MX348699B - Método para el aislamiento de productos de la oligomerización de olefina y la descomposición de residuos de catalizador de oligomerización. - Google Patents
Método para el aislamiento de productos de la oligomerización de olefina y la descomposición de residuos de catalizador de oligomerización.Info
- Publication number
- MX348699B MX348699B MX2013015205A MX2013015205A MX348699B MX 348699 B MX348699 B MX 348699B MX 2013015205 A MX2013015205 A MX 2013015205A MX 2013015205 A MX2013015205 A MX 2013015205A MX 348699 B MX348699 B MX 348699B
- Authority
- MX
- Mexico
- Prior art keywords
- oligomerization
- olefin
- products
- catalyst
- isolation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
- C07C2/04—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation
- C07C2/06—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation of alkenes, i.e. acyclic hydrocarbons having only one carbon-to-carbon double bond
- C07C2/08—Catalytic processes
- C07C2/26—Catalytic processes with hydrides or organic compounds
- C07C2/32—Catalytic processes with hydrides or organic compounds as complexes, e.g. acetyl-acetonates
- C07C2/34—Metal-hydrocarbon complexes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/04—Purification; Separation; Use of additives by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/24—Chromium, molybdenum or tungsten
- B01J23/26—Chromium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
- C07C2/04—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation
- C07C2/06—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation of alkenes, i.e. acyclic hydrocarbons having only one carbon-to-carbon double bond
- C07C2/08—Catalytic processes
- C07C2/26—Catalytic processes with hydrides or organic compounds
- C07C2/32—Catalytic processes with hydrides or organic compounds as complexes, e.g. acetyl-acetonates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/148—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound
- C07C7/17—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound with acids or sulfur oxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/20—Olefin oligomerisation or telomerisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/60—Complexes comprising metals of Group VI (VIA or VIB) as the central metal
- B01J2531/62—Chromium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
- B01J31/14—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron
- B01J31/143—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron of aluminium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
- B01J31/1805—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing nitrogen
- B01J31/181—Cyclic ligands, including e.g. non-condensed polycyclic ligands, comprising at least one complexing nitrogen atom as ring member, e.g. pyridine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- C07C2531/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- C07C2531/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
- C07C2531/14—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- C07C2531/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- C07C2531/22—Organic complexes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- C07C2531/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups C07C2531/02 - C07C2531/24
- C07C2531/34—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups C07C2531/02 - C07C2531/24 of chromium, molybdenum or tungsten
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La invención se relaciona con el campo de producción de oligómeros de olefina, los cuales se usan ampliamente como copolímeros, una materia prima para la preparación de aceites y lubricantes, y también una materia prima para producir otros productos químicos; la invención se relaciona con la producción de oligómeros de olefina por medio de un método de oligomerización de olefinas, y, en particular, con un método de aislamiento de productos de oligomerización de olefina y de descomposición de residuos de catalizador de oligomerización; un método para aislar productos de una reacción de oligomerización de olefinas que comprende un doble enlace terminal, en donde la reacción se lleva a cabo por medio de la acción de un catalizador que comprende compuestos de cromo, un ligando que contiene nitrógeno y compuestos de organoaluminio, comprende un paso de aislar productos independientes de olefina y un paso de tratar residuos de catalizador, caracterizado en que el método comprende los siguientes pasos secuenciales: a) aislar al menos un producto líquido de la reacción de oligomerización de olefinas de una corriente de salida de un reactor de oligomerización; b) tratar un residuo con una solución acuosa de un ácido; y c) separar una capa orgánica y una capa acuosa; primero, el uso de los métodos propuestos permite el aislamiento de productos de reacción objetivo, evitando el ingreso de impurezas de sustancias extrañas, como alcoholes en productos y)o solvente recurrente, y la eliminación de la necesidad de la separación de estas sustancias extrañas; en segundo lugar, el uso del método propuesto hace posible evitar la contaminación de tuberías y dispositivos entre el reactor y la columna de destilación con un producto secundario; en tercer lugar, la solución hace posible separar residuos de catalizador de un subproducto de polímero, facilitando así la regeneración del catalizador o la separación de compuestos metálicos de residuos de catalizador, mientras se evita la precipitación de una resma durante la destilación de los productos de reacción de alta ebullición.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2011125946/04A RU2471762C1 (ru) | 2011-06-22 | 2011-06-22 | Способ выделения продуктов олигомеризации олефинов и разложения остатков катализатора олигомеризации |
| PCT/RU2012/000484 WO2012177183A1 (ru) | 2011-06-22 | 2012-06-21 | Способ выделения продуктов олигомеризации олефинов и разложения остатков катализатора олигомеризации |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2013015205A MX2013015205A (es) | 2014-08-18 |
| MX348699B true MX348699B (es) | 2017-06-26 |
Family
ID=47422810
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2013015205A MX348699B (es) | 2011-06-22 | 2012-06-21 | Método para el aislamiento de productos de la oligomerización de olefina y la descomposición de residuos de catalizador de oligomerización. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US9586874B2 (es) |
| EP (1) | EP2725003B1 (es) |
| JP (1) | JP5866005B2 (es) |
| KR (1) | KR101694388B1 (es) |
| CN (1) | CN103649022B (es) |
| CA (1) | CA2839862C (es) |
| EA (1) | EA024179B1 (es) |
| MX (1) | MX348699B (es) |
| RU (1) | RU2471762C1 (es) |
| WO (1) | WO2012177183A1 (es) |
| ZA (1) | ZA201309147B (es) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX2017008376A (es) * | 2014-12-23 | 2018-04-11 | Sibur Holding Public Joint Stock Co | Metodos de preparacion de oligomeros de una olefina. |
| US10508065B2 (en) * | 2014-12-23 | 2019-12-17 | Public Joint Stock Company “SIBUR Holding” | Methods of preparing oligomers of an olefin |
| KR102113798B1 (ko) * | 2014-12-23 | 2020-05-21 | 퍼블릭 조인트 스톡 컴퍼니 “시부르 홀딩” | 올레핀 올리고머화 반응에서 폴리머 및 불활성화된 유기금속 촉매의 침전 방법 |
| EP3245179A1 (en) * | 2015-01-16 | 2017-11-22 | SABIC Global Technologies B.V. | Method for emulsion removal in amine removal unit |
| MX2019005549A (es) * | 2016-11-14 | 2019-07-04 | Sibur Holding Public Joint Stock Co | Sistema catalizador usado en la oligomerizacion de olefinas y metodo para la oligomerizacion de olefinas. |
| KR102604431B1 (ko) * | 2018-07-26 | 2023-11-22 | 에스케이이노베이션 주식회사 | 선형 알파 올레핀 제조방법 |
| KR20220104418A (ko) * | 2021-01-18 | 2022-07-26 | 주식회사 엘지화학 | 올리고머 제조방법 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2650760B1 (fr) * | 1989-08-08 | 1991-10-31 | Inst Francais Du Petrole | Nouvelle composition catalytique et sa mise en oeuvre pour l'oligomerisation des monoolefines |
| DE4338415C1 (de) * | 1993-11-10 | 1995-03-16 | Linde Ag | Verfahren zur Katalysatordesaktivierung bei der katalytisch beschleunigten Herstellung linearer Alpha-Olefine durch Oligomerisierung von Ethylen |
| JP3841361B2 (ja) * | 1993-11-30 | 2006-11-01 | 三菱化学株式会社 | α−オレフイン低重合体の製造方法 |
| CA2134503C (en) * | 1994-02-18 | 2001-04-10 | Mark E. Lashier | Olefin production |
| KR100414008B1 (ko) * | 1995-03-02 | 2004-04-29 | 미쓰비시 가가꾸 가부시키가이샤 | α-올레핀올리고머의제조방법 |
| JP3632233B2 (ja) * | 1995-03-10 | 2005-03-23 | 三菱化学株式会社 | α−オレフイン低重合体の製造方法 |
| JP3549136B2 (ja) * | 1996-07-30 | 2004-08-04 | 三菱化学株式会社 | α−オレフイン低重合体の製造方法 |
| RU2123501C1 (ru) * | 1997-03-24 | 1998-12-20 | Институт химической физики в Черноголовке РАН | Способ дезактивации комплексного металлоорганического катализатора гомогенных процессов, таких как димеризация или олигомеризация этилена в линейные альфа-олефины, и его выделения из реакционной массы |
| US20020182124A1 (en) * | 1997-10-14 | 2002-12-05 | William M. Woodard | Olefin production process |
| KR20010039657A (ko) * | 1999-06-14 | 2001-05-15 | 조셉 에스. 바이크 | 폴리올레핀 내에서의 올리고머 및 겔 형성 감소 |
| RU2249585C2 (ru) | 1999-12-29 | 2005-04-10 | Филлипс Петролеум Компани | Способ олигомеризации (варианты) и способ предотвращения коррозии в процессе олигомеризации |
| KR20020084170A (ko) * | 2000-03-06 | 2002-11-04 | 이데미쓰세끼유가가꾸가부시끼가이샤 | 비닐 화합물 중합용 촉매 및 비닐 중합체의 제조 방법 |
| AU2009308790B2 (en) * | 2008-10-31 | 2015-05-07 | Chevron Phillips Chemical Company Lp | Compositions and catalyst systems of metal precursors and olefinic diluents |
| RU2430116C1 (ru) * | 2010-01-29 | 2011-09-27 | Закрытое Акционерное Общество "Сибур Холдинг" | Способ полимеризации и сополимеризации олефиновых олигомеров |
-
2011
- 2011-06-22 RU RU2011125946/04A patent/RU2471762C1/ru active
-
2012
- 2012-06-21 EA EA201490054A patent/EA024179B1/ru not_active IP Right Cessation
- 2012-06-21 KR KR1020147001565A patent/KR101694388B1/ko active IP Right Grant
- 2012-06-21 WO PCT/RU2012/000484 patent/WO2012177183A1/ru active Application Filing
- 2012-06-21 CN CN201280030039.7A patent/CN103649022B/zh not_active Expired - Fee Related
- 2012-06-21 JP JP2014516947A patent/JP5866005B2/ja not_active Expired - Fee Related
- 2012-06-21 US US14/128,352 patent/US9586874B2/en active Active
- 2012-06-21 MX MX2013015205A patent/MX348699B/es active IP Right Grant
- 2012-06-21 CA CA2839862A patent/CA2839862C/en not_active Expired - Fee Related
- 2012-06-21 EP EP12802942.8A patent/EP2725003B1/en not_active Not-in-force
-
2013
- 2013-12-05 ZA ZA2013/09147A patent/ZA201309147B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2725003B1 (en) | 2016-11-02 |
| US9586874B2 (en) | 2017-03-07 |
| EP2725003A1 (en) | 2014-04-30 |
| EP2725003A4 (en) | 2014-11-26 |
| KR101694388B1 (ko) | 2017-01-10 |
| JP2014525900A (ja) | 2014-10-02 |
| RU2471762C1 (ru) | 2013-01-10 |
| ZA201309147B (en) | 2014-08-27 |
| EA024179B1 (ru) | 2016-08-31 |
| CN103649022A (zh) | 2014-03-19 |
| KR20140047665A (ko) | 2014-04-22 |
| JP5866005B2 (ja) | 2016-02-17 |
| CA2839862C (en) | 2016-11-08 |
| EA201490054A1 (ru) | 2014-04-30 |
| WO2012177183A1 (ru) | 2012-12-27 |
| CN103649022B (zh) | 2015-11-25 |
| MX2013015205A (es) | 2014-08-18 |
| CA2839862A1 (en) | 2012-12-27 |
| US20140121435A1 (en) | 2014-05-01 |
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| HC | Change of company name or juridical status |
Owner name: IMPACT TECHNOLOGY SYSTEMS AS.* |
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| FG | Grant or registration |