MA61705A1 - Procédé de préparation d'un précurseur ternaire - Google Patents
Procédé de préparation d'un précurseur ternaireInfo
- Publication number
- MA61705A1 MA61705A1 MA61705A MA61705A MA61705A1 MA 61705 A1 MA61705 A1 MA 61705A1 MA 61705 A MA61705 A MA 61705A MA 61705 A MA61705 A MA 61705A MA 61705 A1 MA61705 A1 MA 61705A1
- Authority
- MA
- Morocco
- Prior art keywords
- seed crystal
- salt
- precursor
- stirring
- crystal
- Prior art date
Links
- 239000002243 precursor Substances 0.000 title abstract 6
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000013078 crystal Substances 0.000 abstract 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 6
- 239000000243 solution Substances 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 3
- 238000003756 stirring Methods 0.000 abstract 3
- 230000032683 aging Effects 0.000 abstract 2
- 150000001868 cobalt Chemical class 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 150000002696 manganese Chemical class 0.000 abstract 2
- 229910052751 metal Inorganic materials 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 2
- 150000002815 nickel Chemical class 0.000 abstract 2
- 239000012266 salt solution Substances 0.000 abstract 2
- 239000000725 suspension Substances 0.000 abstract 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 239000000908 ammonium hydroxide Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 239000011164 primary particle Substances 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/006—Compounds containing, besides nickel, two or more other elements, with the exception of oxygen or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Nickelates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/50—Agglomerated particles
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Abstract
La présente invention concerne un procédé de préparation d'un précurseur ternaire, comprenant : tout d'abord, le mélange d'une première solution de sel métallique contenant un sel de nickel, un sel de cobalt et un sel de manganèse solubles, de l'hydroxyde d'ammonium et une solution d'hydroxyde de sodium, la régulation du ph, la réaction sous chauffage et agitation, et le vieillissement et la filtration d'une suspension épaisse obtenue pour obtenir un germe cristallin précurseur ; et ensuite, l'introduction du germe cristallin précurseur dans une solution acide diluée pour agitation, la filtration en vue d'obtenir un germe cristallin acidifié, le mélange d'une seconde solution de sel métallique contenant le sel de nickel, le sel de cobalt et le sel de manganèse solubles, la solution d'hydroxyde de sodium, et le germe cristallin acidifié, l'ajustement du ph, la réaction sous chauffage et agitation, et le vieillissement, la filtration et le séchage de la suspension épaisse obtenue pour obtenir le précurseur ternaire. Selon la présente invention, le germe cristallin précurseur est placé dans la solution acide diluée pour être agité, de sorte que la micropoudre amorphe sur la surface du germe cristallin est dissoute, une structure cristalline se développe, et les particules primaires deviennent également plus fines et plus minces dans la condition de lixiviation acide, créant ainsi des conditions favorables pour la croissance continue d'une plaquette le long de la surface du germe cristallin dans le processus ultérieur sans ammoniac.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110944650.1A CN113697868B (zh) | 2021-08-17 | 2021-08-17 | 一种三元前驱体的制备方法 |
PCT/CN2022/095671 WO2023020063A1 (fr) | 2021-08-17 | 2022-05-27 | Procédé de préparation d'un précurseur ternaire |
Publications (1)
Publication Number | Publication Date |
---|---|
MA61705A1 true MA61705A1 (fr) | 2024-01-31 |
Family
ID=78653196
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MA61705A MA61705A1 (fr) | 2021-08-17 | 2022-05-27 | Procédé de préparation d'un précurseur ternaire |
Country Status (6)
Country | Link |
---|---|
US (1) | US20240025760A1 (fr) |
CN (1) | CN113697868B (fr) |
DE (1) | DE112022000279T5 (fr) |
GB (1) | GB2618684A (fr) |
MA (1) | MA61705A1 (fr) |
WO (1) | WO2023020063A1 (fr) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113697868B (zh) * | 2021-08-17 | 2022-11-15 | 广东邦普循环科技有限公司 | 一种三元前驱体的制备方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103746110A (zh) * | 2014-01-26 | 2014-04-23 | 中国科学院长春应用化学研究所 | 一种镍钴锰三元材料的制备方法和锂离子电池正极材料 |
CN105399154A (zh) * | 2015-11-25 | 2016-03-16 | 兰州金川新材料科技股份有限公司 | 一种镍钴锰三元氢氧化物的生产方法 |
CN108807968A (zh) * | 2018-08-09 | 2018-11-13 | 中国恩菲工程技术有限公司 | 镍钴锰三元前驱体材料及其合成方法 |
CN108807976A (zh) * | 2018-08-09 | 2018-11-13 | 中国恩菲工程技术有限公司 | 窄粒径分布的镍钴锰三元材料前驱体材料及其制备方法 |
CN109546144B (zh) * | 2018-11-29 | 2020-07-31 | 广东佳纳能源科技有限公司 | 三元前驱体的制备方法及其应用 |
CN109896550B (zh) * | 2019-04-29 | 2021-06-22 | 中钢集团南京新材料研究院有限公司 | 一种三元前驱体废液回收利用制备铁红的方法 |
CN111003734A (zh) * | 2019-12-25 | 2020-04-14 | 南通金通储能动力新材料有限公司 | 一种三元前驱体废料回收再利用的方法 |
CN113697868B (zh) * | 2021-08-17 | 2022-11-15 | 广东邦普循环科技有限公司 | 一种三元前驱体的制备方法 |
-
2021
- 2021-08-17 CN CN202110944650.1A patent/CN113697868B/zh active Active
-
2022
- 2022-05-27 DE DE112022000279.4T patent/DE112022000279T5/de active Pending
- 2022-05-27 MA MA61705A patent/MA61705A1/fr unknown
- 2022-05-27 GB GB2310058.9A patent/GB2618684A/en active Pending
- 2022-05-27 WO PCT/CN2022/095671 patent/WO2023020063A1/fr active Application Filing
-
2023
- 2023-09-28 US US18/374,544 patent/US20240025760A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
CN113697868B (zh) | 2022-11-15 |
WO2023020063A1 (fr) | 2023-02-23 |
CN113697868A (zh) | 2021-11-26 |
GB202310058D0 (en) | 2023-08-16 |
DE112022000279T5 (de) | 2023-11-02 |
US20240025760A1 (en) | 2024-01-25 |
GB2618684A (en) | 2023-11-15 |
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