TW200618859A - Continuous production of crosslinked fine particles of addition-polymer gel - Google Patents
Continuous production of crosslinked fine particles of addition-polymer gelInfo
- Publication number
- TW200618859A TW200618859A TW094133757A TW94133757A TW200618859A TW 200618859 A TW200618859 A TW 200618859A TW 094133757 A TW094133757 A TW 094133757A TW 94133757 A TW94133757 A TW 94133757A TW 200618859 A TW200618859 A TW 200618859A
- Authority
- TW
- Taiwan
- Prior art keywords
- kneader
- fine particles
- continuous production
- addition
- polymer gel
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/01—Processes of polymerisation characterised by special features of the polymerisation apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/52—Amides or imides
- C08F220/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F220/56—Acrylamide; Methacrylamide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/008—Treatment of solid polymer wetted by water or organic solvents, e.g. coagulum, filter cakes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/06—Treatment of polymer solutions
- C08F6/10—Removal of volatile materials, e.g. solvents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/0061—Controlling the level
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Accessories For Mixers (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Macromonomer-Based Addition Polymer (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102004047528 | 2004-09-28 | ||
| DE102004051646 | 2004-10-22 | ||
| DE102005023325 | 2005-05-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW200618859A true TW200618859A (en) | 2006-06-16 |
Family
ID=35478620
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW094133757A TW200618859A (en) | 2004-09-28 | 2005-09-28 | Continuous production of crosslinked fine particles of addition-polymer gel |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20080004408A1 (https=) |
| EP (4) | EP1799721B1 (https=) |
| JP (2) | JP4560087B2 (https=) |
| CN (1) | CN101031591B (https=) |
| AT (1) | ATE534671T1 (https=) |
| TW (1) | TW200618859A (https=) |
| WO (1) | WO2006034806A1 (https=) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
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| ATE465188T1 (de) * | 2006-10-19 | 2010-05-15 | Basf Se | Verfahren zur herstellung von superabsorbern |
| BRPI0809157A2 (pt) * | 2007-03-23 | 2014-09-16 | Basf Se | Processos para transportar uma composição manomérica, e para preparar resinas que absorvem água. |
| JP5502749B2 (ja) * | 2007-12-17 | 2014-05-28 | ビーエーエスエフ ソシエタス・ヨーロピア | 吸水性ポリマー粒子の製造方法 |
| CN101959538A (zh) * | 2008-03-05 | 2011-01-26 | 巴斯夫欧洲公司 | 制备超吸收剂的方法 |
| US8148485B2 (en) | 2008-03-13 | 2012-04-03 | Nippon Shokubai Co., Ltd. | Production method for water-absorbing resin |
| WO2009115472A1 (de) * | 2008-03-20 | 2009-09-24 | Basf Se | Verfahren zur herstellung wasserabsorbierender polymerpartikel mit niedriger zentrifugenretentionskapazität |
| EP2275400B1 (en) | 2008-04-27 | 2017-01-11 | Nippon Shokubai Co., Ltd. | Process for producing acrylic acid, and process for producing hydrophilic resin and process for producing water absorptive resin using the process |
| US8404887B2 (en) | 2008-12-26 | 2013-03-26 | Nippon Shokubai Co., Ltd. | Process for producing acrylic acid |
| JP5718060B2 (ja) * | 2009-02-06 | 2015-05-13 | 株式会社日本触媒 | ポリアクリル酸(塩)系親水性樹脂およびその製造方法 |
| SG175379A1 (en) | 2009-05-15 | 2011-12-29 | Nippon Catalytic Chem Ind | Process for producing (meth)acrylic acid and crystallization system |
| JP5580813B2 (ja) | 2009-05-15 | 2014-08-27 | 株式会社日本触媒 | (メタ)アクリル酸の製造方法 |
| CN102428065B (zh) | 2009-05-15 | 2014-02-26 | 株式会社日本触媒 | 制备(甲基)丙烯酸的方法 |
| JP5731390B2 (ja) | 2009-09-30 | 2015-06-10 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂およびその製造方法 |
| WO2011042404A1 (de) * | 2009-10-09 | 2011-04-14 | Basf Se | Verwendung von heizdampfkondensat zur herstellung wasserabsorbierender polymerpartikel |
| WO2011099586A1 (ja) | 2010-02-10 | 2011-08-18 | 株式会社日本触媒 | 吸水性樹脂粉末の製造方法 |
| JP5632906B2 (ja) | 2010-03-12 | 2014-11-26 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US20130018161A1 (en) | 2010-03-31 | 2013-01-17 | Takayuki Ezawa | Catalyst for glycerin dehydration, and process for producing acrolein, process for producing acrylic acid, and process for producing hydrophilic resin each using the catalyst |
| US8524859B2 (en) | 2010-04-30 | 2013-09-03 | Exxonmobil Chemical Patents Inc. | Method for elastomer finishing |
| CN103153455A (zh) | 2010-09-30 | 2013-06-12 | 株式会社日本触媒 | 颗粒状吸水剂及其制造方法 |
| EP2660235A4 (en) | 2010-12-28 | 2016-01-20 | Nippon Catalytic Chem Ind | METHOD FOR THE PRODUCTION OF ACRYLIC ACID AND / OR ESTER THEREOF AND POLYMER FROM ACRYLIC ACID AND / OR ESTER THEREOF |
| US8653215B2 (en) | 2011-05-26 | 2014-02-18 | Basf Se | Process for producing water-absorbing polymer particles |
| EP2714103B1 (de) * | 2011-05-26 | 2019-08-21 | Basf Se | Verfahren zur kontinuierlichen herstellung wasserabsorbierender polymerpartikel |
| JP6253575B2 (ja) | 2011-05-26 | 2017-12-27 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 吸水性ポリマー粒子の製造法 |
| WO2012164081A1 (de) * | 2011-06-03 | 2012-12-06 | Basf Se | Verfahren zur kontinuierlichen herstellung wasserabsorbierender polymerpartikel |
| JP5551836B2 (ja) | 2011-11-16 | 2014-07-16 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂の製造方法 |
| KR20140145213A (ko) | 2012-05-07 | 2014-12-22 | 바스프 에스이 | 혼련 혼합기를 작동시키는 방법 |
| US9415529B2 (en) * | 2012-05-08 | 2016-08-16 | Basf Se | Method for operating an apparatus with at least one rotating shaft |
| CN104364269B (zh) | 2012-06-13 | 2016-10-12 | 巴斯夫欧洲公司 | 在装有至少两个轴向平行旋转轴的聚合反应器中制备吸水性聚合物颗粒的方法 |
| US9248429B2 (en) | 2012-06-13 | 2016-02-02 | Basf Se | Process for producing water-absorbing polymer particles in a polymerization reactor with at least two axially parallel rotating shafts |
| WO2014002886A1 (ja) | 2012-06-27 | 2014-01-03 | 株式会社日本触媒 | (メタ)アクリル酸の製造方法、及び、親水性樹脂の製造方法 |
| JP6096199B2 (ja) | 2012-08-27 | 2017-03-15 | 株式会社日本触媒 | 粒子状吸水剤及びその製造方法 |
| EP3369480B1 (en) | 2012-10-03 | 2020-01-01 | Nippon Shokubai Co., Ltd. | Water absorbing agent |
| JP2016506981A (ja) | 2013-01-29 | 2016-03-07 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 膨潤したゲル床の高い透過性と同時に、速い膨潤速度、かつ高い遠心分離保持容量を有する吸水性ポリマー粒子の製造方法 |
| DE102013105566A1 (de) * | 2013-05-29 | 2014-12-04 | List Holding Ag | Verfahren zur kontinuierlichen Durchführung einer Polymerisation von Monomeren oder Co-Monomeren |
| JP6521668B2 (ja) * | 2014-02-28 | 2019-05-29 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂の製造方法 |
| WO2015163438A1 (ja) * | 2014-04-25 | 2015-10-29 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂の製造方法 |
| JP6646042B2 (ja) | 2014-05-08 | 2020-02-14 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 吸水性ポリマー粒子の製造方法 |
| CN106674388A (zh) * | 2015-11-11 | 2017-05-17 | 上海其福青材料科技有限公司 | 一种降低聚乙烯吡咯烷酮中n-乙烯吡咯烷酮的方法 |
| KR20210091718A (ko) | 2018-11-29 | 2021-07-22 | 바스프 에스이 | 초흡수성 중합체의 물리적 특성 예측 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6018690B2 (ja) | 1981-12-30 | 1985-05-11 | 住友精化株式会社 | 吸水性樹脂の吸水性改良方法 |
| JPS58180233A (ja) | 1982-04-19 | 1983-10-21 | Nippon Shokubai Kagaku Kogyo Co Ltd | 吸収剤 |
| JPS6055002A (ja) * | 1983-09-07 | 1985-03-29 | Nippon Shokubai Kagaku Kogyo Co Ltd | 新規連続重合方法 |
| US4734478A (en) | 1984-07-02 | 1988-03-29 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Water absorbing agent |
| DE3537276A1 (de) * | 1985-10-19 | 1987-04-23 | Basf Ag | Verfahren zur kontinuierlichen herstellung von vernetzten feinteiligen gelfoermigen polymerisaten |
| DE3910563A1 (de) | 1989-04-01 | 1990-10-04 | Cassella Ag | Hydrophile, quellfaehige pfropfcopolymerisate, deren herstellung und verwendung |
| CA2038779A1 (en) | 1990-04-02 | 1991-10-03 | Takumi Hatsuda | Method for production of fluid stable aggregate |
| DE4020780C1 (https=) | 1990-06-29 | 1991-08-29 | Chemische Fabrik Stockhausen Gmbh, 4150 Krefeld, De | |
| JPH04220407A (ja) * | 1990-12-20 | 1992-08-11 | Dainippon Ink & Chem Inc | 高吸水性ポリマーの連続製造方法 |
| DE4138408A1 (de) | 1991-11-22 | 1993-05-27 | Cassella Ag | Hydrophile, hochquellfaehige hydrogele |
| DE4337482A1 (de) * | 1993-11-03 | 1995-05-04 | Basf Ag | Verfahren zur Herstellung von radikalisch vernetzbaren Copolymerisaten |
| DE19807502B4 (de) | 1998-02-21 | 2004-04-08 | Basf Ag | Verfahren zur Nachvernetzung von Hydrogelen mit 2-Oxazolidinonen, daraus hergestellte Hydrogele und deren Verwendung |
| US6265488B1 (en) | 1998-02-24 | 2001-07-24 | Nippon Shokubai Co., Ltd. | Production process for water-absorbing agent |
| US6503979B1 (en) | 1998-02-26 | 2003-01-07 | Basf Aktiengesellschaft | Method for cross-linking hydrogels with bis- and poly-2-oxazolidinones |
| DE19854574A1 (de) | 1998-11-26 | 2000-05-31 | Basf Ag | Verfahren zur Nachvernetzung von Hydrogelen mit N-Acyl-2-Oxazolidinonen |
| DE19854573A1 (de) | 1998-11-26 | 2000-05-31 | Basf Ag | Verfahren zur Nachvernetzung von Hydrogelen mit 2-Oxo-tetrahydro-1,3-oxazinen |
| US6239230B1 (en) | 1999-09-07 | 2001-05-29 | Bask Aktiengesellschaft | Surface-treated superabsorbent polymer particles |
| DE19955861A1 (de) * | 1999-11-20 | 2001-05-23 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von vernetzten feinteiligen gelförmigen Polymerisaten |
| AU2002210553A1 (en) * | 2000-10-19 | 2002-04-29 | Basf Aktiengesellschaft | Cross-linked, water-swellable polymer and method for producing the same |
| US6809158B2 (en) | 2000-10-20 | 2004-10-26 | Nippon Shokubai Co., Ltd. | Water-absorbing agent and process for producing the same |
| KR100909182B1 (ko) | 2001-09-12 | 2009-07-23 | 에보닉 스톡하우젠 게엠베하 | 초흡수성 중합체를 제조하기 위한 연속식 중합방법 |
| JP2005504865A (ja) | 2001-10-05 | 2005-02-17 | ビーエーエスエフ アクチェンゲゼルシャフト | モルホリン−2,3−ジオンを用いたヒドロゲルの架橋法 |
| WO2003051940A1 (en) | 2001-12-19 | 2003-06-26 | Nippon Shokubai Co., Ltd. | Acrylic acid composition and its production process, and process for producing water-absorbent resin using this acrylic acid composition, and water-absorbent resin |
| JP4084648B2 (ja) * | 2001-12-19 | 2008-04-30 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US6867269B2 (en) * | 2001-12-19 | 2005-03-15 | Nippon Shokubai Co., Ltd. | Water-absorbent resin and production process therefor |
| DE10204938A1 (de) | 2002-02-07 | 2003-08-21 | Stockhausen Chem Fab Gmbh | Verfahren zur Nachvernetzung im Bereich der Oberfläche von wasserabsorbierenden Polymeren mit beta-Hydroxyalkylamiden |
| DE10204937A1 (de) | 2002-02-07 | 2003-08-21 | Stockhausen Chem Fab Gmbh | Verfahren zur Nachvernetzung im Bereich der Oberfläche von wasserabsorbierenden Polymeren mit Harnstoffderivaten |
| DE10220494A1 (de) * | 2002-05-07 | 2003-11-20 | Basf Ag | Verfahren zur Herstellung einer wässrigen Alkaliacrylat-Lösung |
| DE60234391D1 (de) * | 2002-09-04 | 2009-12-24 | List Ag | Verfahren zur herstellung superabsorbierender polymere |
| DE10334584A1 (de) | 2003-07-28 | 2005-02-24 | Basf Ag | Verfahren zur Nachvernetzung von Hydrogelen mit bicyclischen Amidacetalen |
| JP4651926B2 (ja) * | 2003-10-03 | 2011-03-16 | 株式会社 日立ディスプレイズ | 画像表示装置 |
| KR20070003874A (ko) * | 2004-01-28 | 2007-01-05 | 바스프 악티엔게젤샤프트 | 중합체 제조방법 |
-
2005
- 2005-09-21 EP EP05796468A patent/EP1799721B1/de not_active Revoked
- 2005-09-21 WO PCT/EP2005/010188 patent/WO2006034806A1/de not_active Ceased
- 2005-09-21 EP EP09177997.5A patent/EP2166025B1/de not_active Expired - Lifetime
- 2005-09-21 US US11/662,824 patent/US20080004408A1/en not_active Abandoned
- 2005-09-21 CN CN200580032773.7A patent/CN101031591B/zh not_active Expired - Lifetime
- 2005-09-21 AT AT05796468T patent/ATE534671T1/de active
- 2005-09-21 JP JP2007533913A patent/JP4560087B2/ja not_active Expired - Lifetime
- 2005-09-21 EP EP09177995A patent/EP2166024A1/de not_active Withdrawn
- 2005-09-21 EP EP09177994.2A patent/EP2166023B1/de not_active Expired - Lifetime
- 2005-09-28 TW TW094133757A patent/TW200618859A/zh unknown
-
2010
- 2010-05-13 JP JP2010110985A patent/JP5322997B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP2166025A1 (de) | 2010-03-24 |
| ATE534671T1 (de) | 2011-12-15 |
| EP2166025B1 (de) | 2013-09-04 |
| WO2006034806A1 (de) | 2006-04-06 |
| EP1799721A1 (de) | 2007-06-27 |
| JP2008537555A (ja) | 2008-09-18 |
| CN101031591B (zh) | 2012-05-23 |
| JP5322997B2 (ja) | 2013-10-23 |
| EP2166023B1 (de) | 2014-06-04 |
| JP2010196069A (ja) | 2010-09-09 |
| JP4560087B2 (ja) | 2010-10-13 |
| US20080004408A1 (en) | 2008-01-03 |
| EP2166023A1 (de) | 2010-03-24 |
| EP2166024A1 (de) | 2010-03-24 |
| EP1799721B1 (de) | 2011-11-23 |
| CN101031591A (zh) | 2007-09-05 |
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