MX167955B - Metodo para elaborar microemulsiones de polidiorganosiloxano - Google Patents

Metodo para elaborar microemulsiones de polidiorganosiloxano

Info

Publication number
MX167955B
MX167955B MX004619A MX461986A MX167955B MX 167955 B MX167955 B MX 167955B MX 004619 A MX004619 A MX 004619A MX 461986 A MX461986 A MX 461986A MX 167955 B MX167955 B MX 167955B
Authority
MX
Mexico
Prior art keywords
polydiorganosiloxane
water
crystalline
emulsion
microemulsions
Prior art date
Application number
MX004619A
Other languages
English (en)
Inventor
Daniel Graiver
Osamu Tanaka
Original Assignee
Dow Corning
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning filed Critical Dow Corning
Publication of MX167955B publication Critical patent/MX167955B/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/06Preparatory processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04Polysiloxanes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2383/00Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2383/04Polysiloxanes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S516/00Colloid systems and wetting agents; subcombinations thereof; processes of
    • Y10S516/924Significant dispersive or manipulative operation or step in making or stabilizing colloid system
    • Y10S516/928Mixing combined with non-mixing operation or step, successively or simultaneously, e.g. heating, cooling, ph change, ageing, milling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Silicon Polymers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

La presente invención se refiere a un método para elaborar microemulsiones cristalinas, estables, acuosas de polidiorganosiloxano, caracterizado porque consiste de: añadir en secuencia una emulsión del precursor que consiste de ciclopolidiorganosiloxano, un surfacante y agua, un medio de polimerización que consiste de agua y una cantidad efectiva de un catalizador de polimerización mientras que se mezcla, en donde el régimen de adición de la emulsión del precursor es efectiva para formar una microemulsión cristalina, estable, que contiene gotitas de polidiorganosloxano de un tamaño promedio menor de 0.15 micrones, y que contiene una relación en peso de suficiente a polidioganosloxano de 0.15 a 5.
MX004619A 1985-12-12 1986-12-10 Metodo para elaborar microemulsiones de polidiorganosiloxano MX167955B (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US80909085A 1985-12-12 1985-12-12

Publications (1)

Publication Number Publication Date
MX167955B true MX167955B (es) 1993-04-26

Family

ID=25200515

Family Applications (1)

Application Number Title Priority Date Filing Date
MX004619A MX167955B (es) 1985-12-12 1986-12-10 Metodo para elaborar microemulsiones de polidiorganosiloxano

Country Status (10)

Country Link
US (1) US5817714A (es)
EP (1) EP0228575B1 (es)
JP (1) JPS62141029A (es)
KR (1) KR940007865B1 (es)
AU (1) AU598215B2 (es)
BR (1) BR8606152A (es)
CA (1) CA1328139C (es)
DE (1) DE3687704T2 (es)
ES (1) ES2053431T3 (es)
MX (1) MX167955B (es)

Families Citing this family (32)

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JPS63153108A (ja) * 1986-07-22 1988-06-25 Toray Silicone Co Ltd 離型剤
JPS63130512A (ja) * 1986-11-18 1988-06-02 Toray Silicone Co Ltd 化粧料
US4935464A (en) * 1987-04-30 1990-06-19 Toray Silicone Company Limited Organopolysiloxane microemulsion, process for its production and application thereof
US4824890A (en) * 1988-02-02 1989-04-25 Dow Corning Corporation Film forming silicone microemulsions
JP2750899B2 (ja) * 1989-06-19 1998-05-13 東レ・ダウコーニング・シリコーン株式会社 シクロヘキシルアミノ基合有オルガノポリシロキサンマイクロエマルジョンの製造方法
FR2658094A1 (fr) * 1990-02-14 1991-08-16 Rhone Poulenc Chimie Procede de preparation d'emulsions, du type huile dans eau, monodisperses.
CA2041599A1 (en) * 1990-06-01 1991-12-02 Michael Gee Method for making polysiloxane emulsions
US5071573A (en) * 1990-07-23 1991-12-10 The Procter & Gamble Company Microemulsified silicones in liquid fabric care compositions containing dye
US5173201A (en) * 1990-07-23 1992-12-22 The Proctor & Gamble Company Microemulsified amine functional silicone in liquid fabric softeners for reducing fiber-fiber and yarn-yarn friction in fabrics
JPH0615613B2 (ja) * 1990-08-23 1994-03-02 信越化学工業株式会社 オルガノポリシロキサンマイクロエマルジョンの製造方法
JPH0615612B2 (ja) * 1990-08-23 1994-03-02 信越化学工業株式会社 オルガノポリシロキサンマイクロエマルジョンの製造方法
JPH05132566A (ja) * 1991-11-13 1993-05-28 Shin Etsu Chem Co Ltd ジオルガノポリシロキサンミクロエマルジヨンの製造方法
US5504149A (en) * 1994-08-25 1996-04-02 Dow Corning Corporation Method of emulsion polymerization
US5661215A (en) * 1995-07-26 1997-08-26 Dow Corning Corporation Microemulsions of gel-free polymers
US5726270A (en) * 1996-12-26 1998-03-10 General Electric Company Process for the synthesis of mono-modal aqueous dispersions of polysiloxanes
US5856402A (en) * 1996-12-30 1999-01-05 General Electric Company Process for the synthesis of multi-modal aqueous dispersions of polysiloxanes
US5925469A (en) * 1997-12-18 1999-07-20 Dow Corning Corporation Organopolysiloxane emulsions
DE19803468A1 (de) 1998-01-29 1999-08-05 Wacker Chemie Gmbh Durch Michael-Addition-ähnliche Reaktionen vernetzte Aminosiliconölemulsionen
TWI222455B (en) * 1998-02-13 2004-10-21 Kanegafuchi Chemical Ind Aqueous emulsion containing silicone rubber particles and process for preparing the same
KR100592008B1 (ko) * 1998-08-12 2006-06-21 신에쓰 가가꾸 고교 가부시끼가이샤 오르가노폴리실록산 에멀젼의 제조 방법
CN1325537C (zh) * 1998-12-07 2007-07-11 通用电气公司 乳液聚合硅橡胶-基冲击改性剂、制备方法及其共混物
US6013683A (en) * 1998-12-17 2000-01-11 Dow Corning Corporation Single phase silicone and water compositions
US6071975A (en) * 1999-01-11 2000-06-06 Dow Corning Corporation Method of preparing silicone oil-in-water microemulsions
DE10011564C1 (de) * 2000-03-09 2001-09-27 Goldschmidt Ag Th Verfahren zur Herstellung von Polyorganosiloxanemulsionen
FR2821282A1 (fr) * 2001-02-23 2002-08-30 Univ Paris Curie Microemulsions et emulsions monodisperses a base de polyosiloxanes, procede de preparation et compositions en comportant
US6525130B1 (en) * 2001-09-24 2003-02-25 Omnova Solutions Inc. Polymerization of silicone in a surfactant medium
WO2006081978A1 (en) * 2005-02-02 2006-08-10 Wacker Chemie Ag Manufacture of stable low particle size organopolysiloxane emulsion
US20060280716A1 (en) * 2005-06-10 2006-12-14 Czech Anna M Cationic aminosilicone emulsions
US9694214B2 (en) * 2008-04-16 2017-07-04 Dow Corning Corporation Preparation of silicone microemulsions
BR112013022310A2 (pt) 2011-03-03 2019-09-24 Dow Corning emulsões bimodais
WO2012119068A2 (en) 2011-03-03 2012-09-07 Dow Corning Corporation Bi-modal emulsions
KR20150086284A (ko) 2012-11-21 2015-07-27 다우 코닝 코포레이션 이중모드 에멀젼을 포함하는 화장품 조성물

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2891920A (en) * 1955-01-26 1959-06-23 Dow Corning Polymerization of organopolysiloxanes in aqueous emulsion
NL204267A (es) * 1955-02-07
GB1024024A (en) * 1963-04-08 1966-03-30 Dow Corning Improvements in or relating to polymerising or co-polymerising organosilicon compounds
NL133796C (es) * 1965-01-21 1900-01-01
FR2205358B1 (es) * 1972-11-03 1976-04-23 Rhone Poulenc Ind
US4052331A (en) * 1972-11-03 1977-10-04 Rhone-Poulenc S.A. Surface active composition
US4146499A (en) * 1976-09-18 1979-03-27 Rosano Henri L Method for preparing microemulsions
JPS54131661A (en) * 1978-04-05 1979-10-12 Toray Silicone Co Ltd Organopolysiloxane latex composition
JPS55144052A (en) * 1979-04-28 1980-11-10 Dainippon Ink & Chem Inc Production of stable organopolysiloxane emulsion polymeric liquid
GB2079300B (en) * 1980-07-01 1984-04-26 Gen Electric Transparent silicone emulsions
DE3024870C2 (de) * 1980-07-01 1985-01-10 Th. Goldschmidt Ag, 4300 Essen Verfahren zur Herstellung einer stabilen Emulsion
JPS58204028A (ja) * 1982-05-21 1983-11-28 Shin Etsu Chem Co Ltd オルガノシランまたはオルガノシロキサンの乳化重合方法
US4472291A (en) * 1983-03-07 1984-09-18 Rosano Henri L High viscosity microemulsions
US4529758A (en) * 1983-05-05 1985-07-16 General Electric Company Water based resin dispersions
US4620878A (en) * 1983-10-17 1986-11-04 Dow Corning Corporation Method of preparing polyorganosiloxane emulsions having small particle size
JPS6088040A (ja) * 1983-10-21 1985-05-17 Mitsubishi Rayon Co Ltd ポリオルガノシロキサンラテツクスの製法
US4999398A (en) * 1985-12-12 1991-03-12 Dow Corning Corporation Methods for making polydiorganosiloxane microemulsions
US4784665A (en) * 1986-07-24 1988-11-15 Toray Silicone Co., Ltd. Agent for the treatment of fibers
US4842766A (en) * 1987-02-17 1989-06-27 Dow Corning Corporation Silane microemulsions
US4935464A (en) * 1987-04-30 1990-06-19 Toray Silicone Company Limited Organopolysiloxane microemulsion, process for its production and application thereof
US4824877A (en) * 1988-02-02 1989-04-25 Dow Corning Corporation High polymer content silicone emulsions
US5106900A (en) * 1990-11-15 1992-04-21 General Electric Company Method and organopolysiloxane/organic polymeric compositions obtained therefrom

Also Published As

Publication number Publication date
KR940007865B1 (ko) 1994-08-26
JPS62141029A (ja) 1987-06-24
US5817714A (en) 1998-10-06
EP0228575A3 (en) 1988-05-11
AU598215B2 (en) 1990-06-21
EP0228575A2 (en) 1987-07-15
EP0228575B1 (en) 1993-02-03
BR8606152A (pt) 1987-09-22
DE3687704T2 (de) 1993-08-19
DE3687704D1 (de) 1993-03-18
CA1328139C (en) 1994-03-29
JPH0471097B2 (es) 1992-11-12
ES2053431T3 (es) 1994-08-01
AU6650586A (en) 1987-06-18
KR870005682A (ko) 1987-07-06

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