RU2005132817A - Способ изготовления изделий с покрытием и изделия с покрытием, изготовленные этим способом - Google Patents

Способ изготовления изделий с покрытием и изделия с покрытием, изготовленные этим способом Download PDF

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Publication number
RU2005132817A
RU2005132817A RU2005132817/03A RU2005132817A RU2005132817A RU 2005132817 A RU2005132817 A RU 2005132817A RU 2005132817/03 A RU2005132817/03 A RU 2005132817/03A RU 2005132817 A RU2005132817 A RU 2005132817A RU 2005132817 A RU2005132817 A RU 2005132817A
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RU
Russia
Prior art keywords
layer
coating
product according
protective coating
alumina
Prior art date
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RU2005132817/03A
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English (en)
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RU2359928C2 (ru
Inventor
Джеймс Дж. ФИНЛИ (US)
Джеймс Дж. ФИНЛИ
Джеймс П. ТИЛЬ (US)
Джеймс П. ТИЛЬ
Original Assignee
Ппг Индастриз Огайо, Инк. (Us)
Ппг Индастриз Огайо, Инк.
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Publication of RU2005132817A publication Critical patent/RU2005132817A/ru
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Publication of RU2359928C2 publication Critical patent/RU2359928C2/ru

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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/58—After-treatment
    • C23C14/5806—Thermal treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10009—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets
    • B32B17/10036—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets comprising two outer glass sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10165—Functional features of the laminated safety glass or glazing
    • B32B17/10174—Coatings of a metallic or dielectric material on a constituent layer of glass or polymer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
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    • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
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    • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
    • B32B17/10761—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing vinyl acetal
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3618—Coatings of type glass/inorganic compound/other inorganic layers, at least one layer being metallic
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
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    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3639—Multilayers containing at least two functional metal layers
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3644—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the metal being silver
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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    • C03C17/3652—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the coating stack containing at least one sacrificial layer to protect the metal from oxidation
    • C—CHEMISTRY; METALLURGY
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    • C03C17/3657—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating having optical properties
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    • C—CHEMISTRY; METALLURGY
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    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3681—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating being used in glazing, e.g. windows or windscreens
    • C—CHEMISTRY; METALLURGY
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    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
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    • C03C17/38—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal at least one coating being a coating of an organic material
    • C—CHEMISTRY; METALLURGY
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    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/42—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating of an organic material and at least one non-metal coating
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/26—Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
    • Y10T428/263—Coating layer not in excess of 5 mils thick or equivalent
    • Y10T428/264—Up to 3 mils
    • Y10T428/265—1 mil or less
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31511—Of epoxy ether
    • Y10T428/31515—As intermediate layer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
    • Y10T428/31627—Next to aldehyde or ketone condensation product
    • Y10T428/3163—Next to acetal of polymerized unsaturated alcohol [e.g., formal butyral, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31678—Of metal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31786—Of polyester [e.g., alkyd, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
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Claims (47)

1. Ламинированное изделие, включающее первую подложку, имеющую первую главную поверхность; конструкционное покрытие, образованное поверх по меньшей мере части первой главной поверхности, при этом конструкционное покрытие включает по меньшей мере одну содержащую оксид металла покровную пленку и по меньшей мере одну отражающую инфракрасные лучи металлическую пленку; защитное покрытие, образованное поверх по меньшей мере части конструкционного покрытия, при этом защитное покрытие включает от 0 до 100 вес.% оксида алюминия и от 0 до 100 вес.% оксида кремния, причем защитное покрытие имеет толщину в пределах от 100 Е до 5 мкм и конструкционное покрытие и защитное покрытие образуют блок покрытий; вторую подложку; и полимерный материал, расположенный между защитным слоем и второй подложкой, причем защитное покрытие имеет показатель преломления в пределах ±0,2 по отношению к показателю преломления полимерного материала.
2. Изделие по п.1, в котором по меньшей мере одна из первой и второй подложек выбрана из стекла, пластика, металла, керамики и их комбинаций.
3. Изделие по п.1, в котором изделие является автомобильной прозрачной деталью.
4. Изделие по п.1, в котором конструкционное покрытие обладает излучательной способностью в пределах от более 0 до 0,1.
5. Изделие по п.1, в котором защитное покрытие увеличивает излучательную способность блока покрытий до по меньшей мере 0,3.
6. Изделие по п.1, в котором защитное покрытие имеет показатель преломления в пределах ±0,2 по отношению к показателю преломления полимерного материала.
7. Изделие по п.1, в котором полимерный материал включает по меньшей мере один полимер, выбираемый из поливинилового, полиуретанового, полиэстерного, акрилового и эпокси-полимеров.
8. Изделие по п.1, в котором защитное покрытие имеет неравномерную толщину.
9. Изделие по п.1, в котором первая и вторая подложки содержат стекло, конструкционное покрытие включает солнцезащитное покрытие, полимерный материал включает поливинилбутираль, и защитное покрытие имеет показатель преломления в пределах 1,5±0,1.
10. Изделие по п.1, в котором защитное покрытие содержит от 15 до 70 вес.% оксида алюминия и от 85 до 30 вес.% оксида кремния.
11. Изделие по п.1, в котором защитное покрытие включает первый слой, образованный поверх конструкционного покрытия, и второй слой, образованный поверх первого слоя, при этом первый слой содержит от 50 до 100 вес.% оксида алюминия и от 50 до 0 вес.% оксида кремния и где второй слой содержит от 50 до 100 вес.% оксида алюминия и от 50 до 0 вес.% оксида кремния.
12. Изделие по п.11, в котором первый слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
13. Изделие по п.12, в котором первый слой имеет толщину в пределах от 50 Е до 1 μм.
14. Изделие по п.13, в котором первый слой имеет толщину в пределах от 100 до 250 Е.
15. Изделие по п.11, в котором второй слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
16. Изделие по п.15, в котором второй слой имеет толщину в пределах от 50 до 2000 Е.
17. Изделие по п.16, в котором второй слой имеет толщину в пределах от 300 до 500 Е.
18. Монолитное изделие, включающее подложку; конструкционное покрытие, образованное поверх по меньшей мере части подложки; защитное покрытие, образованное поверх по меньшей мере части конструкционного покрытия, при этом конструкционное покрытие и защитное покрытие образуют блок покрытий и защитное покрытие имеет толщину в пределах от 100 Е до 5 мкм; и полимерный материал, образованный поверх по меньшей мере части защитного покрытия, в котором защитное покрытие имеет показатель преломления существенно такой же как коэффициент преломления полимерного материала.
19. Изделие по п.18, в котором это изделие является автомобильной прозрачной деталью.
20. Изделие по п.18, в котором конструкционное покрытие обладает излучательной способностью 0,1 или меньше.
21. Изделие по п.18, в котором защитное покрытие содержит от 0 до 100 вес.% оксида алюминия и/или от 0 до 100 вес.% оксида кремния.
22. Изделие по п.21, в котором защитное покрытие содержит от 75 до 85 вес.% оксида алюминия и/или от 15 до 25 вес.% оксида кремния.
23. Изделие по п.18, в котором защитное покрытие имеет толщину в пределах от 1 до 5 мкм.
24. Изделие по п.18, в котором защитное покрытие имеет показатель преломления в пределах ±0,2 от показателя преломления межслойного материала.
25. Изделие по п.18, в котором защитное покрытие включает первый слой, образованный поверх конструкционного покрытия, и второй слой, образованный поверх первого слоя, в котором первый слой содержит от 50 до 100 вес.% оксида алюминия и от 50 до 0 вес.% оксида кремния и второй слой содержит от 50 до 100 вес.% оксида алюминия и от 50 до 0 вес.% оксида кремния.
26. Изделие по п.25, в котором первый слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
27. Изделие по п.26, в котором первый слой имеет толщину в пределах от 50 Е до 1 мкм.
28. Изделие по п.27, в котором первый слой имеет толщину в пределах от 100 до 250 Е.
29. Изделие по п.25, в котором второй слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
30. Изделие по п.29, в котором второй слой имеет толщину в пределах от 50 до 2000 Е.
31. Изделие по п.30, в котором второй слой имеет толщину в пределах от 300 до 500 Е.
32. Изделие по п.18, в котором полимерный материал содержит поливинилбутираль.
33. Изделие по п.18, в котором защитное покрытие имеет неравномерную толщину.
34. Ламинированное изделие, включающее первую подложку, имеющую первую главную поверхность; конструкционное покрытие, образованное поверх по меньшей мере части первой главной поверхности; защитное покрытие, образованное поверх по меньшей мере части конструкционного покрытия с образованием блока покрытий, в котором защитное покрытие является многослойным покрытием, включающим по меньшей мере один слой, содержащий оксид кремния, и по меньшей мере один слой, содержащий оксид алюминия; вторую подложку; и полимерный материал, расположенный между первой и второй подложками, причем защитное покрытие имеет показатель преломления существенно такой же как показатель преломления полимерного материала.
35. Способ изготовления ламинированного изделия, включающий стадии: подготовку первой подложки; образование конструкционного покрытия на по меньшей мере части первой подложки; образование защитного покрытия на по меньшей мере части конструкционного покрытия; и образование полимерного материала на по меньшей мере части защитного покрытия; в котором защитное покрытие и полимерный материал подбираются таким образом, чтобы защитное покрытие и полимерный материал имели существенно один и тот же показатель преломления.
36. Способ по п.35, в котором полимерный материал включает поливинилбутираль, защитный слой содержит от 35 до 100 вес.% оксида алюминия и от 0 до 65 вес.% оксида кремния и защитное покрытие имеет показатель преломления 1,5±0,2.
37. Способ по п.35, в котором защитное покрытие является многослойным покрытием, содержащим по меньшей мере один первый слой, включающий по меньшей мере один оксид кремния и один оксид алюминия, и по меньшей мере один другой слой, включающий по меньшей мере один оксид кремния и один оксид алюминия.
38. Способ по п.35, в котором защитное покрытие имеет толщину в пределах от 100 Е до 5 мкм.
39. Способ по п.35, включающий подготовку второго субстрата и ламинирование первой и второй подложек друг с другом с помощью полимерного материала.
40. Способ изготовления ламинированной подложки, включающий стадии подготовка первой подложки; образование конструкционного покрытия поверх по меньшей мере части первой подложки; и образование защитного покрытия поверх по меньшей мере части первой конструкционного покрытия, в котором защитное покрытие включает первый слой, образованный поверх конструкционного покрытия, и второй слой, образованный поверх первого слоя, где первый слой содержит от 50 до 100 вес.% оксида алюминия и от 50 до 0 вес.% оксида кремния и второй слой содержит от 50 до 100 вес.% оксида кремния и от 50 до 0 вес.% оксида алюминия.
41. Способ по п.40, в котором первый слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
42. Способ по п.41, в котором первый слой имеет толщину в пределах от 50 Е до 1 мкм.
43. Способ по п.42, в котором первый слой имеет толщину в пределах от 100 до 250 Е.
44. Способ по п.40, в котором второй слой содержит от 70 до 100 вес.% оксида алюминия и от 30 до 0 вес.% оксида кремния.
45. Способ по п.44, в котором второй слой имеет толщину в пределах от 50 до 2000 Е.
46. Способ по п.45, в котором второй слой имеет толщину в пределах от 300 до 500 Е.
47. Способ по п.40, дополнительно включающий подготовку второй подложки; помещение второй подложки поверх первой подложки с конструкционным покрытием, расположенным между покрытиями; и нагрев подложек для их выгиба в желаемую форму.
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