SU621318A3 - Способ приготовлени растворов или суспензий хлористого цианура в водосодержащих органических растворител х - Google Patents
Способ приготовлени растворов или суспензий хлористого цианура в водосодержащих органических растворител хInfo
- Publication number
- SU621318A3 SU621318A3 SU752191013A SU2191013A SU621318A3 SU 621318 A3 SU621318 A3 SU 621318A3 SU 752191013 A SU752191013 A SU 752191013A SU 2191013 A SU2191013 A SU 2191013A SU 621318 A3 SU621318 A3 SU 621318A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- cyanuric chloride
- acetone
- solution
- temperature
- chloride
- Prior art date
Links
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 title description 42
- 239000002904 solvent Substances 0.000 title description 20
- 239000000725 suspension Substances 0.000 title description 17
- 238000000034 method Methods 0.000 title description 8
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 59
- 239000000243 solution Substances 0.000 description 33
- 239000000203 mixture Substances 0.000 description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
- 238000006460 hydrolysis reaction Methods 0.000 description 14
- 230000007062 hydrolysis Effects 0.000 description 13
- 239000007788 liquid Substances 0.000 description 11
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- -1 .a-cyclohexane Chemical compound 0.000 description 6
- 239000011521 glass Substances 0.000 description 6
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 5
- 238000001816 cooling Methods 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 description 1
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- ZCJAYDKWZAWMPR-UHFFFAOYSA-N 1-chloro-2-fluorobenzene Chemical compound FC1=CC=CC=C1Cl ZCJAYDKWZAWMPR-UHFFFAOYSA-N 0.000 description 1
- YTCGOUNVIAWCMG-UHFFFAOYSA-N 1-chloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=CC(Cl)=C1 YTCGOUNVIAWCMG-UHFFFAOYSA-N 0.000 description 1
- HFGHRUCCKVYFKL-UHFFFAOYSA-N 4-ethoxy-2-piperazin-1-yl-7-pyridin-4-yl-5h-pyrimido[5,4-b]indole Chemical compound C1=C2NC=3C(OCC)=NC(N4CCNCC4)=NC=3C2=CC=C1C1=CC=NC=C1 HFGHRUCCKVYFKL-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- 206010016807 Fluid retention Diseases 0.000 description 1
- 101000942133 Homo sapiens Leupaxin Proteins 0.000 description 1
- 102100032755 Leupaxin Human genes 0.000 description 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 1
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical class ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 239000002152 aqueous-organic solution Substances 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 150000008422 chlorobenzenes Chemical class 0.000 description 1
- 230000021615 conjugation Effects 0.000 description 1
- 150000001924 cycloalkanes Chemical class 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hcl hcl Chemical compound Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- OVARTBFNCCXQKS-UHFFFAOYSA-N propan-2-one;hydrate Chemical compound O.CC(C)=O OVARTBFNCCXQKS-UHFFFAOYSA-N 0.000 description 1
- 229910002059 quaternary alloy Inorganic materials 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
- PXXNTAGJWPJAGM-UHFFFAOYSA-N vertaline Natural products C1C2C=3C=C(OC)C(OC)=CC=3OC(C=C3)=CC=C3CCC(=O)OC1CC1N2CCCC1 PXXNTAGJWPJAGM-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Paper (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2454910A DE2454910C3 (de) | 1974-11-20 | 1974-11-20 | Verfahren und Vorrichtung zum Herstellen von Lösungen oder Suspensionen von Cyanurchlorid in wasserhaltigen organischen Lösungsmitteln |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU621318A3 true SU621318A3 (ru) | 1978-08-25 |
Family
ID=5931280
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752191013A SU621318A3 (ru) | 1974-11-20 | 1975-11-20 | Способ приготовлени растворов или суспензий хлористого цианура в водосодержащих органических растворител х |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US4017413A (OSRAM) |
| JP (1) | JPS5180879A (OSRAM) |
| AT (1) | AT345296B (OSRAM) |
| BE (1) | BE835743A (OSRAM) |
| CA (1) | CA1036160A (OSRAM) |
| CH (1) | CH625513A5 (OSRAM) |
| DD (1) | DD122383A5 (OSRAM) |
| DE (1) | DE2454910C3 (OSRAM) |
| FR (1) | FR2291972A1 (OSRAM) |
| GB (1) | GB1524537A (OSRAM) |
| NL (1) | NL7513237A (OSRAM) |
| RO (1) | RO70804A (OSRAM) |
| SU (1) | SU621318A3 (OSRAM) |
| YU (2) | YU41809B (OSRAM) |
| ZA (1) | ZA757296B (OSRAM) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1593543A (en) * | 1977-05-10 | 1981-07-15 | Agfa Gevaert | Hardening of proteinaceous materials |
| DE2850339C2 (de) * | 1978-11-20 | 1981-02-26 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von 2-Alkoxy-4,6-dichlor-s-triazinen |
| DE2850243C2 (de) * | 1978-11-20 | 1984-09-20 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Suspensionen von Cyanurchlorid in organischen Lösungsmitteln |
| DE2850271C3 (de) | 1978-11-20 | 1981-10-01 | Degussa Ag, 6000 Frankfurt | Vorrichtung zur intensiven Mischung von Flüssigkeiten |
| DE2850242C2 (de) * | 1978-11-20 | 1984-10-04 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Suspensionen von Cyanurchlorid in Wasser |
| DE2850308C2 (de) * | 1978-11-20 | 1984-09-20 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Suspensionen oder Lösungen von Cyanurchlorid in wasserhaltigen organischen Lösungsmitteln |
| DE4232117A1 (de) * | 1992-09-25 | 1994-03-31 | Degussa | Verfahren zur Herstellung von Suspensionen von Cyanurchlorid in wäßrigen Flüssigkeiten |
| US5629528A (en) | 1996-01-16 | 1997-05-13 | Varian Associates, Inc. | Charged particle beam system having beam-defining slit formed by rotating cyclinders |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE390201C (de) * | 1921-05-30 | 1924-02-14 | Chemische Ind Ges | Verfahren zur Herstellung von Kondensationsprodukten der Anthrachinonreihe |
| FR1411816A (fr) * | 1964-08-11 | 1965-09-24 | Electro Chimie Soc D | Procédé d'obtention de chlorure de cyanuryle purifié à partir de mélanges gazeux le contenant |
| DE1670731B2 (de) * | 1966-08-11 | 1974-01-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung einer von Lösungsmitteln freien, wäßrigen, neutralen Cyanurchlorid-Suspension |
| YU32536B (en) * | 1967-02-17 | 1975-02-28 | Agripat Sa | Pastopek za izdelavo raztopine cianurklorida |
| DE1670568A1 (de) * | 1967-07-07 | 1972-02-24 | Degussa | Verfahren zur Herstellung von substituierten 2-Mercapto-4,6-dichlor-s-triazinen |
| DE1670289B2 (de) * | 1967-11-28 | 1977-02-10 | Basf Ag, 6700 Ludwigshafen | S-triazinderivate |
| US3539565A (en) * | 1968-01-29 | 1970-11-10 | Geigy Chem Corp | Method for producing a solution of cyanuric chloride from gaseous cyanuric chloride |
| DE1695117C3 (de) * | 1968-02-09 | 1974-01-17 | Ciba-Geigy Ag, Basel (Schweiz) | Verfahren zur Herstellung von Chloramino-s-triazinen |
| DK125471B (da) * | 1968-03-20 | 1973-02-26 | Ciba Geigy Ag | 2-Chlor-4-tert.butylamino-6-cyclopropylamino-s-triazin til anvendelse i midler til bekæmpelse af vandukrudt og af ukrudt og ugræs i bomuldskulturer. |
| CH546247A (de) * | 1968-12-27 | 1974-02-28 | Agripat Sa | Adiabatisches verfahren zur herstellung von n-monosubstituierten 2,4-dichlor-6-amino-s-triazinen. |
| US3883515A (en) * | 1969-12-29 | 1975-05-13 | Ciba Geigy Corp | Adiabatic process for the production of 2,4-dichloro-6-amino-S-triazines |
| US3741729A (en) * | 1970-03-26 | 1973-06-26 | Ciba Geigy Corp | Apparatus for producing a solution of cyanuric chloride from gaseous cyanuric chloride |
| CH550546A (de) * | 1971-08-05 | 1974-06-28 | Ciba Geigy Ag | Herbizides mittel. |
| DE2162064A1 (de) * | 1971-12-14 | 1973-06-20 | Sueddeutsche Kalkstickstoff | Verfahren zur gewinnung von festem cyanurchlorid |
| BE793389A (fr) * | 1971-12-27 | 1973-06-27 | Degussa | Composes de phenylenediamine-s-triazine et leur utilisation |
| DD111378A5 (OSRAM) * | 1973-06-27 | 1975-02-12 |
-
1974
- 1974-11-20 RO RO7483987A patent/RO70804A/ro unknown
- 1974-11-20 DE DE2454910A patent/DE2454910C3/de not_active Expired
-
1975
- 1975-10-31 GB GB45253/75A patent/GB1524537A/en not_active Expired
- 1975-11-07 YU YU2814/75A patent/YU41809B/xx unknown
- 1975-11-12 NL NL7513237A patent/NL7513237A/xx not_active Application Discontinuation
- 1975-11-18 US US05/632,952 patent/US4017413A/en not_active Expired - Lifetime
- 1975-11-18 DD DD189531A patent/DD122383A5/xx unknown
- 1975-11-19 CH CH1499875A patent/CH625513A5/de not_active IP Right Cessation
- 1975-11-19 AT AT880575A patent/AT345296B/de not_active IP Right Cessation
- 1975-11-19 BE BE6045257A patent/BE835743A/xx not_active IP Right Cessation
- 1975-11-20 CA CA240,152A patent/CA1036160A/en not_active Expired
- 1975-11-20 FR FR7535496A patent/FR2291972A1/fr active Granted
- 1975-11-20 ZA ZA757296A patent/ZA757296B/xx unknown
- 1975-11-20 SU SU752191013A patent/SU621318A3/ru active
- 1975-11-20 JP JP50139713A patent/JPS5180879A/ja active Pending
-
1983
- 1983-02-09 YU YU00303/83A patent/YU30383A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2454910A1 (de) | 1976-08-12 |
| RO70804A (ro) | 1980-08-15 |
| YU41809B (en) | 1988-02-29 |
| BE835743A (fr) | 1976-05-19 |
| FR2291972B1 (OSRAM) | 1977-12-16 |
| AT345296B (de) | 1978-09-11 |
| YU281475A (en) | 1984-02-29 |
| YU30383A (en) | 1986-02-28 |
| DD122383A5 (OSRAM) | 1976-10-05 |
| JPS5180879A (OSRAM) | 1976-07-15 |
| ATA880575A (de) | 1978-01-15 |
| NL7513237A (nl) | 1976-05-24 |
| GB1524537A (en) | 1978-09-13 |
| DE2454910C3 (de) | 1985-11-21 |
| CA1036160A (en) | 1978-08-08 |
| ZA757296B (en) | 1976-11-24 |
| DE2454910B2 (de) | 1980-03-20 |
| US4017413A (en) | 1977-04-12 |
| CH625513A5 (OSRAM) | 1981-09-30 |
| FR2291972A1 (fr) | 1976-06-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0158798B1 (en) | Method and apparatus for recovering thermal energy | |
| Brown et al. | Hydrides of boron. XI. The reaction of diborane with organic compounds containing a carbonyl group | |
| SU621318A3 (ru) | Способ приготовлени растворов или суспензий хлористого цианура в водосодержащих органических растворител х | |
| KR20080106079A (ko) | 알칼리 금속 알콕사이드의 제조 방법 | |
| Maass et al. | The Properties of Pure Hydrogen Peroxide. I. | |
| CN112429772A (zh) | 一种氟化锆的纯化方法 | |
| US3404162A (en) | Perfluoro-2-oxo-3, 6-dimethyl-1, 4-dioxane | |
| US7230142B1 (en) | Process for purifying fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether | |
| US4827027A (en) | Separation/purification of salicyclic acid | |
| Baxter et al. | The Vapor Pressure of Iodine Between 50° and 95°. | |
| JPH02108682A (ja) | フルフラールの製造および濃縮方法 | |
| Forbes et al. | Relations Between Distribution Ratio, Temperature and Concentration in System: Water, Ether, Succinic Acid. | |
| TW557296B (en) | Separating off trioxane from gaseous mixtures with formaldehyde | |
| US3629997A (en) | Process for producing methanol-formaldehyde solution of low-water content | |
| US2647914A (en) | Manufacture of an alkyl nitrate | |
| JPH0365152B2 (OSRAM) | ||
| US2012787A (en) | Process for absorbing isobutylene | |
| US5035775A (en) | Ultrapure hydrazine production | |
| USRE25057E (en) | Preparation of peracetic acid | |
| US4839103A (en) | Method for obtaining a solution of nuclear fuel not readily dissovable, especially of PuOhd 2 or (U/Pu)O2 mixed oxide | |
| US3372192A (en) | Preparation of fluorine-guanidines and bi-guanides | |
| JPH05979A (ja) | カシユー殻液の分離精製方法 | |
| SU536197A1 (ru) | Способ получени высокомолекул рных сополимеров формальдегида | |
| US3781304A (en) | Production of trioxane | |
| US3296309A (en) | Process for stabilizino an aqueous formaldehyde solution |