WO2007039310A1 - Crucible for the crystallization of silicon and process for making the same - Google Patents

Crucible for the crystallization of silicon and process for making the same Download PDF

Info

Publication number
WO2007039310A1
WO2007039310A1 PCT/EP2006/009671 EP2006009671W WO2007039310A1 WO 2007039310 A1 WO2007039310 A1 WO 2007039310A1 EP 2006009671 W EP2006009671 W EP 2006009671W WO 2007039310 A1 WO2007039310 A1 WO 2007039310A1
Authority
WO
WIPO (PCT)
Prior art keywords
crucible
silicon
silicon nitride
coating
protective coating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/009671
Other languages
English (en)
French (fr)
Inventor
Gilbert Rancoule
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vesuvius Crucible Co
Original Assignee
Vesuvius Crucible Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to US12/089,147 priority Critical patent/US8298333B2/en
Priority to BRPI0616485-4A priority patent/BRPI0616485A2/pt
Priority to CN2006800369429A priority patent/CN101278078B/zh
Priority to CA2624887A priority patent/CA2624887C/en
Priority to PL06806079T priority patent/PL1954856T3/pl
Priority to DE602006008498T priority patent/DE602006008498D1/de
Priority to AT06806079T priority patent/ATE439461T1/de
Priority to EP06806079A priority patent/EP1954856B1/en
Application filed by Vesuvius Crucible Co filed Critical Vesuvius Crucible Co
Priority to AU2006298957A priority patent/AU2006298957B2/en
Priority to JP2008533944A priority patent/JP4917607B2/ja
Publication of WO2007039310A1 publication Critical patent/WO2007039310A1/en
Anticipated expiration legal-status Critical
Priority to NO20082102A priority patent/NO20082102L/no
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/6303Inorganic additives
    • C04B35/6316Binders based on silicon compounds
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/58Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
    • C04B35/584Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62625Wet mixtures
    • C04B35/6264Mixing media, e.g. organic solvents
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5053Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials non-oxide ceramics
    • C04B41/5062Borides, Nitrides or Silicides
    • C04B41/5066Silicon nitride
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/87Ceramics
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C30B11/002Crucibles or containers for supporting the melt
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/10Crucibles or containers for supporting the melt
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details specially adapted for crucible or pot furnaces
    • F27B14/10Crucibles
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/38Non-oxide ceramic constituents or additives
    • C04B2235/3852Nitrides, e.g. oxynitrides, carbonitrides, oxycarbonitrides, lithium nitride, magnesium nitride
    • C04B2235/3873Silicon nitrides, e.g. silicon carbonitride, silicon oxynitride
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/48Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
    • C04B2235/483Si-containing organic compounds, e.g. silicone resins, (poly)silanes, (poly)siloxanes or (poly)silazanes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5445Particle size related information expressed by the size of the particles or aggregates thereof submicron sized, i.e. from 0,1 to 1 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/80Phases present in the sintered or melt-cast ceramic products other than the main phase

Definitions

  • a binder that creates a bond at a temperature lower than the temperature required to oxidise the silicon nitride.
  • the bond is created at a temperature lower than 800 0 C and more preferably lower than 500 0 C.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Silicon Compounds (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)
  • Ceramic Products (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Glass Compositions (AREA)
  • Optical Elements Other Than Lenses (AREA)
PCT/EP2006/009671 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same Ceased WO2007039310A1 (en)

Priority Applications (11)

Application Number Priority Date Filing Date Title
AT06806079T ATE439461T1 (de) 2005-10-06 2006-10-06 Tiegel zur kristallisation von silicium und herstellungsverfahren dafür
CN2006800369429A CN101278078B (zh) 2005-10-06 2006-10-06 用于硅结晶的坩埚及其制造方法
CA2624887A CA2624887C (en) 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same
PL06806079T PL1954856T3 (pl) 2005-10-06 2006-10-06 Tygiel do krystalizacji krzemu i sposób jego wytwarzania
DE602006008498T DE602006008498D1 (de) 2005-10-06 2006-10-06 Tiegel zur kristallisation von silicium und herstellungsverfahren dafür
US12/089,147 US8298333B2 (en) 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same
JP2008533944A JP4917607B2 (ja) 2005-10-06 2006-10-06 ケイ素の結晶化用の坩堝およびその製造方法
EP06806079A EP1954856B1 (en) 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same
AU2006298957A AU2006298957B2 (en) 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same
BRPI0616485-4A BRPI0616485A2 (pt) 2005-10-06 2006-10-06 cadinho para a cristalizaÇço de silÍcio, e, processo para a preparaÇço do mesmo
NO20082102A NO20082102L (no) 2005-10-06 2008-05-05 Smeltedigel for krystallisering av silisium og fremgangsmate for fremstilling av digelen

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP05447224 2005-10-06
EP05447224.6 2005-10-06

Publications (1)

Publication Number Publication Date
WO2007039310A1 true WO2007039310A1 (en) 2007-04-12

Family

ID=35735284

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/009671 Ceased WO2007039310A1 (en) 2005-10-06 2006-10-06 Crucible for the crystallization of silicon and process for making the same

Country Status (18)

Country Link
US (1) US8298333B2 (https=)
EP (1) EP1954856B1 (https=)
JP (1) JP4917607B2 (https=)
KR (1) KR101212924B1 (https=)
CN (1) CN101278078B (https=)
AT (1) ATE439461T1 (https=)
AU (1) AU2006298957B2 (https=)
BR (1) BRPI0616485A2 (https=)
CA (1) CA2624887C (https=)
DE (1) DE602006008498D1 (https=)
ES (1) ES2327570T3 (https=)
NO (1) NO20082102L (https=)
PL (1) PL1954856T3 (https=)
RU (1) RU2401889C2 (https=)
TW (1) TWI400369B (https=)
UA (1) UA89284C2 (https=)
WO (1) WO2007039310A1 (https=)
ZA (1) ZA200803754B (https=)

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008131841A1 (de) * 2007-04-25 2008-11-06 Esk Ceramics Gmbh & Co. Kg Formkörper mit einer dauerhaften siliciumnitridhaltigen hartbeschichtung, verfahren zu dessen herstellung und dessen verwendung
EP1990593A1 (en) * 2007-04-30 2008-11-12 General Electric Company Crucibles For Melting Titanium Alloys
EP2058289A1 (de) 2007-11-08 2009-05-13 ESK Ceramics GmbH & Co.KG Fest haftende siliciumnitridhaltige Trennschicht
DE102008031766A1 (de) 2008-07-04 2009-10-15 Schott Ag Verfahren zur Herstellung eines beschichteten Tiegels aus einem Tiegelgrünkörper oder aus einem zwischengebrannten Tiegelkörper sowie die Verwendung solch eines beschichteten Tiegels
RU2384410C1 (ru) * 2008-12-11 2010-03-20 Открытое акционерное общество Научно-производственное объединение "Искра" Способ подготовки к работе формообразующей оправки
CN101798236A (zh) * 2009-04-30 2010-08-11 山东圣川陶瓷材料有限公司 干法水泥回转窑预热器用陶瓷内筒
CN101870592A (zh) * 2010-06-30 2010-10-27 武汉理工大学 镀氮化钛碳化硅纤维的制备方法
US7833490B2 (en) 2006-01-12 2010-11-16 Vesuvius Crucible Company Crucible for the treatment of molten silicon
WO2012025905A1 (fr) * 2010-08-27 2012-03-01 Commissariat A L'energie Atomique Et Aux Energies Alternatives Creuset pour la solidification de lingot de silicium
US8236232B2 (en) 2007-04-30 2012-08-07 General Electric Company Methods for making reinforced refractory crucibles for melting titanium alloys
WO2013029920A1 (de) 2011-08-31 2013-03-07 Esk Ceramics Gmbh & Co. Kg Siliziumnitridhaltige trennschicht hoher härte
US20130068925A1 (en) * 2011-09-20 2013-03-21 Chung-Hou Tony Hsiao Photovoltaic Ingot Mold Release
WO2014004496A1 (en) * 2012-06-25 2014-01-03 Silicor Materials Inc. Lining for surfaces of a refractory crucible for purification of silicon and method of purification of the silicon melt using that crucible (s) for melting and further directional solidification
DE102013206993A1 (de) 2013-04-18 2014-10-23 Morgan Advanced Materials Haldenwanger GmbH Verfahren zum zumindest bereichsweisen Aufbringen einer Siliciumnitridschutzschicht auf Formkörpern aus Quarzgut
EP2660200A4 (en) * 2010-12-28 2014-10-29 Ube Industries POLYCRYSTALLINE SILICON INJECTION MOLDING AND MANUFACTURING METHOD THEREFOR, SILICON-NITRIDE POWDER FOR MOLDING MATERIAL FOR POLYCRYSTALLINE SILICON INJECTION MOLDING AND SUSPENSION THEREWITH
EP2660201A4 (en) * 2010-12-28 2014-11-05 Ube Industries POLYCRYSTALLINE SILICON INJECTION MOLDING AND MANUFACTURING METHOD THEREFOR, SILICON-NITRIDE POWDER FOR MOLDING MATERIAL FOR POLYCRYSTALLINE SILICON INJECTION MOLDING AND SUSPENSION THEREWITH
EP1780307B1 (de) * 2005-10-21 2015-01-14 ESK Ceramics GmbH & Co.KG Dauerhafte siliciumnitridhaltige Hartbeschichtung
US10023972B2 (en) 2013-09-16 2018-07-17 Commissariat à l'Energie Atomique et aux Energies Alternatives Substrate for solidifying a silicon ingot
WO2019211379A1 (de) * 2018-05-04 2019-11-07 Alzchem Trostberg Gmbh Tiegel zur herstellung von multikristallinem silicium mittels gerichteter erstarrung, verfahren zu dessen herstellung und dessen verwendung, sowie verfahren zur herstellung von multikristallinem silicium mittels gerichteter erstarrung

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE1017674A3 (fr) * 2007-07-05 2009-03-03 Fib Services Internat Composition de traitement de chambre a parois refractaires et son procede de mise en oeuvre.
CN101433890B (zh) * 2008-12-05 2010-12-29 江阴海润太阳能电力有限公司 低压下在石英坩埚内壁上喷涂氮化硅涂层的方法及装置
CN101775639B (zh) * 2009-01-08 2012-05-30 常熟华融太阳能新型材料有限公司 用于多晶硅结晶炉炉壁保护的内衬及其制造方法
CN101508590B (zh) * 2009-03-20 2012-07-04 江西赛维Ldk太阳能高科技有限公司 一种多晶硅铸锭用坩埚涂层以及制备方法
WO2011009062A2 (en) * 2009-07-16 2011-01-20 Memc Singapore Pte, Ltd. Coated crucibles and methods for preparing and use thereof
JP5518584B2 (ja) * 2010-06-16 2014-06-11 電気化学工業株式会社 離型剤用窒化珪素粉末。
JP5788891B2 (ja) * 2010-10-08 2015-10-07 Jx日鉱日石金属株式会社 シリコンインゴット製造用容器
WO2012092369A2 (en) * 2010-12-30 2012-07-05 Saint-Gobain Ceramics & Plastics, Inc. Crucible body and method of forming same
US20130239882A1 (en) * 2011-09-09 2013-09-19 Robert Billings Bramhall, JR. Coated crucible and method of making a coated crucible
CN102358953B (zh) * 2011-09-28 2015-12-09 江西赛维Ldk太阳能高科技有限公司 一种减少粘埚的坩埚及其制备方法
US8858697B2 (en) 2011-10-28 2014-10-14 General Electric Company Mold compositions
CN103130528B (zh) * 2011-12-05 2014-06-11 江苏协鑫硅材料科技发展有限公司 多晶硅铸锭用的免烧结坩埚涂层结构及其制备方法
US9011205B2 (en) 2012-02-15 2015-04-21 General Electric Company Titanium aluminide article with improved surface finish
US8932518B2 (en) 2012-02-29 2015-01-13 General Electric Company Mold and facecoat compositions
CN103360077B (zh) * 2012-04-01 2014-12-24 浙江昱辉阳光能源有限公司 一种氮化硅坩埚及其制备方法
JP5901448B2 (ja) * 2012-06-28 2016-04-13 デンカ株式会社 離型剤用窒化ケイ素粉末
US8906292B2 (en) 2012-07-27 2014-12-09 General Electric Company Crucible and facecoat compositions
US8708033B2 (en) 2012-08-29 2014-04-29 General Electric Company Calcium titanate containing mold compositions and methods for casting titanium and titanium aluminide alloys
US8992824B2 (en) 2012-12-04 2015-03-31 General Electric Company Crucible and extrinsic facecoat compositions
US9592548B2 (en) 2013-01-29 2017-03-14 General Electric Company Calcium hexaluminate-containing mold and facecoat compositions and methods for casting titanium and titanium aluminide alloys
CN103243392A (zh) * 2013-05-09 2013-08-14 天津英利新能源有限公司 多晶硅铸锭炉与制备均匀细小晶粒多晶硅铸锭的方法
CN103526290A (zh) * 2013-10-24 2014-01-22 阿特斯(中国)投资有限公司 多晶硅铸锭的制备方法
US9511417B2 (en) 2013-11-26 2016-12-06 General Electric Company Silicon carbide-containing mold and facecoat compositions and methods for casting titanium and titanium aluminide alloys
US9192983B2 (en) 2013-11-26 2015-11-24 General Electric Company Silicon carbide-containing mold and facecoat compositions and methods for casting titanium and titanium aluminide alloys
US10391547B2 (en) 2014-06-04 2019-08-27 General Electric Company Casting mold of grading with silicon carbide
TWI663126B (zh) 2014-07-09 2019-06-21 法商維蘇威法國公司 包含可磨塗層之輥、其製造方法及其用途
CN104140759B (zh) * 2014-07-17 2016-08-24 宁波晶元太阳能有限公司 多晶硅铸锭用石英坩埚底部引晶涂层的制备方法
CN105063757B (zh) * 2015-09-17 2017-12-29 晶科能源有限公司 一种低氧喷涂方法
CN105603374B (zh) * 2016-02-19 2018-06-12 中科院微电子研究所昆山分所 一种在多晶硅铸锭坩埚上制备Si3N4薄膜的方法
KR102571434B1 (ko) * 2016-12-28 2023-08-29 오씨아이 주식회사 실리카 도가니 내벽에 질화규소를 코팅하는 방법
CN107162001A (zh) * 2017-06-20 2017-09-15 晋能清洁能源光伏工程有限责任公司 一种多晶硅分凝铸造方法及分凝装置
CN107876362B (zh) * 2017-11-10 2021-03-23 江苏协鑫硅材料科技发展有限公司 大尺寸铸锭用坩埚涂层的自动喷涂工艺及坩埚
CN109750351A (zh) * 2018-05-31 2019-05-14 河北高富氮化硅材料有限公司 一种多晶硅铸锭用高效Si3N4粉
CN109704782B (zh) * 2019-01-30 2021-12-14 中国科学院理化技术研究所 一种用于光伏多晶硅生产的Si2N2O陶瓷粉体的制备方法
US12545623B2 (en) * 2019-04-17 2026-02-10 Materion Corporation Crucibles and compositions and processes for making same
CN114477781B (zh) * 2020-10-23 2024-05-24 中国科学院理化技术研究所 一种复合陶瓷涂层脱模剂的制备工艺
KR102407043B1 (ko) * 2022-03-04 2022-06-10 주식회사 에스티아이 탄화규소 분말의 합성방법

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4218418A (en) * 1978-06-22 1980-08-19 Crystal Systems, Inc. Processes of casting an ingot and making a silica container
US4741925A (en) * 1987-09-14 1988-05-03 Gte Products Corporation Method of forming silicon nitride coating
US6165425A (en) * 1997-02-06 2000-12-26 Bayer Aktiengesellschaft Melting pot with silicon protective layers, method for applying said layer and the use thereof
WO2004053207A1 (en) * 2002-12-06 2004-06-24 Vesuvius France S.A. Vessel for holding silicon and method of producing the same

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5283124A (en) 1990-03-02 1994-02-01 Kansai Paint Co., Ltd. Coating resin composition
RU2036983C1 (ru) * 1991-06-03 1995-06-09 Государственный научно-исследовательский и проектный институт редкометаллической промышленности "Гиредмет" Покрытие графитового тигля
US6479108B2 (en) * 2000-11-15 2002-11-12 G.T. Equipment Technologies, Inc. Protective layer for quartz crucibles used for silicon crystallization
ATE398196T1 (de) 2004-04-29 2008-07-15 Vesuvius Crucible Co Tiegel für die kristallisation von silicium
EP1739209A1 (en) 2005-07-01 2007-01-03 Vesuvius Crucible Company Crucible for the crystallization of silicon
EP1811064A1 (fr) * 2006-01-12 2007-07-25 Vesuvius Crucible Company Creuset pour le traitement de silicium à l'état fondu

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4218418A (en) * 1978-06-22 1980-08-19 Crystal Systems, Inc. Processes of casting an ingot and making a silica container
US4741925A (en) * 1987-09-14 1988-05-03 Gte Products Corporation Method of forming silicon nitride coating
US6165425A (en) * 1997-02-06 2000-12-26 Bayer Aktiengesellschaft Melting pot with silicon protective layers, method for applying said layer and the use thereof
WO2004053207A1 (en) * 2002-12-06 2004-06-24 Vesuvius France S.A. Vessel for holding silicon and method of producing the same

Cited By (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1780307B1 (de) * 2005-10-21 2015-01-14 ESK Ceramics GmbH & Co.KG Dauerhafte siliciumnitridhaltige Hartbeschichtung
US7833490B2 (en) 2006-01-12 2010-11-16 Vesuvius Crucible Company Crucible for the treatment of molten silicon
WO2008131841A1 (de) * 2007-04-25 2008-11-06 Esk Ceramics Gmbh & Co. Kg Formkörper mit einer dauerhaften siliciumnitridhaltigen hartbeschichtung, verfahren zu dessen herstellung und dessen verwendung
EP1985594B1 (de) * 2007-04-25 2011-10-12 ESK Ceramics GmbH & Co.KG Formkörper mit einer dauerhaften siliciumnitridhaltigen Hartbeschichtung, Verfahren zu dessen Herstellung und dessen Verwendung
US8236232B2 (en) 2007-04-30 2012-08-07 General Electric Company Methods for making reinforced refractory crucibles for melting titanium alloys
EP1990593A1 (en) * 2007-04-30 2008-11-12 General Electric Company Crucibles For Melting Titanium Alloys
EP2058289A1 (de) 2007-11-08 2009-05-13 ESK Ceramics GmbH & Co.KG Fest haftende siliciumnitridhaltige Trennschicht
KR101307478B1 (ko) * 2007-11-08 2013-09-11 이에스케이 세라믹스 게엠베하 운트 코. 카게 질화규소를 포함하는 견고하게 부착된 분리층
WO2009059756A1 (de) * 2007-11-08 2009-05-14 Esk Ceramics Gmbh & Co. Kg Fest haftende siliciumnitridhaltige trennschicht
JP2011507981A (ja) * 2007-11-08 2011-03-10 イーエスケイ セラミクス ゲーエムベーハー アンド カンパニー カーゲー 強固に接着する窒化ケイ素含有剥離層
TWI461492B (zh) * 2007-11-08 2014-11-21 Esk Ceramics Gmbh & Co Kg 含四氮化三矽的膠粘劑、成型體、成型體的製造方法以及成型體的用途
US8231705B2 (en) 2007-11-08 2012-07-31 Esk Ceramics Gmbh & Co. Kg Firmly adhering silicon nitride-containing release layer
DE102007053284A1 (de) 2007-11-08 2009-05-20 Esk Ceramics Gmbh & Co. Kg Fest haftende siliciumnitridhaltige Trennschicht
DE102008031766A1 (de) 2008-07-04 2009-10-15 Schott Ag Verfahren zur Herstellung eines beschichteten Tiegels aus einem Tiegelgrünkörper oder aus einem zwischengebrannten Tiegelkörper sowie die Verwendung solch eines beschichteten Tiegels
RU2384410C1 (ru) * 2008-12-11 2010-03-20 Открытое акционерное общество Научно-производственное объединение "Искра" Способ подготовки к работе формообразующей оправки
CN101798236A (zh) * 2009-04-30 2010-08-11 山东圣川陶瓷材料有限公司 干法水泥回转窑预热器用陶瓷内筒
CN101870592A (zh) * 2010-06-30 2010-10-27 武汉理工大学 镀氮化钛碳化硅纤维的制备方法
FR2964117A1 (fr) * 2010-08-27 2012-03-02 Commissariat Energie Atomique Creuset pour la solidification de lingot de silicium
WO2012025905A1 (fr) * 2010-08-27 2012-03-01 Commissariat A L'energie Atomique Et Aux Energies Alternatives Creuset pour la solidification de lingot de silicium
US8973888B2 (en) 2010-12-28 2015-03-10 Ube Industries, Ltd. Polycrystalline silicon ingot casting mold and method for producing same, and silicon nitride powder for mold release material for polycrystalline silicon ingot casting mold and slurry containing same
EP2660200A4 (en) * 2010-12-28 2014-10-29 Ube Industries POLYCRYSTALLINE SILICON INJECTION MOLDING AND MANUFACTURING METHOD THEREFOR, SILICON-NITRIDE POWDER FOR MOLDING MATERIAL FOR POLYCRYSTALLINE SILICON INJECTION MOLDING AND SUSPENSION THEREWITH
EP2660201A4 (en) * 2010-12-28 2014-11-05 Ube Industries POLYCRYSTALLINE SILICON INJECTION MOLDING AND MANUFACTURING METHOD THEREFOR, SILICON-NITRIDE POWDER FOR MOLDING MATERIAL FOR POLYCRYSTALLINE SILICON INJECTION MOLDING AND SUSPENSION THEREWITH
US9022343B2 (en) 2010-12-28 2015-05-05 Ube Industries, Ltd. Polycrystalline silicon ingot casting mold and method for producing same, and silicon nitride powder for mold release material for polycrystalline silicon ingot casting mold and slurry containing same
WO2013029920A1 (de) 2011-08-31 2013-03-07 Esk Ceramics Gmbh & Co. Kg Siliziumnitridhaltige trennschicht hoher härte
US9625213B2 (en) 2011-08-31 2017-04-18 3M Innovative Properties Company Silicon-nitride-containing separating layer having high hardness
US8747538B2 (en) * 2011-09-20 2014-06-10 Chung-Hou Tony Hsiao Photovoltaic ingot mold release
US20130068925A1 (en) * 2011-09-20 2013-03-21 Chung-Hou Tony Hsiao Photovoltaic Ingot Mold Release
KR101697027B1 (ko) 2012-06-25 2017-01-16 실리코르 머티리얼즈 인코포레이티드 실리콘 용융물의 정제용 내화 도가니의 표면용 라이닝 및 용융 및 추가적인 방향성 고체화를 위하여 상기 도가니(들)를 이용하는 실리콘 용융물의 정제 방법
KR20150022997A (ko) * 2012-06-25 2015-03-04 실리코르 머티리얼즈 인코포레이티드 실리콘 용융물의 정제용 내화 도가니의 표면용 라이닝 및 용융 및 추가적인 방향성 고체화를 위하여 상기 도가니(들)를 이용하는 실리콘 용융물의 정제 방법
WO2014004496A1 (en) * 2012-06-25 2014-01-03 Silicor Materials Inc. Lining for surfaces of a refractory crucible for purification of silicon and method of purification of the silicon melt using that crucible (s) for melting and further directional solidification
DE102013206993A1 (de) 2013-04-18 2014-10-23 Morgan Advanced Materials Haldenwanger GmbH Verfahren zum zumindest bereichsweisen Aufbringen einer Siliciumnitridschutzschicht auf Formkörpern aus Quarzgut
US10023972B2 (en) 2013-09-16 2018-07-17 Commissariat à l'Energie Atomique et aux Energies Alternatives Substrate for solidifying a silicon ingot
WO2019211379A1 (de) * 2018-05-04 2019-11-07 Alzchem Trostberg Gmbh Tiegel zur herstellung von multikristallinem silicium mittels gerichteter erstarrung, verfahren zu dessen herstellung und dessen verwendung, sowie verfahren zur herstellung von multikristallinem silicium mittels gerichteter erstarrung

Also Published As

Publication number Publication date
TW200720496A (en) 2007-06-01
KR101212924B1 (ko) 2012-12-14
AU2006298957B2 (en) 2010-06-03
EP1954856B1 (en) 2009-08-12
UA89284C2 (ru) 2010-01-11
RU2008117093A (ru) 2009-11-20
CA2624887C (en) 2013-07-09
CN101278078B (zh) 2011-01-19
ATE439461T1 (de) 2009-08-15
AU2006298957A1 (en) 2007-04-12
US8298333B2 (en) 2012-10-30
DE602006008498D1 (de) 2009-09-24
NO20082102L (no) 2008-05-05
KR20080051144A (ko) 2008-06-10
ES2327570T3 (es) 2009-10-30
CA2624887A1 (en) 2007-04-12
ZA200803754B (en) 2009-09-30
EP1954856A1 (en) 2008-08-13
RU2401889C2 (ru) 2010-10-20
PL1954856T3 (pl) 2010-01-29
JP4917607B2 (ja) 2012-04-18
BRPI0616485A2 (pt) 2012-12-25
CN101278078A (zh) 2008-10-01
JP2009510387A (ja) 2009-03-12
US20080260608A1 (en) 2008-10-23
TWI400369B (zh) 2013-07-01

Similar Documents

Publication Publication Date Title
CA2624887C (en) Crucible for the crystallization of silicon and process for making the same
AU2006265391B2 (en) Crucible for the crystallization of silicon
CN1946881B (zh) 用于硅结晶的坩埚
JP5209195B2 (ja) 窒化ケイ素を含有する耐久性ハードコーティング
CN102884024B (zh) 用于光伏领域的坩埚
WO2012092369A2 (en) Crucible body and method of forming same
CN101370968A (zh) 处理熔融硅的坩埚
CN101357393A (zh) 硅脱模涂层、其制备方法及其使用方法
CN115448731A (zh) 一种钒氮合金用石墨坩埚涂层的制备方法
CN117480142A (zh) 耐火构件及其制造方法
US20070086937A1 (en) Use of a silicon carbide-based ceramic material in aggressive environments
JP2025518243A (ja) 炭素汚染を低減した単結晶シリコンインゴットの形成方法およびそのような方法で使用するサセプタ
JP3612187B2 (ja) ルツボ用サセプタ
JP2011067839A (ja) 珪素鋳造用離型剤の調製方法及び珪素鋳造用鋳型の製造方法

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200680036942.9

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application
WWE Wipo information: entry into national phase

Ref document number: 2006298957

Country of ref document: AU

WWE Wipo information: entry into national phase

Ref document number: 1020087007304

Country of ref document: KR

WWE Wipo information: entry into national phase

Ref document number: 2006806079

Country of ref document: EP

ENP Entry into the national phase

Ref document number: 2006298957

Country of ref document: AU

Date of ref document: 20061006

Kind code of ref document: A

WWE Wipo information: entry into national phase

Ref document number: 12089147

Country of ref document: US

WWP Wipo information: published in national office

Ref document number: 2006298957

Country of ref document: AU

WWE Wipo information: entry into national phase

Ref document number: 2624887

Country of ref document: CA

Ref document number: 2008533944

Country of ref document: JP

Ref document number: MX/a/2008/004523

Country of ref document: MX

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 3118/DELNP/2008

Country of ref document: IN

WWE Wipo information: entry into national phase

Ref document number: 2008117093

Country of ref document: RU

WWP Wipo information: published in national office

Ref document number: 2006806079

Country of ref document: EP

ENP Entry into the national phase

Ref document number: PI0616485

Country of ref document: BR

Kind code of ref document: A2

Effective date: 20080331