WO2000040773A3 - Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung - Google Patents

Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung Download PDF

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Publication number
WO2000040773A3
WO2000040773A3 PCT/EP1999/010368 EP9910368W WO0040773A3 WO 2000040773 A3 WO2000040773 A3 WO 2000040773A3 EP 9910368 W EP9910368 W EP 9910368W WO 0040773 A3 WO0040773 A3 WO 0040773A3
Authority
WO
WIPO (PCT)
Prior art keywords
heat exchanger
relates
metal
producing same
reduced tendency
Prior art date
Application number
PCT/EP1999/010368
Other languages
English (en)
French (fr)
Other versions
WO2000040773A2 (de
Inventor
Stephan Hueffer
Axel Franke
Stephan Scholl
Hans Mueller-Steinhagen
Qi Zhao
Bernd Diebold
Peter Dillmann
Original Assignee
Basf Ag
Stephan Hueffer
Axel Franke
Stephan Scholl
Mueller Steinhagen Hans
Qi Zhao
Bernd Diebold
Peter Dillmann
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag, Stephan Hueffer, Axel Franke, Stephan Scholl, Mueller Steinhagen Hans, Qi Zhao, Bernd Diebold, Peter Dillmann filed Critical Basf Ag
Priority to EP99964672A priority Critical patent/EP1144724B1/de
Priority to DE59903362T priority patent/DE59903362D1/de
Priority to KR1020017008321A priority patent/KR20010103724A/ko
Priority to JP2000592465A priority patent/JP2002534605A/ja
Priority to CA002358097A priority patent/CA2358097A1/en
Priority to US09/869,275 priority patent/US6513581B1/en
Priority to AT99964672T priority patent/ATE227360T1/de
Publication of WO2000040773A2 publication Critical patent/WO2000040773A2/de
Publication of WO2000040773A3 publication Critical patent/WO2000040773A3/de

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • F28F19/02Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • F28F19/02Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings
    • F28F19/06Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings of metal
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601Process or apparatus
    • C23C18/1603Process or apparatus coating on selected surface areas
    • C23C18/1614Process or apparatus coating on selected surface areas plating on one side
    • C23C18/1616Process or apparatus coating on selected surface areas plating on one side interior or inner surface
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601Process or apparatus
    • C23C18/1633Process of electroless plating
    • C23C18/1655Process features
    • C23C18/1662Use of incorporated material in the solution or dispersion, e.g. particles, whiskers, wires
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31Coating with metals
    • C23C18/32Coating with nickel, cobalt or mixtures thereof with phosphorus or boron
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31Coating with metals
    • C23C18/32Coating with nickel, cobalt or mixtures thereof with phosphorus or boron
    • C23C18/34Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents
    • C23C18/36Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents using hypophosphites
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31Coating with metals
    • C23C18/38Coating with copper
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F2245/00Coatings; Surface treatments
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12535Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.] with additional, spatially distinct nonmetal component
    • Y10T428/12556Organic component
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771Transition metal-base component
    • Y10T428/12861Group VIII or IB metal-base component
    • Y10T428/12944Ni-base component
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31678Of metal

Abstract

Ein Gegenstand der Erfindung ist ein Verfahren zur Herstellung eines Wärmeüberträgers, gekennzeichnet durch das stromlose chemische Abscheiden einer Metall-Polymer-Dispersionsschicht, bei der das Polymer halogeniert ist, auf einer Wärmeübertragungsoberfläche. Ein weiterer Gegenstand der Erfindung ist ein Verfahren zur Herstellung eines Wärmeüberträgers, dadurch gekennzeichnet, daß vor dem Aufbringen der Metall-Polymer-Dispersionsschicht eine 1 bis 15 νm dicke Metall-Phosphor-Schicht durch stromloses chemisches Abscheiden aufgebracht wird. Weitere Gegenstände der Erfindung sind ein Wämeübertrager, der durch ein erfindungsgemäßes Verfahren herstellbar ist und die Verwendung einer Beschichtung, hergestellt durch das stromlose chemische Abscheiden einer Metall-Polymer-Dispersionsschicht, bei der das Polymer halogeniert ist, zur Verringerung der Neigung der beschichteten Flächen, Feststoffe aus Fluiden unter Bildung von Ablagerungen anzulagern.
PCT/EP1999/010368 1998-12-30 1999-12-24 Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung WO2000040773A2 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
EP99964672A EP1144724B1 (de) 1998-12-30 1999-12-24 Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung
DE59903362T DE59903362D1 (de) 1998-12-30 1999-12-24 Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung
KR1020017008321A KR20010103724A (ko) 1998-12-30 1999-12-24 감소된 파울링 경향을 갖는 열전달 장치 및 그의 제조 방법
JP2000592465A JP2002534605A (ja) 1998-12-30 1999-12-24 付着汚染傾向の低い熱伝達装置およびこれらの製造
CA002358097A CA2358097A1 (en) 1998-12-30 1999-12-24 Heat exchanger with a reduced tendency to produce deposits and method for producing same
US09/869,275 US6513581B1 (en) 1998-12-30 1999-12-24 Heat exchanger with a reduced tendency to produce deposits and method for producing same
AT99964672T ATE227360T1 (de) 1998-12-30 1999-12-24 Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19860526A DE19860526A1 (de) 1998-12-30 1998-12-30 Wärmeüberträger mit verringerter Neigung, Ablagerungen zu bilden und Verfahren zu deren Herstellung
DE19860526.9 1998-12-30

Publications (2)

Publication Number Publication Date
WO2000040773A2 WO2000040773A2 (de) 2000-07-13
WO2000040773A3 true WO2000040773A3 (de) 2000-11-09

Family

ID=7892984

Family Applications (3)

Application Number Title Priority Date Filing Date
PCT/EP1999/010368 WO2000040773A2 (de) 1998-12-30 1999-12-24 Wärmeüberträger mit verringerter neigung, ablagerungen zu bilden und verfahren zu deren herstellung
PCT/EP1999/010371 WO2000040774A2 (de) 1998-12-30 1999-12-24 Verfahren zur beschichtung von apparaten und apparateteilen für den chemischen anlagenbau
PCT/EP1999/010372 WO2000040775A2 (de) 1998-12-30 1999-12-24 Verfahren zur beschichtung von reaktoren für die hochdruckpolymerisation von 1-olefinen

Family Applications After (2)

Application Number Title Priority Date Filing Date
PCT/EP1999/010371 WO2000040774A2 (de) 1998-12-30 1999-12-24 Verfahren zur beschichtung von apparaten und apparateteilen für den chemischen anlagenbau
PCT/EP1999/010372 WO2000040775A2 (de) 1998-12-30 1999-12-24 Verfahren zur beschichtung von reaktoren für die hochdruckpolymerisation von 1-olefinen

Country Status (10)

Country Link
US (3) US6509103B1 (de)
EP (3) EP1144724B1 (de)
JP (3) JP2003511551A (de)
KR (3) KR20010103724A (de)
CN (3) CN1636305A (de)
AT (3) ATE245210T1 (de)
CA (2) CA2358099A1 (de)
DE (4) DE19860526A1 (de)
ES (2) ES2204184T3 (de)
WO (3) WO2000040773A2 (de)

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WO2000040774A2 (de) 2000-07-13
EP1144723A2 (de) 2001-10-17
EP1144724B1 (de) 2002-11-06
ES2204184T3 (es) 2004-04-16
ATE227360T1 (de) 2002-11-15
EP1144723A3 (de) 2002-11-13
DE19860526A1 (de) 2000-07-06
WO2000040773A2 (de) 2000-07-13
JP2002534605A (ja) 2002-10-15
CN1332810A (zh) 2002-01-23
ATE245210T1 (de) 2003-08-15
US6513581B1 (en) 2003-02-04
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CN1636305A (zh) 2005-07-06
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DE59906313D1 (de) 2003-08-21
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