WO2011041358A2 - Substrate and rubber composition and method of making the composition - Google Patents

Substrate and rubber composition and method of making the composition Download PDF

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Publication number
WO2011041358A2
WO2011041358A2 PCT/US2010/050645 US2010050645W WO2011041358A2 WO 2011041358 A2 WO2011041358 A2 WO 2011041358A2 US 2010050645 W US2010050645 W US 2010050645W WO 2011041358 A2 WO2011041358 A2 WO 2011041358A2
Authority
WO
WIPO (PCT)
Prior art keywords
rubber
composition
silanes
substrate
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2010/050645
Other languages
English (en)
French (fr)
Other versions
WO2011041358A3 (en
Inventor
Richard E. Dewald
Suky Singh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Federal Mogul LLC
Original Assignee
Federal Mogul LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Federal Mogul LLC filed Critical Federal Mogul LLC
Priority to EP10821140.0A priority Critical patent/EP2483444A4/en
Priority to KR1020167036978A priority patent/KR101749150B1/ko
Priority to CN201080040108.3A priority patent/CN102482782B/zh
Priority to BR112012004137A priority patent/BR112012004137A2/pt
Priority to JP2012532253A priority patent/JP2013506763A/ja
Publication of WO2011041358A2 publication Critical patent/WO2011041358A2/en
Publication of WO2011041358A3 publication Critical patent/WO2011041358A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
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    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
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    • C23C22/03—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using non-aqueous solutions containing phosphorus compounds
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Definitions

  • This invention provides a product comprised of a substrate and rubber composition attached to the substrate in which the product and its components are able to withstand extreme environmental conditions.
  • the product is produced using methods that significantly reduce or eliminate the use of metal treatment steps that result in having to dispose of excess metals used during the process.
  • the processes used to produce the product also reduce or simplify the steps of previously used manufacturing processes.
  • Preferred phosphoric acid compounds include phosphoric acid compounds of the general formula:
  • R is alkyl of 1 to 30 carbons and aryl of 6 to 30 carbons
  • n is an integer of from 1 to 6; including +1 and +2 metal salts of the phosphonic acids.
  • Examples of phosphonic acids and their salts include, but are not limited to, phosphonic acid (mono-alkyl and di-alkyl phosphonic acid, with alkyl having 1 to 10 carbons), n-dodecylphosphonic acid, ethylphosphonic acid, phenyl phosphonic acid, di-phenyl phosphonic acid, n-hexylphosphonic acid, n-butylphosphonic acid, n-decylphosphonic acid, n- undecylphosphonic acid, n-tridecylphosphonic acid, n-tetradecylphosphonic acid, n- pentadecylphosphonic acid, propylene diphosphonic acid, N,N-bis(phosphonomethyl)glycine, 1 ,2-ethylenediphosphonic acid, methylenediphosphonic acid, 1 , 1 -ethylidenediphosphonic acid, dimethylmethylenediphosphonic acid, nitrilotris(methylene
  • the mixture of phosphatizing reagent and silane coupling agent further comprises the addition of at least one phenolic resin.
  • the phenolic resin can be a resol resin, a novolac resin, or a combination thereof.
  • resol resins are produced by reacting a phenol compound with a stoichiometric excess of an aldehyde compound in the presence of an alkaline catalyst.
  • Novolac resins are generally produced by reacting an aldehyde compound with a stoichiometric excess of a phenol compound in the presence of an acid catalyst.
  • the mixture is formed from at least one phosphatizing reagent and at least one silane coupling agent selected from the group consisting of amino-silanes and vinyl-silanes.
  • the mixture is formed from at least one phosphatizing reagent and at least one silane coupling agent selected from the group consisting of amino-silanes and vinyl-silanes, without adding phenolic resin to produce the mixture.
  • acrylic rubber examples include rubber comprised of alkyl acrylate as a main component, such as a copolymer of an alkyl acrylate and a chlorine-containing crosslinkable monomer (ACM), a copolymer of an alkyl acrylate and acrylonitrile (ANM), a copolymer of an alkyl acrylate and a carboxyl group- and/or epoxy group-containing monomer, and an ethyl ene- acrylic rubber.
  • ACM chlorine-containing crosslinkable monomer
  • ANM acrylonitrile
  • ethyl ene- acrylic rubber examples include rubber comprised of alkyl acrylate as a main component, such as a copolymer of an alkyl acrylate and a chlorine-containing crosslinkable monomer (ACM), a copolymer of an alkyl acrylate and acrylonitrile (ANM), a copolymer of an alkyl acrylate and a carboxyl group- and/or epoxy
  • the silicone-series rubber (Q) includes, for example, a methylsilicone rubber (MQ), a vinylsilicone rubber (VMQ), a phenylsilicone rubber (PMQ), a phenylvinylsilicone rubber (PVMQ), a fluorosilicone rubber (FVMQ), and the like. Further, such a silicone-series rubber includes not only a solid rubber of the High Temperature Vulcanizable (HTV) silicone rubber but also a Room Temperature Vulcanizable (RTV) silicone rubber or Low Temperature
  • HTV High Temperature Vulcanizable
  • RTV Room Temperature Vulcanizable

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  • Chemical & Material Sciences (AREA)
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  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Laminated Bodies (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Adhesive Tapes (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Inorganic Chemistry (AREA)
  • Gasket Seals (AREA)
PCT/US2010/050645 2009-09-30 2010-09-29 Substrate and rubber composition and method of making the composition Ceased WO2011041358A2 (en)

Priority Applications (5)

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EP10821140.0A EP2483444A4 (en) 2009-09-30 2010-09-29 SUBSTRATE AND RUBBER COMPOSITION, AND METHOD FOR MANUFACTURING THE COMPOSITION
KR1020167036978A KR101749150B1 (ko) 2009-09-30 2010-09-29 기판 및 고무 조성물 및 구성물의 제조방법
CN201080040108.3A CN102482782B (zh) 2009-09-30 2010-09-29 一种基质和橡胶的复合物及其制造方法
BR112012004137A BR112012004137A2 (pt) 2009-09-30 2010-09-29 método para ligar uma composição de borracha a um substrato, e, composição
JP2012532253A JP2013506763A (ja) 2009-09-30 2010-09-29 基体およびゴム組成物、ならびに該組成物を作る方法

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US12/571,083 US8182646B2 (en) 2009-09-30 2009-09-30 Substrate and rubber composition and method of making the composition
US12/571,083 2009-09-30

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DE102019217128A1 (de) * 2019-11-06 2021-05-06 Robert Bosch Gmbh Verfahren zur Herstellung eines Bauteil-Elastomer-Verbundes

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US10197163B2 (en) * 2014-09-24 2019-02-05 Aktiebolaget Skf Dynamic seal
CN109280910A (zh) * 2018-10-10 2019-01-29 安徽腾龙泵阀制造有限公司 一种化工泵表面磷化处理工艺
CN112708391A (zh) * 2020-12-10 2021-04-27 晟大科技(南通)有限公司 柔性线路板fpc专用胶黏剂及其制备方法

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US8182646B2 (en) 2012-05-22
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US20110076501A1 (en) 2011-03-31
BR112012004137A2 (pt) 2019-09-24
WO2011041358A3 (en) 2011-07-28
CN102482782A (zh) 2012-05-30
JP2016128260A (ja) 2016-07-14
US9382451B2 (en) 2016-07-05
EP2483444A4 (en) 2014-03-19
JP6185092B2 (ja) 2017-08-23
EP2483444A2 (en) 2012-08-08
CN102482782B (zh) 2014-01-22
JP2013506763A (ja) 2013-02-28
KR20170003739A (ko) 2017-01-09
US20120237781A1 (en) 2012-09-20

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