WO2011008009A3 - 유기 클로로하이드로실란과 이의 제조방법 - Google Patents

유기 클로로하이드로실란과 이의 제조방법 Download PDF

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Publication number
WO2011008009A3
WO2011008009A3 PCT/KR2010/004548 KR2010004548W WO2011008009A3 WO 2011008009 A3 WO2011008009 A3 WO 2011008009A3 KR 2010004548 W KR2010004548 W KR 2010004548W WO 2011008009 A3 WO2011008009 A3 WO 2011008009A3
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WO
WIPO (PCT)
Prior art keywords
chlorosilane
organic
present
preparing same
bond
Prior art date
Application number
PCT/KR2010/004548
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English (en)
French (fr)
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WO2011008009A2 (ko
WO2011008009A9 (ko
Inventor
정일남
홍순현
김은성
현상일
Original Assignee
삼성정밀화학 주식회사
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by 삼성정밀화학 주식회사 filed Critical 삼성정밀화학 주식회사
Priority to US13/383,697 priority Critical patent/US20120114544A1/en
Priority to JP2012520540A priority patent/JP2012532927A/ja
Priority to CN201080040874XA priority patent/CN102498117A/zh
Publication of WO2011008009A2 publication Critical patent/WO2011008009A2/ko
Publication of WO2011008009A3 publication Critical patent/WO2011008009A3/ko
Publication of WO2011008009A9 publication Critical patent/WO2011008009A9/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/123—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-halogen linkages
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0267—Phosphines or phosphonium compounds, i.e. phosphorus bonded to at least one carbon atom, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, the other atoms bonded to phosphorus being either carbon or hydrogen
    • B01J31/0268—Phosphonium compounds, i.e. phosphine with an additional hydrogen or carbon atom bonded to phosphorous so as to result in a formal positive charge on phosphorous

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

본 발명은 실리콘 고분자를 제조하는데 유용한 출발물질인 유기 클로로하이드로실란과 이의 제조방법에 관한 것으로서, 더욱 상세하게는 4차 유기 포스포니움염 화합물을 촉매로 사용하여 값싸고 쉽게 얻을 수 있는 클로로실란의 Si-H 결합과 다른 유기클로로실란의 Si-Cl 결합을 교환시켜 여러 가지 새로운 유기 클로로하이드로실란을 고 수율로 합성하고, 또한 촉매를 사용한 후 회수하여 재사용이 가능하기 때문에 매우 경제적이므로 실리콘 원료물질을 대량생산하는데 효과적이다.
PCT/KR2010/004548 2009-07-13 2010-07-13 유기 클로로하이드로실란과 이의 제조방법 WO2011008009A2 (ko)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US13/383,697 US20120114544A1 (en) 2009-07-13 2010-07-13 Organic chlorohydrosilane and method for preparing them
JP2012520540A JP2012532927A (ja) 2009-07-13 2010-07-13 有機クロロヒドロシラン及びその製造方法
CN201080040874XA CN102498117A (zh) 2009-07-13 2010-07-13 有机氢氯硅烷及其制备方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2009-0063616 2009-07-13
KR1020090063616A KR101263789B1 (ko) 2009-07-13 2009-07-13 유기 클로로하이드로실란과 이의 제조방법

Publications (3)

Publication Number Publication Date
WO2011008009A2 WO2011008009A2 (ko) 2011-01-20
WO2011008009A3 true WO2011008009A3 (ko) 2011-06-23
WO2011008009A9 WO2011008009A9 (ko) 2011-08-04

Family

ID=43449959

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2010/004548 WO2011008009A2 (ko) 2009-07-13 2010-07-13 유기 클로로하이드로실란과 이의 제조방법

Country Status (5)

Country Link
US (1) US20120114544A1 (ko)
JP (1) JP2012532927A (ko)
KR (1) KR101263789B1 (ko)
CN (1) CN102498117A (ko)
WO (1) WO2011008009A2 (ko)

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SG183291A1 (en) 2010-02-17 2012-09-27 Air Liquide VAPOR DEPOSITION METHODS OF SiCOH LOW-K FILMS
US8697901B2 (en) * 2011-12-30 2014-04-15 Momentive Performance Materials Inc. Synthesis of organohalosilane monomers via enhanced cleavage of direct process residue
US8637695B2 (en) * 2011-12-30 2014-01-28 Momentive Performance Materials Inc. Synthesis of organohalosilane monomers from conventionally uncleavable Direct Process Residue
CN102850387A (zh) * 2012-09-18 2013-01-02 太仓市运通化工厂 一种二环戊基二氯硅烷的合成方法
JP6044361B2 (ja) * 2013-01-21 2016-12-14 信越化学工業株式会社 ジクロロモノヒドロシラン化合物の製造方法
JP6775418B2 (ja) * 2013-03-14 2020-10-28 モーメンティブ・パフォーマンス・マテリアルズ・インク 高屈折率シロキサン
KR101728308B1 (ko) 2015-09-14 2017-04-19 기초과학연구원 비전이금속 촉매법 수소규소화 반응을 이용한 규소 고분자 제조방법
WO2018186882A1 (en) * 2017-04-07 2018-10-11 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Catalytic reduction of halogenated carbosilanes and halogenated carbodisilanes
JP2020534324A (ja) * 2017-09-20 2020-11-26 モメンティブ パフォーマンス マテリアルズ インコーポレイテッドＭｏｍｅｎｔｉｖｅ Ｐｅｒｆｏｒｍａｎｃｅ Ｍａｔｅｒｉａｌｓ Ｉｎｃ． オルガノヒドリドクロロシランの製造方法
WO2019060486A1 (en) 2017-09-20 2019-03-28 Momentive Performance Materials Inc. PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES FROM HYDRUROSILANES
EP3781578B1 (de) 2018-09-06 2021-10-27 Wacker Chemie AG Verfahren zur dehydrierung von dichlorsilan
KR102654573B1 (ko) * 2018-12-10 2024-04-05 엔테그리스, 아이엔씨. 트리아이오도실란의 제조
KR102231991B1 (ko) * 2019-10-30 2021-03-25 주식회사 서연이화 테일게이트 인너 판넬용 폴리프로필렌 수지 조성물 및 이의 성형품

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JPH09173859A (ja) * 1995-11-30 1997-07-08 Wacker Chemie Gmbh オルガノシランを製造するための方法および触媒、ならびに該触媒の製造法
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KR20060112237A (ko) * 2005-04-26 2006-10-31 와커 헤미 아게 유기수소실란의 제조 방법

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Publication number Priority date Publication date Assignee Title
JPH08337588A (ja) * 1995-06-07 1996-12-24 Huels Ag アルキルヒドロゲンクロルシランの製造方法
JPH09173859A (ja) * 1995-11-30 1997-07-08 Wacker Chemie Gmbh オルガノシランを製造するための方法および触媒、ならびに該触媒の製造法
KR20020034849A (ko) * 2000-11-01 2002-05-09 박호군 유기 실란의 제조방법
KR20060112237A (ko) * 2005-04-26 2006-10-31 와커 헤미 아게 유기수소실란의 제조 방법

Also Published As

Publication number Publication date
KR101263789B1 (ko) 2013-05-13
WO2011008009A2 (ko) 2011-01-20
KR20110006125A (ko) 2011-01-20
JP2012532927A (ja) 2012-12-20
US20120114544A1 (en) 2012-05-10
WO2011008009A9 (ko) 2011-08-04
CN102498117A (zh) 2012-06-13

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