SU411111A1 - - Google Patents

Info

Publication number

SU411111A1

SU411111A1 SU1725409A SU1725409A SU411111A1 SU 411111 A1 SU411111 A1 SU 411111A1 SU 1725409 A SU1725409 A SU 1725409A SU 1725409 A SU1725409 A SU 1725409A SU 411111 A1 SU411111 A1 SU 411111A1

Authority

SU

USSR - Soviet Union

Prior art keywords

dye

weight

disulfonic acid

diphenylguanidine

salt

Prior art date

1971-12-13

Links

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• WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 9
• 239000000975 dye Substances 0.000 description 9
• 150000003839 salts Chemical class 0.000 description 8
• OWRCNXZUPFZXOS-UHFFFAOYSA-N 1,3-diphenylguanidine Chemical compound C=1C=CC=CC=1NC(=N)NC1=CC=CC=C1 OWRCNXZUPFZXOS-UHFFFAOYSA-N 0.000 description 6
• 239000000047 product Substances 0.000 description 6
• 239000002253 acid Substances 0.000 description 5
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• RBTKNAXYKSUFRK-UHFFFAOYSA-N heliogen blue Chemical compound [Cu].[N-]1C2=C(C=CC=C3)C3=C1N=C([N-]1)C3=CC=CC=C3C1=NC([N-]1)=C(C=CC=C3)C3=C1N=C([N-]1)C3=CC=CC=C3C1=N2 RBTKNAXYKSUFRK-UHFFFAOYSA-N 0.000 description 4
• 238000000034 method Methods 0.000 description 4
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 235000019445 benzyl alcohol Nutrition 0.000 description 3
• DIRCCMJPRSFUPX-UHFFFAOYSA-N copper 2,11,20,29,38,40-hexaza-37,39-diazanidanonacyclo[28.6.1.13,10.112,19.121,28.04,9.013,18.022,27.031,36]tetraconta-1(36),2,4(9),5,7,10(40),11,13,15,17,19,21(38),22(27),23,25,28,30,32,34-nonadecaene-6,25-disulfonic acid Chemical compound [Cu++].OS(=O)(=O)c1ccc2c3nc(nc4[n-]c(nc5nc(nc6[n-]c(n3)c3ccccc63)c3ccc(cc53)S(O)(=O)=O)c3ccccc43)c2c1 DIRCCMJPRSFUPX-UHFFFAOYSA-N 0.000 description 3
• 150000007530 organic bases Chemical class 0.000 description 3
• 239000001007 phthalocyanine dye Substances 0.000 description 3
• 239000011541 reaction mixture Substances 0.000 description 3
• QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 2
• VVBLNCFGVYUYGU-UHFFFAOYSA-N 4,4'-Bis(dimethylamino)benzophenone Chemical compound C1=CC(N(C)C)=CC=C1C(=O)C1=CC=C(N(C)C)C=C1 VVBLNCFGVYUYGU-UHFFFAOYSA-N 0.000 description 2
• RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
• KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
• 239000007900 aqueous suspension Substances 0.000 description 2
• 239000010949 copper Substances 0.000 description 2
• 229910052802 copper Inorganic materials 0.000 description 2
• 238000001035 drying Methods 0.000 description 2
• 238000001914 filtration Methods 0.000 description 2
• 239000012535 impurity Substances 0.000 description 2
• 229910052500 inorganic mineral Inorganic materials 0.000 description 2
• 238000004898 kneading Methods 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• 238000002844 melting Methods 0.000 description 2
• 230000008018 melting Effects 0.000 description 2
• 239000011707 mineral Substances 0.000 description 2
• 238000002156 mixing Methods 0.000 description 2
• 239000003960 organic solvent Substances 0.000 description 2
• XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 238000006277 sulfonation reaction Methods 0.000 description 2
• AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 description 2
• 229910001369 Brass Inorganic materials 0.000 description 1
• OBINFTYONZIMAY-UHFFFAOYSA-N N',N'-diethyl-N-(2-phenyldiazenylphenyl)ethane-1,2-diamine Chemical compound CCN(CC)CCNC1=CC=CC=C1N=NC2=CC=CC=C2 OBINFTYONZIMAY-UHFFFAOYSA-N 0.000 description 1
• JLTDJTHDQAWBAV-UHFFFAOYSA-N N,N-dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 description 1
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
• 239000001045 blue dye Substances 0.000 description 1
• 239000010951 brass Substances 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 150000001879 copper Chemical class 0.000 description 1
• 235000011950 custard Nutrition 0.000 description 1
• 150000002500 ions Chemical class 0.000 description 1
• -1 monoethyl a-naphthylamine Chemical compound 0.000 description 1
• AJDUTMFFZHIJEM-UHFFFAOYSA-N n-(9,10-dioxoanthracen-1-yl)-4-[4-[[4-[4-[(9,10-dioxoanthracen-1-yl)carbamoyl]phenyl]phenyl]diazenyl]phenyl]benzamide Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2NC(=O)C(C=C1)=CC=C1C(C=C1)=CC=C1N=NC(C=C1)=CC=C1C(C=C1)=CC=C1C(=O)NC1=CC=CC2=C1C(=O)C1=CC=CC=C1C2=O AJDUTMFFZHIJEM-UHFFFAOYSA-N 0.000 description 1
• 230000003647 oxidation Effects 0.000 description 1
• 238000007254 oxidation reaction Methods 0.000 description 1
• 239000003495 polar organic solvent Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000725 suspension Substances 0.000 description 1
• 239000001043 yellow dye Substances 0.000 description 1