KR940703724A - 매우 얇은 연속 무정형 알루미늄 수화 산화물의 코팅물을 갖는 자기 입자로 제조된 자기 기록 매체(Magnetic recording media prepared from magnetic particles having an extremely thin, continuous amorphous, aluminum hydrous oxide coating) - Google Patents

매우 얇은 연속 무정형 알루미늄 수화 산화물의 코팅물을 갖는 자기 입자로 제조된 자기 기록 매체(Magnetic recording media prepared from magnetic particles having an extremely thin, continuous amorphous, aluminum hydrous oxide coating)

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KR940703724A
KR940703724A KR1019940702376A KR19940702376A KR940703724A KR 940703724 A KR940703724 A KR 940703724A KR 1019940702376 A KR1019940702376 A KR 1019940702376A KR 19940702376 A KR19940702376 A KR 19940702376A KR 940703724 A KR940703724 A KR 940703724A
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range
coating
aqueous
magnetic particles
particles
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KR1019940702376A
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잭 지. 트루옹
토머스 이. 우드
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라저 로이 탬트
미네소타 마이닝 앤드 매뉴팩츄어링 컴패니
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Publication of KR940703724A publication Critical patent/KR940703724A/ko

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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/032Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
    • H01F1/10Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials non-metallic substances, e.g. ferrites, e.g. [(Ba,Sr)O(Fe2O3)6] ferrites with hexagonal structure
    • H01F1/11Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials non-metallic substances, e.g. ferrites, e.g. [(Ba,Sr)O(Fe2O3)6] ferrites with hexagonal structure in the form of particles
    • H01F1/112Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials non-metallic substances, e.g. ferrites, e.g. [(Ba,Sr)O(Fe2O3)6] ferrites with hexagonal structure in the form of particles with a skin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/08Metallic powder characterised by particles having an amorphous microstructure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/16Metallic particles coated with a non-metal
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/62Record carriers characterised by the selection of the material
    • G11B5/68Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent
    • G11B5/70Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer
    • G11B5/712Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the surface treatment or coating of magnetic particles
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/44Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of magnetic liquids, e.g. ferrofluids
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/90Magnetic feature
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/25Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/25Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
    • Y10T428/256Heavy metal or aluminum or compound thereof
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/25Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
    • Y10T428/256Heavy metal or aluminum or compound thereof
    • Y10T428/257Iron oxide or aluminum oxide
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991Coated
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991Coated
    • Y10T428/2998Coated including synthetic resin or polymer

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  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Dermatology (AREA)
  • General Health & Medical Sciences (AREA)
  • Paints Or Removers (AREA)
  • Hard Magnetic Materials (AREA)
  • Magnetic Record Carriers (AREA)

Abstract

제 1 특징으로서, 본 발명은 코팅된 자기 입자를 제조하는 방법에 관한 것이다. 상기 방법에 의하며, 무정형 가수분해된 알루미늄 함유 콜로이드 입자의 수성 졸을 자기 입자를 포함한 수성 현택액과 혼합한다. 무정형가수분해된 알루미늄 함유 콜로이드 입자의 평균 입자 크기는 약 0.5 내지 5㎚범위내이며, 이의 평균 가수분해도는 1.5 내지 약 3범위내이다. 혼합하는 동안, 무정형 가수분해된 알루미늄 함유 콜로이드 입자는 자기 입자상에 연속 무정형 알루미늄 수화 산화물의 코팅물을 형성하며, 이때, 코팅물의 평균 두께는 약 0.5 내지 약 5㎚범위내이다. 또한, 본 발명은 코팅된 자기 입자에 관한 것이다. 본 발명에 의한 코팅된 자기 입자는 자기화 코어 및 상기 자기화 코어상에 형성된 연속 무정형 알루미늄 수화 산화물의 코팅물을 포함한다. 코팅물의 평균 두께는 약 0.5 내지 약 5㎚범위내이다. 제 2 특징으로서, 본 발명은 비자기화 지지체상에 형성된 자기 층을 포함하는 자기 기록 매체에 관한 것이다. 자기 층은 중합체 결합제에 분산되어 있는 상기 설명되어 있는 코팅된 자기 입자를 포함한다.

Description

매우 얇은 연속 무정형 알루미늄 수화 산화물의 코팅물을 갖는 자기 입자로 제조된 자기 기록 매체(Magnetic recording media prepared from magnetic particles having an extremely thin, continuous, amorphous, aluminum hydrous oxide coating)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (11)

  1. a)자기 입자의 수성 현탁액을 제공하고 ; b)평균 입자 지경이 약 0.5 내지 5㎚범위내이고, 평균 가수분해도가 약 1.5 내지 약 3범위내인 무정형 가수분해된 알루미늄 함유 콜로이드 입자를 포함하는 수성 졸을 제공하고 ; c)상기 수성 졸을 상기 입자 수성 현탁액과 혼합하는 단계를 포함하여 상기 무정형 가수분해된 알루미늄 함유 콜로이드 입자가 자기 입자상에서 연속 무정형 알루미늄 수화 산화물의 코팅물을 형성하며, 상기 코팅물의 평균 두께가 약 0.5 내지 5㎚범위내인 코팅된 자기 입자를 제조하는 방법.
  2. 제 1 항에 있어서, 상기 무정형 가수분해된 알루미늄 함유 콜로이드 입자의 평균 입자 지경이 약 2㎚인 방법.
  3. 제 1 항에 있어서, 상기 자기 입자의 수성 현탁액이 전해질을 부가로 포함하며, 상기 전해질의 농도가 OM 내지 약 0.1M범위내인 방법.
  4. 제 1 항에 있어서, 염기성 알루미늄 염 수용액을 순한 염기 수용액과 반응시켜 상기 수성 졸을 제조하는 방법.
  5. 제 4 항에 있어서, 상기 순한 염기 수용액이 0.03M 내지 0.25M범위내의 농도로 중탄산 암모늄을 포함하는 방법.
  6. 제 5 항에 있어서, 상기 염기성 알루미늄 염 용액을 순한 염기 수용액과 반응시키기 전에, 상기 염기성 알루미늄 염 용액을 30℃ 내지 130℃범위내의 온도에서 1분 내지 2시간 범위내의 시간동안 예열시키는 방법.
  7. a)자기화 코어 ; 및 b)상기 자기화 코어상에 형성되고, 평균 두께가 약 0.5 내지 5㎚ 범위내인 연속 무정형 알루미늄 수화 산화물의 코팅물을 포함하는 자기 기록에 적합한 코팅된 복합재료 입자.
  8. 제 7 항에 있어서, 상기 연속 무정형 알루미늄 수화 산화물 코팅물의 평균 두께가 약 2㎚인 코팅된 복합재료 입자.
  9. 중합체 결합제에 분산되어 있는 코팅된 복합재료 입자를 포함하는 자기화층이 비자기화 지지체상에 형성되어 있고, 상기 코팅된 복합재료 입자가 a)자기화 코어 ; 및 b)상기 자기화 코어상에 형성되고, 평균 두께가 약 0.5 내지 5㎚ 범위내인 연속 무정형 알루미늄 수화 산화물의 코팅물을 포함하는 자기 기록 매체.
  10. 제 9 항에 있어서, 상기 중합체 결합제가 측쇄 산성 또는 이온성 부분을 포함하고, 상기 친수성기가 -SO3M, -OSO3M, -COOM, -PO(OM')2, 4차 암모늄기 및 OH로 구성된 군에서 선택되고, M이 수소, Na, K, Li 또는 암모늄이고, M'이 수소, Na, K, Li, 암모늄 또는 저급 알킬기인 자기 기록 매체.
  11. 제 9 항에 있어서, 상기 연속 무정형 알루미늄 수화산화물의 코팅물의 두께가 약 2㎚인 자기 기록 매체.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019940702376A 1992-01-10 1992-12-14 매우 얇은 연속 무정형 알루미늄 수화 산화물의 코팅물을 갖는 자기 입자로 제조된 자기 기록 매체(Magnetic recording media prepared from magnetic particles having an extremely thin, continuous amorphous, aluminum hydrous oxide coating) KR940703724A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US818,852 1992-01-10
US07/818,852 US5965194A (en) 1992-01-10 1992-01-10 Magnetic recording media prepared from magnetic particles having an extremely thin, continuous, amorphous, aluminum hydrous oxide coating
PCT/US1992/010810 WO1993013896A1 (en) 1992-01-10 1992-12-14 Magnetic recording media prepared from magnetic particles having an extremely thin, continuous, amorphous, aluminum hydrous oxide coating

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KR940703724A true KR940703724A (ko) 1994-12-12

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Country Status (14)

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US (2) US5965194A (ko)
EP (1) EP0620772B1 (ko)
JP (1) JPH07502864A (ko)
KR (1) KR940703724A (ko)
CN (1) CN1075818A (ko)
AU (1) AU3279793A (ko)
BR (1) BR9207032A (ko)
CA (1) CA2126453A1 (ko)
DE (1) DE69213763T2 (ko)
ES (1) ES2093403T3 (ko)
IL (1) IL104191A0 (ko)
MX (1) MX9300058A (ko)
TW (1) TW221510B (ko)
WO (1) WO1993013896A1 (ko)

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WO1993013896A1 (en) 1993-07-22
EP0620772A1 (en) 1994-10-26
ES2093403T3 (es) 1996-12-16
US5965194A (en) 1999-10-12
MX9300058A (es) 1993-09-01
DE69213763D1 (de) 1996-10-17
IL104191A0 (en) 1993-05-13
US6136428A (en) 2000-10-24
BR9207032A (pt) 1995-12-05
DE69213763T2 (de) 1997-04-10
JPH07502864A (ja) 1995-03-23

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