to perform film formation by plasma polymerization.
- a thin film of the source gas is deposited on the surface of the workpiece W by the plasma polymerization reaction.
- the inside of the chamber 10 is vented.
- the inside of the chamber 10 is vented by dry air by opening the on-off valve 81 and supplying dry air from the dry air supply unit 83 into the chamber 10.
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Abstract
Description
11 本体
12 開閉部
13 ワーク載置部
19 接地部
21 電極部
22 ターゲット材料
23 スパッタ電極
31 開閉弁
32 流量調整弁
33 不活性ガスの供給部
34 開閉弁
35 流量調整弁
36 原料ガスの供給源
37 ターボ分子ポンプ
38 補助ポンプ
39 開閉弁
41 直流電源
45 高周波電源
46 マッチングボックス
48 開閉弁
49 開閉弁
51 シャッター
81 開閉弁
82 流量調整弁
83 ドライエアの供給部
W ワーク
Claims (8)
- 樹脂製のワークに対してスパッタリングによる成膜を実行する成膜装置であって、
ワークを収納するチャンバーと、
前記チャンバー内を0.1パスカル以上1.0パスカル未満の圧力に減圧する減圧手段と、
前記チャンバー内に不活性ガスを供給する不活性ガス供給部と、
ターゲット材料を備え、前記チャンバー内に配設されたスパッタ電極と、
前記ターゲット材料の表面積に対して、1平方センチ当たり25ワット以上の投入電力となるように、前記スパッタ電極に直流電圧を印加する直流電源と、
を備えたことを特徴とする成膜装置。 - 請求項1に記載の成膜装置において、
前記チャンバー内に露点が摂氏0度以下の気体を供給する気体供給部をさらに備える成膜装置。 - 請求項1に記載の成膜装置において、
前記減圧手段は、最大排気速度が1秒当たり300リットル以上のターボ分子ポンプを有する成膜装置。 - 請求項1から請求項3のいずれかに記載の成膜装置において、
前記チャンバー内に配設されたCVD電極と、
前記CVD電極に高周波電圧を印加する高周波電源と、
前記チャンバー内に原料ガスを供給する原料ガス供給部と、
前記スパッタ電極と当接することにより前記ターゲット材料を覆う当接位置と、前記スパッタ電極から離隔する退避位置との間を移動可能なシャッターと、
をさらに備える成膜装置。 - 樹脂製のワークに対してスパッタリングによる成膜を実行する成膜方法であって、
射出成型された樹脂製のワークを、射出成形機よりチャンバー内に搬入する搬入工程と、
前記チャンバー内を0.1パスカル以上1.0パスカル未満の圧力に減圧する減圧工程と、
前記チャンバー内に不活性ガスを供給する不活性ガス供給工程と、
ターゲット材料を備え前記チャンバー内に配設されたスパッタ電極に対し、前記ターゲット材料の表面積に対して、1平方センチ当たり25ワット以上の投入電力となるように、前記スパッタ電極に直流電圧を印加する直流電圧印加工程と、
前記チャンバー内を大気圧までベントするベント工程と、
成膜完了後のワークを前記チャンバー内から搬出する搬出工程と、
を備えたことを特徴とする成膜装置。 - 請求項5に記載の成膜方法において、
前記ベント工程においては、前記チャンバー内に露点が摂氏0度以下の気体を供給する成膜方法。 - 請求項5に記載の成膜方法において、
前記減圧工程においては、1秒当たり300リットル以上の排気速度で前記チャンバー内から排気を行う成膜方法。 - 請求項5から請求項7のいずれかに記載の成膜方法において、
前記直流電圧印加工程の後で前記ベント工程の前に、
前記ターゲット材料をシャッターにより覆うシャッター配置工程と、
前記チャンバー内に原料ガスを供給する原料ガス供給工程と、
前記チャンバー内に配設されたCVD電極に高周波電圧を印加する高周波印加工程と、
をさらに備える成膜方法。
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JP2016211051A (ja) * | 2015-05-12 | 2016-12-15 | 株式会社島津製作所 | 成膜装置、プラズマ処理装置および成膜方法 |
JP2017082291A (ja) * | 2015-10-29 | 2017-05-18 | 株式会社島津製作所 | 成膜方法および成膜装置 |
JP2020196942A (ja) * | 2019-06-05 | 2020-12-10 | 株式会社島津製作所 | 成膜方法、樹脂製品の製造方法および成膜装置 |
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JP7094154B2 (ja) * | 2018-06-13 | 2022-07-01 | 東京エレクトロン株式会社 | 成膜装置および成膜方法 |
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JP2020196942A (ja) * | 2019-06-05 | 2020-12-10 | 株式会社島津製作所 | 成膜方法、樹脂製品の製造方法および成膜装置 |
JP7188281B2 (ja) | 2019-06-05 | 2022-12-13 | 株式会社島津製作所 | 成膜方法、樹脂製品の製造方法および成膜装置 |
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JPWO2015037315A1 (ja) | 2017-03-02 |
JP6202098B2 (ja) | 2017-09-27 |
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