PH11998002119A1 - Processes for producing glufosinate and phosphorus-containing aminonitriles as intermediates - Google Patents

Processes for producing glufosinate and phosphorus-containing aminonitriles as intermediates

Info

Publication number
PH11998002119A1
PH11998002119A1 PH11998002119A PH11998002119A PH11998002119A1 PH 11998002119 A1 PH11998002119 A1 PH 11998002119A1 PH 11998002119 A PH11998002119 A PH 11998002119A PH 11998002119 A PH11998002119 A PH 11998002119A PH 11998002119 A1 PH11998002119 A1 PH 11998002119A1
Authority
PH
Philippines
Prior art keywords
aminonitriles
intermediates
phosphorus
processes
producing glufosinate
Prior art date
Application number
PH11998002119A
Other languages
English (en)
Inventor
Lothar Willms
Original Assignee
Hoechst Schering Agrevo Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Schering Agrevo Gmbh filed Critical Hoechst Schering Agrevo Gmbh
Publication of PH11998002119A1 publication Critical patent/PH11998002119A1/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/657163—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom
    • C07F9/657172—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom the ring phosphorus atom and one oxygen atom being part of a (thio)phosphinic acid ester: (X = O, S)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32—Esters thereof
    • C07F9/3205—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/3211—Esters of acyclic saturated acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
PH11998002119A 1997-08-20 1998-08-19 Processes for producing glufosinate and phosphorus-containing aminonitriles as intermediates PH11998002119A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19736125A DE19736125A1 (de) 1997-08-20 1997-08-20 Verfahren zur Herstellung von Glufosinate und phosphorhaltige alpha-Aminonitrile als Zwischenprodukte

Publications (1)

Publication Number Publication Date
PH11998002119A1 true PH11998002119A1 (en) 2003-10-10

Family

ID=7839559

Family Applications (1)

Application Number Title Priority Date Filing Date
PH11998002119A PH11998002119A1 (en) 1997-08-20 1998-08-19 Processes for producing glufosinate and phosphorus-containing aminonitriles as intermediates

Country Status (27)

Country Link
US (1) US6359162B1 (ko)
EP (1) EP1005475B1 (ko)
JP (1) JP4519316B2 (ko)
KR (1) KR100674326B1 (ko)
CN (1) CN1261442C (ko)
AR (1) AR015932A1 (ko)
AT (1) ATE258180T1 (ko)
AU (1) AU756471B2 (ko)
BR (1) BR9811971B1 (ko)
CA (1) CA2301181C (ko)
CO (1) CO5031316A1 (ko)
CZ (1) CZ2000593A3 (ko)
DE (2) DE19736125A1 (ko)
DK (1) DK1005475T3 (ko)
ES (1) ES2214727T3 (ko)
HU (1) HUP0003501A3 (ko)
IL (1) IL134633A0 (ko)
MY (1) MY132853A (ko)
PH (1) PH11998002119A1 (ko)
PL (1) PL191587B1 (ko)
PT (1) PT1005475E (ko)
RU (1) RU2275376C2 (ko)
TR (1) TR200000456T2 (ko)
TW (1) TW530063B (ko)
UA (1) UA66806C2 (ko)
WO (1) WO1999009039A1 (ko)
ZA (1) ZA987465B (ko)

Families Citing this family (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101516898B (zh) * 2006-09-20 2013-07-10 明治制果株式会社 含有磷的α-氨基酸的制造方法及其制造中间体
CA2796158C (en) 2010-04-14 2022-06-14 Strategic Enzyme Applications, Inc. Process for producing phosphinothricin employing nitrilases
CN102372738B (zh) * 2010-08-14 2017-11-10 武汉工程大学 Lj反应在制备维蒂希试剂和草铵膦中的应用
KR101931843B1 (ko) 2011-09-30 2018-12-21 메이지 세이카 파루마 가부시키가이샤 글루포시네이트 ｐ 유리산의 제조 방법
CN102372739B (zh) * 2011-12-05 2017-06-16 河北威远生化农药有限公司 一种草铵膦的合成方法
CN102399240A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种改进的草铵膦及类似物的合成方法
CN102399239A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种草铵膦及类似物的合成方法
CN103183707B (zh) * 2011-12-30 2016-06-15 中化蓝天集团有限公司 一种草胺膦的制备方法
CN102584893B (zh) * 2012-02-07 2015-03-04 浙江工业大学 一种草铵膦的制备方法
CN103374030B (zh) * 2012-04-13 2016-03-23 浙江新安化工集团股份有限公司 一种制备草铵膦的方法及其中间体的制备方法
CN103483379A (zh) * 2013-09-26 2014-01-01 江苏辉丰农化股份有限公司 一种草铵膦酸的制备方法
US9850263B2 (en) 2014-05-13 2017-12-26 Bayer Cropscience Aktiengesellschaft Process for preparing phosphorus containing cyanohydrins
CN104558033B (zh) * 2014-12-19 2016-05-18 浙江工业大学 一种l-草铵膦-n-羧酸酐及其制备和应用
CU24529B1 (es) 2015-04-27 2021-06-08 Bayer Cropscience Ag Combinaciones herbicidas que comprenden glufosinato e indaziflam
KR20180048662A (ko) 2015-09-02 2018-05-10 바이엘 크롭사이언스 악티엔게젤샤프트 인 함유 시아노히드린 에스테르의 제조 방법
CN108026122B (zh) 2015-09-02 2021-03-09 拜耳作物科学股份公司 制备含磷氰醇酯的方法
CN108137628B (zh) 2015-09-02 2020-10-09 拜耳农作物科学股份公司 制备含磷的氰醇酯的方法
CN108350004B (zh) 2015-09-02 2021-03-12 拜耳作物科学股份公司 含磷氰醇酯的制备方法
ES2754603T3 (es) 2015-09-29 2020-04-20 Basf Se Procedimiento para la preparación de fosfinatos
CN107236001A (zh) * 2016-04-06 2017-10-10 四川省乐山市福华通达农药科技有限公司 一种膦醛的合成方法
CN107417721B (zh) * 2016-05-24 2019-05-28 四川福思达生物技术开发有限责任公司 一种氢氰酸加成工艺
WO2018108794A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von d-glufosinat oder dessen salzen unter verwendung von ephedrin
WO2018108797A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von l-glufosinat oder dessen salzen unter verwendung von ephedrin
EP3392237B1 (de) 2017-04-21 2019-10-02 Evonik Degussa GmbH Verfahren zur herstellung von acroleincyanhydrinen
EP3655413B1 (de) 2017-07-21 2021-08-11 Basf Se Herstellung von glufosinat durch umsetzung von 3-[n-butoxy(methyl)phosphoryl]-1-cyanopropylacetat zu einer mischung aus n-butyl(3-amino-3-cyanopropyl)-methylphosphinat und (3-amino-3-cyanopropyl)-methylphosphinsäure ammoniumsalz
CN111479816B (zh) 2017-12-19 2023-10-27 巴斯夫欧洲公司 制备含磷α-氨基腈的方法
CN109134534B (zh) * 2018-08-08 2020-09-08 江苏好收成韦恩农化股份有限公司 一种3,3-二烷氧基丙基甲基膦酸酯简易制备方法
KR102131687B1 (ko) * 2018-09-10 2020-07-08 주식회사 휴런 파킨슨 병 진단 장치 및 방법
CN113316580A (zh) 2019-01-11 2021-08-27 Cj第一制糖株式会社 L-草铵膦的制备方法
CN111662324B (zh) * 2019-03-05 2023-02-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN111662325B (zh) * 2019-03-05 2023-03-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN111662326B (zh) * 2019-03-05 2023-03-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN110003269B (zh) * 2019-04-29 2022-04-05 利尔化学股份有限公司 低能耗生产草铵膦的方法
CN110590836B (zh) * 2019-09-30 2022-07-26 江苏七洲绿色化工股份有限公司 一种草铵膦中间体的合成方法
CN112898338A (zh) * 2019-12-04 2021-06-04 利尔化学股份有限公司 草铵膦中间体及草铵膦的制备方法
CN111659330B (zh) * 2020-04-23 2021-05-07 河北威远生物化工有限公司 一种连续化生产草铵膦的工艺与设备
CN112358499A (zh) * 2020-11-12 2021-02-12 江苏春江润田农化有限公司 一种草铵膦的合成方法
EP4151643A1 (en) 2021-09-16 2023-03-22 Evonik Operations GmbH Improved process for production of phosphoesters of glufosinate precursors
CN114163472A (zh) * 2021-11-27 2022-03-11 永农生物科学有限公司 醇溶剂下合成α-氨基腈的方法及草铵膦的合成方法和产品
CN116789695B (zh) * 2022-11-17 2024-03-29 永农生物科学有限公司 一种草铵膦的制备方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5484529A (en) * 1977-12-19 1979-07-05 Meiji Seika Kaisha Ltd Production of d,l-2-amino-4-methylphosphinobutyric acid
DE2849003A1 (de) 1978-11-11 1980-08-21 Hoechst Ag Phosphorhaltige cyanhydrinderivate und verfahren zu ihrer herstellung
DE3508573A1 (de) * 1985-03-11 1986-09-11 Hoechst Ag, 6230 Frankfurt Phosphorhaltige (alpha)-aminonitrile und verfahren zu ihrer herstellung
JP2615777B2 (ja) * 1987-05-26 1997-06-04 日産化学工業株式会社 ホスフィニルアミノ酸誘導体の製造方法

Also Published As

Publication number Publication date
PL338855A1 (en) 2000-11-20
CA2301181A1 (en) 1999-02-25
TR200000456T2 (tr) 2000-07-21
AR015932A1 (es) 2001-05-30
MY132853A (en) 2007-10-31
CN1261442C (zh) 2006-06-28
AU9259898A (en) 1999-03-08
RU2275376C2 (ru) 2006-04-27
KR100674326B1 (ko) 2007-01-24
HUP0003501A2 (en) 2001-03-28
BR9811971B1 (pt) 2010-12-28
ZA987465B (en) 1999-02-22
CA2301181C (en) 2008-08-05
HUP0003501A3 (en) 2002-01-28
AU756471B2 (en) 2003-01-16
US6359162B1 (en) 2002-03-19
DE19736125A1 (de) 1999-02-25
ES2214727T3 (es) 2004-09-16
BR9811971A (pt) 2000-08-15
CO5031316A1 (es) 2001-04-27
DK1005475T3 (da) 2004-05-17
JP2001515084A (ja) 2001-09-18
CN1267305A (zh) 2000-09-20
EP1005475B1 (de) 2004-01-21
DE59810636D1 (de) 2004-02-26
ATE258180T1 (de) 2004-02-15
JP4519316B2 (ja) 2010-08-04
KR20010023069A (ko) 2001-03-26
TW530063B (en) 2003-05-01
WO1999009039A1 (de) 1999-02-25
PL191587B1 (pl) 2006-06-30
UA66806C2 (uk) 2004-06-15
PT1005475E (pt) 2004-06-30
EP1005475A1 (de) 2000-06-07
CZ2000593A3 (cs) 2000-06-14
IL134633A0 (en) 2001-04-30

Similar Documents

Publication Publication Date Title
PH11998002119A1 (en) Processes for producing glufosinate and phosphorus-containing aminonitriles as intermediates
HU9801045D0 (en) Substituted diamino-carboxylic acids
PL327374A1 (en) Air distributing method
GB2328686B (en) Method for producing arylamine
HUP9801420A3 (en) Process for producing l-amino acids by fermentition
IL126054A0 (en) Process for preparing pesticidal intermediates
PL334701A1 (en) Novel method
HK1027102A1 (en) Processes for preparing pesticidal intermediates
AU2923699A (en) Continuous method for producing polyamides from aminonitriles
HUP0101072A3 (en) Method for producing polyamides from aminonitriles
AU2721399A (en) Continuous method for producing polyamides from aminonitriles
HUP0003019A3 (en) Process for preparing 4-substituted-1h-indole-3-glyoxamides and their intermediates
HUP0001444A3 (en) Process for preparing carboxamido-4-azasteroids and their intermediates
HUP0001596A3 (en) Method for producing 5-aminomethyl-2-chloropyridines
EP1032591A4 (en) INNOVATIVE pth
HUP9801597A3 (en) Method for purifying phosphorus oxichloride
HUP0003768A3 (en) Method for producing thiochloroformates
DE69829876D1 (en) Hypusin reagenz zur peptidsynthese
GB9702659D0 (en) Distillation method
KR100641508B1 (en) Improved process for the preparation of phosphites
SI0966445T1 (en) Processes for preparing pesticidal intermediates
GB9725462D0 (en) Novel method
ZA971127B (en) Distillation method
GB9702748D0 (en) Manufacture of N-phosphonomethylglycine
SI1053274T1 (en) Method for producing polyamides from aminonitriles