WO2010126132A3 - 変性ポリイミドの製造方法及び変性ポリイミド - Google Patents

変性ポリイミドの製造方法及び変性ポリイミド Download PDF

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Publication number
WO2010126132A3
WO2010126132A3 PCT/JP2010/057678 JP2010057678W WO2010126132A3 WO 2010126132 A3 WO2010126132 A3 WO 2010126132A3 JP 2010057678 W JP2010057678 W JP 2010057678W WO 2010126132 A3 WO2010126132 A3 WO 2010126132A3
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WIPO (PCT)
Prior art keywords
modified polyimide
polyimide
tetracarboxylic dianhydride
aromatic
oligomer
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PCT/JP2010/057678
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English (en)
French (fr)
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WO2010126132A2 (ja
Inventor
敏之 五島
モーソー ウイン
栄花 許
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株式会社ピーアイ技術研究所
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Priority to US13/266,925 priority Critical patent/US8779085B2/en
Priority to CN201080029680.XA priority patent/CN102459417B/zh
Priority to KR1020117028278A priority patent/KR101679356B1/ko
Priority to EP10769830A priority patent/EP2431400A4/en
Publication of WO2010126132A2 publication Critical patent/WO2010126132A2/ja
Publication of WO2010126132A3 publication Critical patent/WO2010126132A3/ja

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/36—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino acids, polyamines and polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1035—Preparatory processes from tetracarboxylic acids or derivatives and diisocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/34—Carboxylic acids; Esters thereof with monohydroxyl compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/44—Polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1042—Copolyimides derived from at least two different tetracarboxylic compounds or two different diamino compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1075—Partially aromatic polyimides
    • C08G73/1078—Partially aromatic polyimides wholly aromatic in the diamino moiety
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/016—Flame-proofing or flame-retarding additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
    • C08L79/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C08L79/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D179/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen, with or without oxygen, or carbon only, not provided for in groups C09D161/00 - C09D177/00
    • C09D179/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C09D179/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00—Apparatus or processes for manufacturing printed circuits
    • H05K3/22—Secondary treatment of printed circuits
    • H05K3/28—Applying non-metallic protective coatings
    • H05K3/285—Permanent coating compositions
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2379/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen, or carbon only, not provided for in groups C08J2361/00 - C08J2377/00
    • C08J2379/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C08J2379/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K2201/00—Indexing scheme relating to printed circuits covered by H05K1/00
    • H05K2201/01—Dielectrics
    • H05K2201/0137—Materials
    • H05K2201/0154—Polyimide

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Non-Metallic Protective Coatings For Printed Circuits (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

　電気的特性、密着性が優れ、更に耐熱性、柔軟性、屈曲性、低そり性、耐薬品性、保存安定性の優れた、ポリカーボネートを含んだ変性ポリイミドの製造方法及び該変性ポリイミド、並びに該変性ポリイミドを含む組成物及びその用途が開示されている。柔軟性に優れたポリカーボネート部分を含むイソシアネート末端オリゴマーとテトラカルボン酸二無水物とを反応させてポリカーボネート部分を含むテトラカルボン酸二無水物オリゴマーを合成し、次いで、このオリゴマーをさらに芳香族ジアミン及び芳香族テトラカルボン酸二無水物と反応させてポリイミドブロックコポリマーとする方法によれば、芳香族ジアミンの選択の幅が広く、芳香族ジアミンを適切に選択することにより、上記した各種特性を同時に満足する優れた変性ポリイミドを作出することが可能である。
PCT/JP2010/057678 2009-04-30 2010-04-30 変性ポリイミドの製造方法及び変性ポリイミド WO2010126132A2 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
US13/266,925 US8779085B2 (en) 2009-04-30 2010-04-30 Modified polyimide and method for producing modified polyimide
CN201080029680.XA CN102459417B (zh) 2009-04-30 2010-04-30 改性聚酰亚胺的制备方法及改性聚酰亚胺
KR1020117028278A KR101679356B1 (ko) 2009-04-30 2010-04-30 변성 폴리이미드의 제조 방법 및 변성 폴리이미드
EP10769830A EP2431400A4 (en) 2009-04-30 2010-04-30 MODIFIED POLYIMIDE AND METHOD FOR PRODUCING THE SAME

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2009-110914 2009-04-30
JP2009110914A JP5755401B2 (ja) 2009-04-30 2009-04-30 変性ポリイミドの製造方法及び変性ポリイミド

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WO2010126132A2 WO2010126132A2 (ja) 2010-11-04
WO2010126132A3 true WO2010126132A3 (ja) 2010-12-23

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PCT/JP2010/057678 WO2010126132A2 (ja) 2009-04-30 2010-04-30 変性ポリイミドの製造方法及び変性ポリイミド

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US (1) US8779085B2 (ja)
EP (1) EP2431400A4 (ja)
JP (1) JP5755401B2 (ja)
KR (1) KR101679356B1 (ja)
CN (1) CN102459417B (ja)
WO (1) WO2010126132A2 (ja)

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JP5515394B2 (ja) * 2009-04-30 2014-06-11 株式会社ピーアイ技術研究所 感光性変性ポリイミド樹脂組成物及びその用途
JP5477327B2 (ja) * 2011-04-08 2014-04-23 日立金属株式会社 ポリイミド樹脂の製造方法
JP2013191356A (ja) * 2012-03-13 2013-09-26 Hitachi Cable Ltd 絶縁電線及びそれを用いて形成されたコイル
CN103547059A (zh) * 2012-07-17 2014-01-29 昆山雅森电子材料科技有限公司 软性印刷电路板
CN106471065B (zh) * 2014-05-24 2018-12-04 株式会社钟化 烷氧基硅烷改性聚酰胺酸溶液、层积体及柔性器件、聚酰亚胺薄及层积体的制造方法
TWI548315B (zh) * 2015-07-31 2016-09-01 臻鼎科技股份有限公司 電路基板及其製作方法、電路板和電子裝置
CN112940253A (zh) * 2015-09-24 2021-06-11 旭化成株式会社 聚酰亚胺前体、树脂组合物和树脂薄膜的制造方法
US20200045833A1 (en) * 2016-04-19 2020-02-06 Kaneka Corporation Printed wiring board and method for manufacturing same
JP6062097B1 (ja) * 2016-07-07 2017-01-18 第一工業製薬株式会社 ポリイミド水分散体の製造方法
CN107474250B (zh) * 2017-09-22 2020-07-03 长春理工大学 一种可多次熔体加工的酰亚胺材料及其制备方法
JPWO2019220968A1 (ja) * 2018-05-17 2021-05-27 三菱瓦斯化学株式会社 ポリイミド樹脂組成物
CN109762166B (zh) * 2018-12-26 2021-02-12 哈尔滨工程大学 一种聚酰亚胺前驱体及聚酰亚胺薄膜的制备方法

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JP2005036025A (ja) * 2003-07-15 2005-02-10 Hitachi Chem Co Ltd ポリイミド樹脂組成物、それを用いた被膜形成材料、および電子部品
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WO2010010831A1 (ja) * 2008-07-22 2010-01-28 株式会社カネカ 新規なポリイミド前駆体組成物及びその利用

Also Published As

Publication number Publication date
JP5755401B2 (ja) 2015-07-29
EP2431400A4 (en) 2013-01-09
CN102459417A (zh) 2012-05-16
US20120097439A1 (en) 2012-04-26
KR20120023024A (ko) 2012-03-12
WO2010126132A2 (ja) 2010-11-04
EP2431400A2 (en) 2012-03-21
US8779085B2 (en) 2014-07-15
CN102459417B (zh) 2014-01-29
KR101679356B1 (ko) 2016-11-24
JP2010260906A (ja) 2010-11-18

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