WO2011095447A2 - Pigment compositions with improved sparkling effect - Google Patents

Pigment compositions with improved sparkling effect Download PDF

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Publication number
WO2011095447A2
WO2011095447A2 PCT/EP2011/051288 EP2011051288W WO2011095447A2 WO 2011095447 A2 WO2011095447 A2 WO 2011095447A2 EP 2011051288 W EP2011051288 W EP 2011051288W WO 2011095447 A2 WO2011095447 A2 WO 2011095447A2
Authority
WO
WIPO (PCT)
Prior art keywords
pigment
trasub
perlite
platelet
pigments
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2011/051288
Other languages
English (en)
French (fr)
Other versions
WO2011095447A3 (en
Inventor
Raimund Schmid
Carolyn Lavallee
S. A. Jones
James Carroll
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to EP11701407.6A priority Critical patent/EP2531562B1/en
Priority to CN201180008112.6A priority patent/CN102741358B/zh
Priority to JP2012551585A priority patent/JP5984678B2/ja
Priority to KR1020127023000A priority patent/KR101821431B1/ko
Publication of WO2011095447A2 publication Critical patent/WO2011095447A2/en
Publication of WO2011095447A3 publication Critical patent/WO2011095447A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0081—Composite particulate pigments or fillers, i.e. containing at least two solid phases, except those consisting of coated particles of one compound
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0024—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings comprising a stack of coating layers with alternating high and low refractive indices, wherein the first coating layer on the core surface has the high refractive index
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1004—Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
    • C09C2200/1025—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin comprising at least one metal layer adjacent to core material, e.g. core-M or M-core-M
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1054—Interference pigments characterized by the core material the core consisting of a metal
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1087—Interference pigments characterized by the core material the core consisting of bismuth oxychloride, magnesium fluoride, nitrides, carbides, borides, lead carbonate, barium or calcium sulfate, zinc sulphide, molybdenum disulphide or graphite
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/301—Thickness of the core

Definitions

  • Plateletlike organic pigments such as plateletlike quinacridones, phthalocyanine, fluororu- bine, dioxazines, or diketopyrrolopyrroles can advantageously be used as component A.
  • Examples are plateletlike copperphthaloycyanine, 1 ,9-dichloroquinacridone or 1 ,9- dichloroanthraquinone.
  • 2,9-dichloroquinacridone in platelet form is, for example, described in WO08/055807.
  • the 2,9-dichloroquinacridone in platelet form described therein has a length of 1 to 45 ⁇ , a width of 0.1 to 20 ⁇ and an average thickness of 0.01 to 5 ⁇ .
  • Preferred examples of that type of metal acid ester are zirconium acetylacetonate, aluminium acetylacetonate, titanium acetylacetonate and diisobutyloleyl acetoacetylaluminate or diisopropyloleyl acetoacetylacetonate and mixtures of metal acid esters, for example Dynasil® (Hijls), a mixed aluminium/silicon metal acid ester.
  • a metal oxide having a high refractive index titanium dioxide is preferably used, the method described in US-B-3,553,001 being used, in accordance with an embodiment of the present invention, for application of the titanium dioxide layers.
  • the high molecular weight organic material for the pigmenting of which the pigment compositions according to the invention may be used may be of natural or synthetic origin.
  • High molecular weight organic materials usually have molecular weights of about from 10 3 to 10 8 g/mol or even more. They may be, for example, natural resins, drying oils, rubber or casein, or natural substances derived therefrom, such as chlorinated rubber, oil-modified alkyd resins, viscose, cellulose ethers or esters, such as ethylcellulose, cellulose acetate, cellulose propionate, cellulose acetobutyrate or nitrocellulose, but especially totally synthetic organic polymers (thermosetting plastics and thermoplastics), as are obtained by polymerisation, polycondensation or polyaddition.
  • the high molecular weight organic materials and the pigment compositions according to the invention where appropriate together with customary additives such as, for example, fillers, other pigments, siccatives or plasticisers, are finely dispersed or dissolved in the same organic solvent or solvent mixture, it being possible for the individual components to be dissolved or dispersed separately or for a number of components to be dissolved or dispersed together, and only thereafter for all the compo- nents to be brought together.
  • Processing a pigment composition according to the invention is preferably carried out subject to conditions under which only relatively weak shear forces occur so that the effect pigment is not broken up into smaller portions.
  • Paints, printing inks, plastics, cosmetics etc. can also be produced by adding an effect pigment and a platelet-like perlite separately to the formulations.
  • the present invention relates to paints, printing inks, plastics, cosmetics, ceramics and glass, which are pigmented with A) a platelet-like perlite (perlite); and B) an effect pigment.
  • the platelet-like perlite (perlite); and the effect pigment are as defined above.
  • Fig. 6 is a graph showing the Sparkling intensity (S_i) vs. the Sparkling area (S_a) of Pro17 to Pro20 and ComPro6.
  • the sparkling effects of the pigment compositions of Examples 1 to 8 are measured using a Byk-mac device from Byk-Gardner GmbH (Lausitzer StraBe 8, 82538 Geretsried, Germany). This device is allowing to measure sparkle and graininess for flake characterization. Accordingly, the sparkling behaviour of the products (Pro1 to Pro28) and the comparative products (ComProl to ComPro8) is characterized for three different illumination angles (direct illumination: 15°, 45° and 75° from perpendicular; camera detection: 0°) with the following parameters :

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Composite Materials (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Cosmetics (AREA)
PCT/EP2011/051288 2010-02-04 2011-01-31 Pigment compositions with improved sparkling effect Ceased WO2011095447A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP11701407.6A EP2531562B1 (en) 2010-02-04 2011-01-31 Pigment compositions with improved sparkling effect
CN201180008112.6A CN102741358B (zh) 2010-02-04 2011-01-31 具有改进闪光效应的颜料组合物
JP2012551585A JP5984678B2 (ja) 2010-02-04 2011-01-31 改善されたきらめき効果を有する顔料組成物
KR1020127023000A KR101821431B1 (ko) 2010-02-04 2011-01-31 개선된 스파클링 효과를 갖는 안료 조성물

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US30124510P 2010-02-04 2010-02-04
US61/301,245 2010-02-04

Publications (2)

Publication Number Publication Date
WO2011095447A2 true WO2011095447A2 (en) 2011-08-11
WO2011095447A3 WO2011095447A3 (en) 2011-10-06

Family

ID=43618253

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2011/051288 Ceased WO2011095447A2 (en) 2010-02-04 2011-01-31 Pigment compositions with improved sparkling effect

Country Status (6)

Country Link
US (2) US20110237683A1 (enExample)
EP (1) EP2531562B1 (enExample)
JP (1) JP5984678B2 (enExample)
KR (1) KR101821431B1 (enExample)
CN (1) CN102741358B (enExample)
WO (1) WO2011095447A2 (enExample)

Cited By (10)

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EP2727966A1 (de) * 2012-11-06 2014-05-07 Eckart GmbH Pigment mit photokatalytischer Aktivität, Verfahren zu dessen Herstellung und Beschichtungsmittel
WO2014142884A1 (en) * 2013-03-14 2014-09-18 Basf Se Coated perlite flakes
CN104661665A (zh) * 2012-03-19 2015-05-27 巴斯夫公司 经过处理的片状基材
CN104704063A (zh) * 2012-10-05 2015-06-10 巴斯夫公司 含氧化铁的效果颜料、其制备及其用途
US9839587B2 (en) 2012-03-12 2017-12-12 Basf Corporation Treated platy substrates
US9878348B2 (en) 2013-12-19 2018-01-30 Hyundai Motor Company Coating composition with improved sense of sparkle and coating method using coating composition
EP4006109A4 (en) * 2019-07-23 2023-07-26 Nippon Sheet Glass Company, Limited NEAR INFRARED SHIELDING MATERIAL
US11713277B2 (en) * 2012-04-20 2023-08-01 Schott Ag Glass or glass ceramic substrate provided with a decorative coating and method for producing same
CN117887306A (zh) * 2023-12-27 2024-04-16 广东精英无机材料有限公司 一种陶瓷喷墨打印墨水用红色色素及其制备方法和应用
WO2025219190A1 (en) 2024-04-17 2025-10-23 Eckart Gmbh Effect pigment preparation for powder coating

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US10131808B2 (en) * 2012-03-14 2018-11-20 Basf Coatings Gmbh Solventborne pigment pastes comprising metallic pigments and use thereof for producing solventborne effect coating materials
KR101405194B1 (ko) 2012-10-24 2014-06-13 현대자동차 주식회사 차량용 스털링 냉동기
US9320687B2 (en) 2013-03-13 2016-04-26 Johnson & Johnson Consumer Inc. Pigmented skin-care compositions
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US8585818B1 (en) * 2013-03-14 2013-11-19 Basf Se Coated perlite flakes
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EP2799398B1 (en) 2013-04-30 2018-05-23 Merck Patent GmbH alpha-Alumina flakes
DE112015001639B4 (de) 2014-04-01 2023-12-14 Toyota Jidosha Kabushiki Kaisha Nicht-farbverschiebende mehrschichtige strukturen
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JP6162901B2 (ja) * 2014-07-10 2017-07-12 日本ペイントホールディングス株式会社 赤外反射性顔料及び赤外反射性塗料組成物
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JP6336948B2 (ja) * 2015-08-24 2018-06-06 富士フイルム株式会社 赤外線反射パターン形成用インク組成物、赤外線反射パターン形成方法、及び赤外線反射体
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EP3403824A4 (en) * 2016-01-13 2019-09-11 Nippon Paint Holdings Co., Ltd. MULTILAYER COATING FILM AND METHOD FOR FORMING A MULTILAYER COATING FILM
CN108463524B (zh) * 2016-01-13 2021-01-01 日本涂料控股有限公司 红外反射性涂料组合物
US10613727B2 (en) 2016-02-19 2020-04-07 Ppg Industries Ohio, Inc. Color and texture match ratings for optimal match selection
WO2018049223A2 (en) * 2016-09-09 2018-03-15 Melior Innovations Polymer derived ceramic effects particles, uses and methods of making
JP6647694B2 (ja) * 2016-11-17 2020-02-14 ナトコ株式会社 光輝性塗料組成物、光輝性塗装物、及び光輝性塗膜の形成方法
GB201620917D0 (en) * 2016-12-08 2017-01-25 Crown Packaging Technology Inc Forming a texture in a can surface decoration
CA3111745C (en) * 2016-12-21 2023-04-04 Viavi Solutions Inc. Particles having a vapor deposited colorant
CA2988904C (en) 2016-12-21 2020-05-05 Viavi Solutions Inc. Hybrid colored metallic pigment
CN110914371A (zh) 2017-04-04 2020-03-24 巴斯夫色彩与效果有限公司 无机效果颜料
PL3480263T3 (pl) * 2017-11-06 2021-10-11 Imertech Sas Przezroczyste kompozycje powłokowe
KR102656601B1 (ko) * 2018-06-29 2024-04-12 비아비 솔루션즈 아이엔씨. 반사 입자를 포함하는 조성물
WO2020115451A1 (en) * 2018-12-03 2020-06-11 Loughborough University Composite material
CN111303881A (zh) * 2018-12-11 2020-06-19 江苏罗化新材料有限公司 一种窄带绿色荧光粉及其制备方法和发光器件
JP7224938B2 (ja) * 2019-01-30 2023-02-20 象印マホービン株式会社 加熱容器の製造方法
CN113518839A (zh) 2019-03-04 2021-10-19 Viavi科技有限公司 具有纳米颗粒涂层的薄膜干涉颜料
CN113728057A (zh) 2019-03-04 2021-11-30 Viavi科技有限公司 包含纳米颗粒涂层的颜料
ES2937084T3 (es) 2019-04-12 2023-03-23 Eckart Gmbh Mezcla de pigmentos de efecto transparentes a la frecuencia de radar, formulaciones y revestimientos de la misma
DE102019210687A1 (de) * 2019-07-19 2021-01-21 Henkel Ag & Co. Kgaa Farbige Effektpigmente und deren Herstellung
US12365802B2 (en) 2019-11-29 2025-07-22 Viavi Solutions Inc. Composition including a color shifting pigment having a different particle size
EP3854856B1 (en) 2020-01-27 2023-08-23 Viavi Solutions Inc. Thin film interference pigments with a coating of nanoparticles
JP7186198B2 (ja) * 2020-07-03 2022-12-08 日本ペイント・オートモーティブコーティングス株式会社 塗料組成物および塗料組成物の製造方法
KR102471930B1 (ko) * 2020-12-03 2022-11-30 씨큐브 주식회사 폭발 안정성이 우수한 판상 알루미늄을 포함하는 안료 조성물 및 이의 제조방법
CN113248963A (zh) * 2021-05-07 2021-08-13 贵州永锐材料科技有限公司 一种汽车涂料用改性闪光粉
US20230046620A1 (en) * 2021-07-28 2023-02-16 L'oreal Long-wearing cosmetic composition comprising expanded perlite
US20250197609A1 (en) 2023-12-13 2025-06-19 Blue Evolution, Inc. Ecofriendly, biodegradable biological polysaccharide composition for packaging materials

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US20200032067A1 (en) 2020-01-30
JP5984678B2 (ja) 2016-09-06
CN102741358A (zh) 2012-10-17
JP2013518953A (ja) 2013-05-23
WO2011095447A3 (en) 2011-10-06
KR20120118515A (ko) 2012-10-26
CN102741358B (zh) 2015-11-25
EP2531562A2 (en) 2012-12-12
US20110237683A1 (en) 2011-09-29
KR101821431B1 (ko) 2018-01-23

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