MX2017006297A - Procesos para producir un producto de acido acetico que tiene bajo contenido de acetato de butilo. - Google Patents

Procesos para producir un producto de acido acetico que tiene bajo contenido de acetato de butilo.

Info

Publication number
MX2017006297A
MX2017006297A MX2017006297A MX2017006297A MX2017006297A MX 2017006297 A MX2017006297 A MX 2017006297A MX 2017006297 A MX2017006297 A MX 2017006297A MX 2017006297 A MX2017006297 A MX 2017006297A MX 2017006297 A MX2017006297 A MX 2017006297A
Authority
MX
Mexico
Prior art keywords
acetic acid
butyl acetate
acid product
producing
acetate content
Prior art date
Application number
MX2017006297A
Other languages
English (en)
Inventor
O Scates Mark
Hwa LIU Yaw-
Original Assignee
Celanese Int Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Int Corp filed Critical Celanese Int Corp
Publication of MX2017006297A publication Critical patent/MX2017006297A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/46—Ruthenium, rhodium, osmium or iridium
    • B01J23/464—Rhodium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08—Acetic acid

Abstract

Un proceso para producir un producto de ácido acético que tiene un contenido bajo de acetato de butilo mediante una reacción de carbonilación. La reacción de carbonilación se lleva a cabo a una temperatura de 100 a 300°C, una presión parcial de hidrógeno de 0.3 a 2 atm, y una concentración de catalizador de rodio de 100 a 3,000 ppm en peso, tomando como base el peso del medio de reacción. La concentración de acetato de butilo en el producto de ácido acético se puede controlar retirando el acetaldehído de una corriente derivada a partir del medio de reacción y/o ajustando por lo menos uno de temperatura de reacción, presión parcial de hidrógeno, y concentración de catalizador metálico.
MX2017006297A 2014-11-14 2015-10-02 Procesos para producir un producto de acido acetico que tiene bajo contenido de acetato de butilo. MX2017006297A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201462079991P 2014-11-14 2014-11-14
US14/694,932 US9260369B1 (en) 2014-11-14 2015-04-23 Processes for producing acetic acid product having low butyl acetate content
PCT/US2015/053843 WO2016076972A1 (en) 2014-11-14 2015-10-02 Processes for producing an acetic acid product having low butyl acetate content

Publications (1)

Publication Number Publication Date
MX2017006297A true MX2017006297A (es) 2017-08-21

Family

ID=55275322

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2017006297A MX2017006297A (es) 2014-11-14 2015-10-02 Procesos para producir un producto de acido acetico que tiene bajo contenido de acetato de butilo.

Country Status (12)

Country Link
US (4) US9260369B1 (es)
EP (1) EP3218344B1 (es)
JP (3) JP2016094384A (es)
KR (1) KR102465082B1 (es)
CN (2) CN107108433A (es)
ES (1) ES2846182T3 (es)
MX (1) MX2017006297A (es)
MY (1) MY181881A (es)
RS (1) RS61473B1 (es)
SA (1) SA517381516B1 (es)
SG (1) SG11201703427QA (es)
WO (1) WO2016076972A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
US9540304B2 (en) 2014-11-14 2017-01-10 Celanese International Corporation Processes for producing an acetic acid product having low butyl acetate content
MY187274A (en) 2017-01-18 2021-09-17 Daicel Corp Method for producing acetic acid
US10457622B2 (en) 2017-03-08 2019-10-29 Daicel Corporation Method for producing acetic acid
CN110114331A (zh) * 2017-03-08 2019-08-09 株式会社大赛璐 乙酸的制备方法
BR112019017941A2 (pt) 2017-03-22 2020-05-19 Daicel Corp método para produzir ácido acético
JP6588657B1 (ja) * 2018-05-02 2019-10-09 株式会社ダイセル 酢酸の製造方法
JP6626988B1 (ja) * 2018-05-29 2019-12-25 株式会社ダイセル 酢酸の製造方法
WO2019229857A1 (ja) 2018-05-29 2019-12-05 株式会社ダイセル 酢酸の製造方法

Family Cites Families (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
FR2496644A1 (fr) 1980-12-24 1982-06-25 Rhone Poulenc Ind Procede de preparation de l'anhydride acetique
US4733006A (en) 1980-12-29 1988-03-22 Monsanto Company Carbonylation process with an alkali metal acetate as catalyst stabilizer
US4792620A (en) * 1983-10-14 1988-12-20 Bp Chemicals Limited Carbonylation catalysts
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US5001259A (en) * 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US4615806B1 (en) 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
JPH0487284A (ja) 1990-07-30 1992-03-19 Mitsubishi Electric Corp 避雷器切離し装置
AU8790391A (en) 1990-11-19 1992-05-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
CA2093752C (en) 1992-04-15 1999-06-15 David W. Studer Integrated process for oxygenated acetyl compounds from synthesis gas via dimethyl ether
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
US5672743A (en) 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
JP3377555B2 (ja) 1993-05-31 2003-02-17 ダイセル化学工業株式会社 カルボニル化反応生成物に含有されるヨウ素化合物の除去方法
TW283702B (es) 1993-07-08 1996-08-21 Daicel Chem
JP3244351B2 (ja) 1993-07-08 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
JP3244350B2 (ja) 1993-07-08 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
JP3244385B2 (ja) * 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
US5625095A (en) * 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
US5696284A (en) 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof
US5783731A (en) 1995-09-11 1998-07-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
EP0920407B1 (en) 1995-10-27 2002-12-11 Hoechst Celanese Corporation Process for improving productivity of a carbonylation catalyst solution by removing corrosion metals
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
IN192600B (es) 1996-10-18 2004-05-08 Hoechst Celanese Corp
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
GB9626429D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626428D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626317D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
US6066762A (en) 1996-12-30 2000-05-23 Chiyoda Corporation Process for the production of carbonyl compound
JPH10231267A (ja) 1997-02-19 1998-09-02 Chiyoda Corp 有機カルボン酸の製造方法
JPH10237009A (ja) 1997-02-28 1998-09-08 Mitsubishi Gas Chem Co Inc ギ酸メチルからの酢酸の製造方法
KR100378643B1 (ko) 1998-03-31 2003-04-03 할도르 토프쉐 에이/에스 아세트산의 제조방법
US6211405B1 (en) 1998-10-23 2001-04-03 Celanese International Corporation Addition of iridium to the rhodium/inorganic iodide catalyst system
US6303813B1 (en) * 1999-08-31 2001-10-16 Celanese International Corporation Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile
US6225498B1 (en) 2000-03-24 2001-05-01 Celanese International Corporation Method of removing organic iodides from organic media
US6657078B2 (en) * 2001-02-07 2003-12-02 Celanese International Corporation Low energy carbonylation process
JP2004131389A (ja) 2002-10-08 2004-04-30 Daicel Chem Ind Ltd カルボン酸の製造方法及び製造システム
US7005541B2 (en) 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
JP4526381B2 (ja) 2004-12-27 2010-08-18 ダイセル化学工業株式会社 酢酸の製造方法
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
US7989659B2 (en) 2007-05-17 2011-08-02 Celanese International Corporation Method and apparatus for making acetic acid with improved light ends column productivity
WO2008153708A2 (en) * 2007-05-21 2008-12-18 Celanese International Corporation Reaction product of rhodium-catalyzed methanol carbonylation
US8062482B2 (en) 2007-10-30 2011-11-22 Celanese International Corporation Acetaldehyde removal from methyl acetate by distillation at elevated pressure
EP2303447B1 (en) 2008-04-29 2014-10-15 Celanese International Corporation Methanol carbonylation system having absorber with multiple solvent options
US7884237B2 (en) 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8889904B2 (en) 2010-05-18 2014-11-18 Celanese International Corporation Processes for producing acetic acid
KR101747484B1 (ko) 2010-07-26 2017-06-14 주식회사 다이셀 아세트산의 제조 방법
WO2012046593A1 (ja) 2010-10-06 2012-04-12 ダイセル化学工業株式会社 酢酸の製造方法
MX338849B (es) 2010-12-15 2016-05-02 Daicel Corp Procedimiento para producir acido acetico.
ES2651953T3 (es) 2010-12-15 2018-01-30 Daicel Corporation Método de producción de ácido acético
CN103370297B (zh) 2010-12-15 2015-10-07 株式会社大赛璐 乙酸的制备方法
KR101865436B1 (ko) 2010-12-24 2018-06-07 주식회사 다이셀 아세트산의 제조 방법
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
US9193657B2 (en) 2012-08-17 2015-11-24 Celanese International Corporation Catalyst stability in carbonylation processes
WO2014097867A1 (ja) 2012-12-21 2014-06-26 株式会社ダイセル 酢酸の製造方法
AR094541A1 (es) 2013-01-25 2015-08-12 Daicel Corp Procedimiento para producir ácido carboxílico
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
US10183905B2 (en) 2015-09-29 2019-01-22 Daicel Corporation Method for producing acetic acid
US11014868B2 (en) 2016-03-01 2021-05-25 Daicel Corporation Method for producing acetic acid

Also Published As

Publication number Publication date
US10173955B2 (en) 2019-01-08
EP3218344A1 (en) 2017-09-20
US9776942B2 (en) 2017-10-03
US11014867B2 (en) 2021-05-25
KR20170083617A (ko) 2017-07-18
US20190119190A1 (en) 2019-04-25
SG11201703427QA (en) 2017-05-30
SA517381516B1 (ar) 2021-11-24
RS61473B1 (sr) 2021-03-31
CN107108433A (zh) 2017-08-29
JP2022110086A (ja) 2022-07-28
CN116143604A (zh) 2023-05-23
WO2016076972A1 (en) 2016-05-19
ES2846182T3 (es) 2021-07-28
US20170349522A1 (en) 2017-12-07
US20160159721A1 (en) 2016-06-09
JP2018030831A (ja) 2018-03-01
KR102465082B1 (ko) 2022-11-09
US9260369B1 (en) 2016-02-16
EP3218344B1 (en) 2020-11-25
MY181881A (en) 2021-01-12
JP2016094384A (ja) 2016-05-26
JP7108385B2 (ja) 2022-07-28

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